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Coating Methods
Coating is a very Important process involved in Manufacture of  Coated Products Today we shall review some of these as listed below. Gravure Coating Comma Coating Reverse Roll Coating Hot Melt Coating Metering Rod  / Myer Bar Coating Knife over roll coating Slot  Orifice coating Immersion  / Dip coating Curtain Coating
To understand the process of coating an adhesive on a  substrate for the manufacture  of Adhesive tape  is  quite simple .  Let’s quote the example spreading butter on bread.  The Butter  must have good spread ability in order to apply  it evenly . Try spreading frozen butter on bread and you will learn the difficulties encountered. Similarly, the adhesive to be coated must have good  spread ablity .  And let’s not forget one must have a  correct equipment  to spread or coat the adhesive. There are other variable factors  also involved , but we shall look into coating methods  Exclusively.
The Coating methods  Their Capabilities and Limitations 20-100 200 500-20000 Slot Orifice 3.-25. 200 10-200 Myer Bar 10-300 300 500-20000 Hot Melt 10-200 300 1000-6000 Reverse Roll Nip 10-200 100 200-6000 Reverse Roll Pan 10-200 300 1000-6000 Comma 3.-20. 700  Mtrs. 100-2000 Gravure 20-100 200 500-20000 Curtain Heavy 50 1000-10000 Immersion / Dip Coating 3.-15. 1500 100-20000 Knife over Roll Coating Wt .  gm per sq. mtr Max Speed  per Min Viscosity  in CPS Coating  Method
Gravure Coating The  gravure coating process   relies on an engraved roller running in a coating bath, which fills the engraved dots or lines of the roller with the coating material.  The excess coating on the roller is wiped off by the  Doctor Blade  and the coating is then deposited onto the substrate as it passes between  the  Engraved roller  and a  Pressure Roller . There are three different ways of gravure roll manufacturing . One has to  choose a correct type depending upon the required coating gram mage and the material to be coated
 
CHARACTERISTICS  OF  ENGRAVED  GRAVURE ROLLERS 11.7 63.1 0.010 0.055 47 9 120 24 Trihelical 3.6 49.5 0.005 0.065 79 6 200 16 Quadrangular 2.4 27.6 0.003 0.037 79 16 200 40 Pyramidal Lines/cm Lines/in Deposit gm/m 2 Cell Depth mm Screen Type of Engraving
Pyramidal cells Quadrangular Tri helical
Comma Coating
Reverse Roll Coating
Reverse Roll Coating In this procedure, the  coating material  is measured onto  the  applicator roller  by precision setting of the gap between  the upper  metering roller  and the application roller below it.  The coating is  'wiped'  off the application roller by  the substrate as it passes around the  support roller at the bottom.  The diagram illustrates a 3-roll reverse roll coating process,  although 4-roll versions are common.
Reverse Roll Coater  The three roll reverse coater is used for many specialty applications. This method  is more expensive and generally slower in line speed than the Mayer rod coater.  However, the versatility in terms of coat weight range and coating width, and the  good coat quality of the three roll reverse has made it popular with many converters.  In this process, the middle roll is coated with a precise thickness of adhesive,  determined by the size of the gap between the top and middle rolls. The adhesive  is then transferred as the rubber backing roll brings the web into contact.  The adhesive coat weight can also be varied by increasing or decreasing the  speed of the applicator roll relative to the web speed. The metering roll speed  can be varied to adjust the smoothness of the coating.                                                                                         Figure 2  : Reverse Roll Coater  There are several variations of the reverse roll coating method, such as four-roll,  nip fed, and pan fed systems. A nip-fed, three roll reverse coater is shown here.  Medium to high coat weights are possible with reverse roll.
 
Myer Bar Coating In this coating process, an excess of the coating is deposited  onto the substrate as it passes over the bath roller.  The wire-wound metering rod, sometimes known as a  Meyer Rod, allows the desired quantity of the coating to  remain on the substrate.  The quantity is determined by the diameter of the wire used on the rod.  This process is remarkably tolerant of non-precision engineering of the other components of the coating machine .
