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2011 International Transaction Journal of Engineering, Management, & Applied Sciences & Technologies.




                 International Transaction Journal of Engineering,
                 Management, & Applied Sciences & Technologies
                           http://www.TuEngr.com,               http://go.to/Research




A Study on Weld Quality Characteristics of Pulsed Current Micro
Plasma Arc Welding of SS304L Sheets
                              a*                          b                                  b
Kondapalli Siva Prasad , Ch.Srinivasa Rao , and D. Nageswara Rao

a
  Department of Mechanical Engineering, Anil Neerukonda Institute of Technology & Sciences,
Visakhapatnam, INDIA
b
  Department of Mechanical Engineering, Andhra University, Visakhapatnam, INDIA

ARTICLEINFO                        A B S T RA C T
Article history:                  Micro Plasma Arc Welding plays a vital role in attaining
Received 17 June 2011     good weld quality in various engineering applications like bellows,
Received in revised form
23 September 2011
                          diaphragms etc. The main objective of the present work is to use
Accepted 25 September 2011current pulsing technique while welding SS304L sheets. The paper
Available online          focuses on studying the influence of various Micro Plasma Arc
25 September 2011         Welding process parameters like peak current, back current, pulse
Keywords:                 and pulse width on the weld quality characteristics like weld pool
Weld Quality,             geometry, microstructure, grain size, hardness and tensile
Pulsed current,           properties. The results reveals that the usage of pulsing current,
Micro Plasma Arc Welding, grain refinement has taken place in weld fusion zone, because of
SS304L
                          which improvement in weld quality characteristics have been
                          observed.

                                      2011 International Transaction Journal of Engineering, Management, &
                                   Applied Sciences & Technologies.



1. Introduction 
     Welding thin sheets is quite different from welding thick sections, because during welding
of thin sheets many problems are experienced. These problems are usually linked with heat
input. Fusion welding generally involves joining of metals by application of heat for melting of
metals to be joined. Almost all the conventional arc welding processes offer high heat input,
which in turn leads to various problems such as burn through or melt trough, distortion,
*Corresponding author (Kondapalli Siva Prasad). Tel/Fax: +91-9849212391. E-mail
addresses:kspanits@gmail.com.     2011. International Transaction Journal of Engineering,
Management, & Applied Sciences & Technologies.       Volume 2 No.4.      ISSN 2228-9860.
                                                                                                            437
eISSN 1906-9642. Online Available at http://TuEngr.com/V02/437-446.pdf
porosity, buckling warping & twisting of welded sheets, grain coarsening , evaporation of
useful elements present in coating of the sheets, joint gap variation during welding, fume
generation form coated sheets etc. Use of proper welding process, procedure and technique is
one tool to address this issue (M.Balasubramanian et al., 2010). MPAW is a good process for
joining thin sheet, but it suffers high equipment cost compared to GTAW. However it is more
economical when compare with Laser Beam welding and Electron Beam Welding processes.

    The plasma welding process was introduced to the welding industry in 1964 as a method of
bringing better control to the arc welding process in lower current ranges (Modern Application
News, 1999). Today, plasma retains the original advantages it brought to the industry by
providing an advanced level of control and accuracy to produce high quality welds in both
miniature and pre precision applications and to provide long electrode life for high production
requirements at all levels of amperage. Plasma welding is equally suited to manual and
automatic applications. It is used in a variety of joining operations ranging from welding of
miniature components to seam welding to high volume production welding and many others.

    Pulsed current MPAW involves cycling the welding current at selected regular frequency.
The maximum current is selected to give adequate penetration and bead contour, while the
minimum is set at a level sufficient to maintain a stable arc (K.Prasad Rao, 2001 &
G.Madusudhan Reddy et al., 1993). This permits arc energy to be used effectively to fuse a spot
of controlled dimensions in a short time producing the weld as a series of overlapping nuggets.
By contrast, in constant current welding, the heat required to melt the base material is supplied
only during the peak current pulses allowing the heat to dissipate into the base material leading
to narrower heat affected zone (HAZ) (M.Balasubramanian et al., 2006). Advantages include
improved bead contours, greater tolerance to heat sink variations, lower heat input
requirements,, reduced residual stresses and distortion, refinement of fusion zone
microstructure and reduced with of HAZ. There are four independent parameters that influence
the process are peak current, back current, pulse and pulse width.

    From earlier works, it has been observed that much work is not reported so far to
investigate the effect of pulsed current MPAW process parameters particularly joining thin
sheets.   Hence an attempt has been made to study important pulsed MPAW process
parameters. This work presents the influence of weld input parameters like Peak Current,
Back Current, Pulse and Pulse Width on weld quality characteristics of MPAW welded SS
304L joint.
    438          Kondapalli Siva Prasad, Ch.Srinivasa Rao, and D.Nageswara Rao
2. Experimental Procedure 
     Experiments are conducted using the Pulsed Micro Plasma Arc Welding (MPAW) process.
Industrial pure and commercial grade argon gases are used for shielding and back purging,
respectively. Automatic voltage control available in the welding equipment is used. Fixture
variation effects are not considered as the same setup has been used throughout the experiment.

     There are many influential process parameters which effect the weld quality characteristics