 
The market for wire-wound rods has grown rapidly during the past few decades,  because they provide predictable, accurate coatings time after time, at a minimal cost. Although the technology goes back almost a century, today's high quality materials,  multi-wire designs and special wire surfaces have made this system more popular than ever before.   Rods give users the ability to fine-tune coating thickness quickly and easily, without altering the chemistry of their coating material, and without time-consuming  and expensive changeovers.     Wire-wound rods were first used in coating machines built by Charles Mayer in the  1900's to manufacture waxed paper and carbon paper. They are still called "Mayer Bars“ by many coaters.     Wet coating thickness can be accurately predicted within one tenth of a mil (.0001"). Rod selection tables allow coaters to consider coat weight and percent of solids in  choosing the proper rod size for each production run.     Bottom-line profits have encouraged many coaters to modify existing machines,  in order to take advantage of the flexibility, the ease of use and the dollar savings  associated with rod coating.
Coating Rods are accurate easy to use inexpensive
One of the more common methods of coating is the Mayer rod coater,  sometimes called a metering rod coater. This equipment has advantages such  as low capital cost, ease of coat weight adjustment, ease of operation, and  a broad range of coat weights are possible.                                                                                           
 
 
Figure 1  : Mayer Road Coater  In this coating method, an applicator roll delivers adhesive to the substrate being coated. The applicator roll may turn either with or against the primary web,  delivering an excess of adhesive. Wire wound rods are then used to remove  the excess. The rods may also turn in either direction.  The amount of adhesive removed depends upon the diameter of the wire which  is wound around the steel rod. Coat weight is increased by simply switching to a rod wrapped with larger diameter wire. Two rods in series often give better  coating results than a single rod. The first rod has larger diameter wire and removes most of the excess adhesive. The second rod, with smaller diameter wire,  smoothes the coating and produces the final desired coat weight. Mayer rod coating can deliver a broad range of coat weights.
 
      Where heavier coatings are required, manufactures provide special drawdown rods with two wires. A standard single-wire rod is over wound with a smaller wire which follows the spiral of the base wire. The result is a modified groove between the wires that will produce wet coatings up to 19 mils (.019") thick. TWO-WIRE DRAWDOWN RODS
Three Rod technology developed by  for Coatings up to 56 mils (.056") thick can be produced, using three standard wires wound in a unique configuration. Two wires are wound side by side on a core rod, then a third wire follows one spiral of the base wires. The resulting groove will maximize the area between the wires, producing a coating more than six times the thickness produced by a single-wire rod! TRI-WIRE DRAWDOWN RODS
(1)  1 in = 1,000 mils; 1 mm = 1,000 microns. Thickness varies somewhat, notably for high viscosity liquids and small wire rods.  (2)  Lbs/ft 2  assumes 10 lb/gal; g/m 2  assumes 1 g/cm 3 ; use the following formulas for other densities — wt/ga = 8.312 x specific gravity (density); lbs/1,000 ft 2  = 0.1 x wt/gal x table value; g/m 2  = specific gravity x table  254 62.3 3.9 160 254 10.0 100 203 50.0 4.9 201 200 8.0 80 127 31.2 7.9 320 127 5.0 50 107 26.2 9.2 382 107 4.2 42 76.2 18.7 13.1 535 76.2 3.0 30 60.3 14.9 16.1 669 60.3 2.4 24 55.9 13.7 17.9 727 55.9 2.2 22 45.7 11.2 21.9 891 45.7 1.8 18 38.1 9.36 26.3 1,075 38.1 1.5 15 30.5 7.48 32.8 1,340 30.5 1.2 12 25.4 6.23 39.4 1,600 25.4 1.0 10 20.3 4.99 49.2 2,010 20.3 0.8 8 15.2 3.74 65.6 2,670 15.2 0.6 6 12.7 3.12 78.7 3,210 12.7 0.5 5 10.2 2.49 98.4 4,010 10.2 0.4 4 7.6 1.87 131 5,350 7.6 0.3 3 3.8 0.94 263 10,700 3.8 0.15 1 g/m 2 lbs/1000ft 2 m 2 /l Ft 2 /gal Microns Mils Rod # Wet Film Weight Coverage Thickness (1) Metering Rod Application Chart
Knife over Roll
This process relies on a coating being applied to  the substrate which then passes through a ' gap '  between a ' knife ' and a  support roller.  As the coating and substrate pass through, the excess is scraped off.  This process can be used for  high viscosity   coatings and very high coat weights,  such as plastisols and rubber coatings.  There are innumerable variants of the relatively simple process which is rugged, hard-working and  somewhat inaccurate .  Knife over Roll
Slot Orifice Coating
Slot Orifice Coating In the Slot Die process, the coating is squeezed out by  gravity or under pressure through a slot and onto the  substrate. If the coating is 100% solids, the process is termed 'Extrusion' and in this case, the line speed is  frequently much faster than the speed of the extrusion. This enables coatings to be considerably thinner than  the width of the slot.
Slot Die Coater  The slot die coater does not use rollers to deliver the adhesive to the web.  Instead, adhesive is pumped into a chamber, where it exits through a long,  narrow slot directly in contact with a moving web. The web is usually supported immediately behind the slot with a rubber or steel backing roll.                                                                     Figure 4  : Slot Die Head Set-Up  The slot die coating method is inherently low foaming, and is capable of producing  good quality material at high line speeds. However, the equipment is relatively  expensive and requires a high level of operator expertise. Moderate to high  coat weights are possible with slot die.
Die Coating Methods - a family of coating methods: SLOT-BEAD ("slot", "die", "on-roll slot")  EXTRUSION  TENSIONED-WEB SLOT ("off-roll slot", "TWSC")  SLOT-ON-RUBBER ROLL  SLIDE-BEAD ("slide", "cascade")  SLOT-CURTAIN ("curtain", "hopper", "inverted fountain")  SLIDE-CURTAIN ("multilayer curtain")  JET COATING  Die Coating Characteristics: Coating process utilizes a "die" applicator for achieving two sequential flows: internal manifold flow  - distributes flow across intended coating width internal manifold flow is similar for all die coating methods  external transfer flow  -transfers the width-distributed flow to the moving substrate different methods are distinguished by their particular transfer flows
Slot-Curtain Coating section displaying Manifold and Transfer Flows                                                         Slot Die section view displaying internal manifold                                                        
Commercial Advantages Precision Die Coating allows participation in higher-margin markets exclusive to superior product functionality and more frugal manufacturing  (reduced waste, higher productivity)  when compared with other coatings methods such as roll, blade, gravure, rod, etc.
Slot Die section view displaying internal manifold                                                         Transfer flow of slot-bead coating                                                         Slot-bead Coating with applied vacuum.                                                        
              WebFlight adhesive coating technology is a  contactless method   of applying adhesive coating solutions to web materials by modifying  the micro-environment in which the adhesive coating solution  and web meet. WebFlight adhesive coating does not employ rollers, knives, blades,  or other contact devices to apply or level coating solutions across the web. Instead, WebFlight adhesive coating uses the following methods to  optimize the adhesive coating process: Contactless Adhesive Coating
 
In this simple process, the substrate is dipped into a bath of the coating, which is normally of a low viscosity to enable the coating to run back into the bath as the substrate emerges. This process is frequently used on porous substrates.   Immersion (Dip) Coating
Curtain Coater  A curtain coating head functions very similarly to a slot die coater except that the  slot is position several centimeters above the moving web, and edge guides are used to control the width of the falling curtain. With carefully designed emulsion  properties such as rheology and surface tension, acrylic emulsion pressure sensitive adhesives may be coated via curtain coater at speeds in excess of 1000 meters  per minute. Elimination of foam in the adhesive is also critical to achieving maximum  line speeds with this method.                                                                                                            
In the Curtain Coating process, a bath with a slot in the base allows a continuous curtain of the coating to fall into the gap between two conveyors. The object to be coated, such as a door, is passed along the conveyor at a controlled speed and so receives the coating on its upper face. Smelly and crude versions of these machines were once common.    Curtain Coating
Air Knife Coating A simple process where the coating is applied to the substrate and the excess is 'blown off' by a powerful jet from the air knife. This procedure is typically used for aqueous coatings and is particularly noisy.   Air Knife Coating

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06.presentation on coating methods

  • 2. Coating is a very Important process involved in Manufacture of Coated Products Today we shall review some of these as listed below. Gravure Coating Comma Coating Reverse Roll Coating Hot Melt Coating Metering Rod / Myer Bar Coating Knife over roll coating Slot Orifice coating Immersion / Dip coating Curtain Coating
  • 3. To understand the process of coating an adhesive on a substrate for the manufacture of Adhesive tape is quite simple . Let’s quote the example spreading butter on bread. The Butter must have good spread ability in order to apply it evenly . Try spreading frozen butter on bread and you will learn the difficulties encountered. Similarly, the adhesive to be coated must have good spread ablity . And let’s not forget one must have a correct equipment to spread or coat the adhesive. There are other variable factors also involved , but we shall look into coating methods Exclusively.
  • 4. The Coating methods Their Capabilities and Limitations 20-100 200 500-20000 Slot Orifice 3.-25. 200 10-200 Myer Bar 10-300 300 500-20000 Hot Melt 10-200 300 1000-6000 Reverse Roll Nip 10-200 100 200-6000 Reverse Roll Pan 10-200 300 1000-6000 Comma 3.-20. 700 Mtrs. 100-2000 Gravure 20-100 200 500-20000 Curtain Heavy 50 1000-10000 Immersion / Dip Coating 3.-15. 1500 100-20000 Knife over Roll Coating Wt . gm per sq. mtr Max Speed per Min Viscosity in CPS Coating Method
  • 5. Gravure Coating The gravure coating process relies on an engraved roller running in a coating bath, which fills the engraved dots or lines of the roller with the coating material. The excess coating on the roller is wiped off by the Doctor Blade and the coating is then deposited onto the substrate as it passes between the Engraved roller and a Pressure Roller . There are three different ways of gravure roll manufacturing . One has to choose a correct type depending upon the required coating gram mage and the material to be coated
  • 6.  
  • 7. CHARACTERISTICS OF ENGRAVED GRAVURE ROLLERS 11.7 63.1 0.010 0.055 47 9 120 24 Trihelical 3.6 49.5 0.005 0.065 79 6 200 16 Quadrangular 2.4 27.6 0.003 0.037 79 16 200 40 Pyramidal Lines/cm Lines/in Deposit gm/m 2 Cell Depth mm Screen Type of Engraving
  • 11. Reverse Roll Coating In this procedure, the coating material is measured onto the applicator roller by precision setting of the gap between the upper metering roller and the application roller below it. The coating is 'wiped' off the application roller by the substrate as it passes around the support roller at the bottom. The diagram illustrates a 3-roll reverse roll coating process, although 4-roll versions are common.
  • 12. Reverse Roll Coater The three roll reverse coater is used for many specialty applications. This method is more expensive and generally slower in line speed than the Mayer rod coater. However, the versatility in terms of coat weight range and coating width, and the good coat quality of the three roll reverse has made it popular with many converters. In this process, the middle roll is coated with a precise thickness of adhesive, determined by the size of the gap between the top and middle rolls. The adhesive is then transferred as the rubber backing roll brings the web into contact. The adhesive coat weight can also be varied by increasing or decreasing the speed of the applicator roll relative to the web speed. The metering roll speed can be varied to adjust the smoothness of the coating.                                                                                       Figure 2 : Reverse Roll Coater There are several variations of the reverse roll coating method, such as four-roll, nip fed, and pan fed systems. A nip-fed, three roll reverse coater is shown here. Medium to high coat weights are possible with reverse roll.
  • 13.  
  • 14. Myer Bar Coating In this coating process, an excess of the coating is deposited onto the substrate as it passes over the bath roller. The wire-wound metering rod, sometimes known as a Meyer Rod, allows the desired quantity of the coating to remain on the substrate. The quantity is determined by the diameter of the wire used on the rod. This process is remarkably tolerant of non-precision engineering of the other components of the coating machine .
  • 15.  
  • 16. The market for wire-wound rods has grown rapidly during the past few decades, because they provide predictable, accurate coatings time after time, at a minimal cost. Although the technology goes back almost a century, today's high quality materials, multi-wire designs and special wire surfaces have made this system more popular than ever before.   Rods give users the ability to fine-tune coating thickness quickly and easily, without altering the chemistry of their coating material, and without time-consuming and expensive changeovers.     Wire-wound rods were first used in coating machines built by Charles Mayer in the 1900's to manufacture waxed paper and carbon paper. They are still called "Mayer Bars“ by many coaters.     Wet coating thickness can be accurately predicted within one tenth of a mil (.0001"). Rod selection tables allow coaters to consider coat weight and percent of solids in choosing the proper rod size for each production run.     Bottom-line profits have encouraged many coaters to modify existing machines, in order to take advantage of the flexibility, the ease of use and the dollar savings associated with rod coating.
  • 17. Coating Rods are accurate easy to use inexpensive
  • 18. One of the more common methods of coating is the Mayer rod coater, sometimes called a metering rod coater. This equipment has advantages such as low capital cost, ease of coat weight adjustment, ease of operation, and a broad range of coat weights are possible.                                                                                          
  • 19.  
  • 20.  
  • 21. Figure 1 : Mayer Road Coater In this coating method, an applicator roll delivers adhesive to the substrate being coated. The applicator roll may turn either with or against the primary web, delivering an excess of adhesive. Wire wound rods are then used to remove the excess. The rods may also turn in either direction. The amount of adhesive removed depends upon the diameter of the wire which is wound around the steel rod. Coat weight is increased by simply switching to a rod wrapped with larger diameter wire. Two rods in series often give better coating results than a single rod. The first rod has larger diameter wire and removes most of the excess adhesive. The second rod, with smaller diameter wire, smoothes the coating and produces the final desired coat weight. Mayer rod coating can deliver a broad range of coat weights.
  • 22.  
  • 23.       Where heavier coatings are required, manufactures provide special drawdown rods with two wires. A standard single-wire rod is over wound with a smaller wire which follows the spiral of the base wire. The result is a modified groove between the wires that will produce wet coatings up to 19 mils (.019") thick. TWO-WIRE DRAWDOWN RODS
  • 24. Three Rod technology developed by for Coatings up to 56 mils (.056") thick can be produced, using three standard wires wound in a unique configuration. Two wires are wound side by side on a core rod, then a third wire follows one spiral of the base wires. The resulting groove will maximize the area between the wires, producing a coating more than six times the thickness produced by a single-wire rod! TRI-WIRE DRAWDOWN RODS
  • 25. (1) 1 in = 1,000 mils; 1 mm = 1,000 microns. Thickness varies somewhat, notably for high viscosity liquids and small wire rods. (2) Lbs/ft 2 assumes 10 lb/gal; g/m 2 assumes 1 g/cm 3 ; use the following formulas for other densities — wt/ga = 8.312 x specific gravity (density); lbs/1,000 ft 2 = 0.1 x wt/gal x table value; g/m 2 = specific gravity x table 254 62.3 3.9 160 254 10.0 100 203 50.0 4.9 201 200 8.0 80 127 31.2 7.9 320 127 5.0 50 107 26.2 9.2 382 107 4.2 42 76.2 18.7 13.1 535 76.2 3.0 30 60.3 14.9 16.1 669 60.3 2.4 24 55.9 13.7 17.9 727 55.9 2.2 22 45.7 11.2 21.9 891 45.7 1.8 18 38.1 9.36 26.3 1,075 38.1 1.5 15 30.5 7.48 32.8 1,340 30.5 1.2 12 25.4 6.23 39.4 1,600 25.4 1.0 10 20.3 4.99 49.2 2,010 20.3 0.8 8 15.2 3.74 65.6 2,670 15.2 0.6 6 12.7 3.12 78.7 3,210 12.7 0.5 5 10.2 2.49 98.4 4,010 10.2 0.4 4 7.6 1.87 131 5,350 7.6 0.3 3 3.8 0.94 263 10,700 3.8 0.15 1 g/m 2 lbs/1000ft 2 m 2 /l Ft 2 /gal Microns Mils Rod # Wet Film Weight Coverage Thickness (1) Metering Rod Application Chart
  • 27. This process relies on a coating being applied to the substrate which then passes through a ' gap ' between a ' knife ' and a support roller. As the coating and substrate pass through, the excess is scraped off. This process can be used for high viscosity coatings and very high coat weights, such as plastisols and rubber coatings. There are innumerable variants of the relatively simple process which is rugged, hard-working and somewhat inaccurate . Knife over Roll
  • 29. Slot Orifice Coating In the Slot Die process, the coating is squeezed out by gravity or under pressure through a slot and onto the substrate. If the coating is 100% solids, the process is termed 'Extrusion' and in this case, the line speed is frequently much faster than the speed of the extrusion. This enables coatings to be considerably thinner than the width of the slot.
  • 30. Slot Die Coater The slot die coater does not use rollers to deliver the adhesive to the web. Instead, adhesive is pumped into a chamber, where it exits through a long, narrow slot directly in contact with a moving web. The web is usually supported immediately behind the slot with a rubber or steel backing roll.                                                                   Figure 4 : Slot Die Head Set-Up The slot die coating method is inherently low foaming, and is capable of producing good quality material at high line speeds. However, the equipment is relatively expensive and requires a high level of operator expertise. Moderate to high coat weights are possible with slot die.
  • 31. Die Coating Methods - a family of coating methods: SLOT-BEAD ("slot", "die", "on-roll slot") EXTRUSION TENSIONED-WEB SLOT ("off-roll slot", "TWSC") SLOT-ON-RUBBER ROLL SLIDE-BEAD ("slide", "cascade") SLOT-CURTAIN ("curtain", "hopper", "inverted fountain") SLIDE-CURTAIN ("multilayer curtain") JET COATING Die Coating Characteristics: Coating process utilizes a "die" applicator for achieving two sequential flows: internal manifold flow - distributes flow across intended coating width internal manifold flow is similar for all die coating methods external transfer flow -transfers the width-distributed flow to the moving substrate different methods are distinguished by their particular transfer flows
  • 32. Slot-Curtain Coating section displaying Manifold and Transfer Flows                                                         Slot Die section view displaying internal manifold                                                        
  • 33. Commercial Advantages Precision Die Coating allows participation in higher-margin markets exclusive to superior product functionality and more frugal manufacturing (reduced waste, higher productivity) when compared with other coatings methods such as roll, blade, gravure, rod, etc.
  • 34. Slot Die section view displaying internal manifold                                                         Transfer flow of slot-bead coating                                                         Slot-bead Coating with applied vacuum.                                                        
  • 35.               WebFlight adhesive coating technology is a contactless method of applying adhesive coating solutions to web materials by modifying the micro-environment in which the adhesive coating solution and web meet. WebFlight adhesive coating does not employ rollers, knives, blades, or other contact devices to apply or level coating solutions across the web. Instead, WebFlight adhesive coating uses the following methods to optimize the adhesive coating process: Contactless Adhesive Coating
  • 36.  
  • 37. In this simple process, the substrate is dipped into a bath of the coating, which is normally of a low viscosity to enable the coating to run back into the bath as the substrate emerges. This process is frequently used on porous substrates.   Immersion (Dip) Coating
  • 38. Curtain Coater A curtain coating head functions very similarly to a slot die coater except that the slot is position several centimeters above the moving web, and edge guides are used to control the width of the falling curtain. With carefully designed emulsion properties such as rheology and surface tension, acrylic emulsion pressure sensitive adhesives may be coated via curtain coater at speeds in excess of 1000 meters per minute. Elimination of foam in the adhesive is also critical to achieving maximum line speeds with this method.                                                                                                           
  • 39. In the Curtain Coating process, a bath with a slot in the base allows a continuous curtain of the coating to fall into the gap between two conveyors. The object to be coated, such as a door, is passed along the conveyor at a controlled speed and so receives the coating on its upper face. Smelly and crude versions of these machines were once common.   Curtain Coating
  • 40. Air Knife Coating A simple process where the coating is applied to the substrate and the excess is 'blown off' by a powerful jet from the air knife. This procedure is typically used for aqueous coatings and is particularly noisy.   Air Knife Coating

Editor's Notes

  1. Gravure Coating Method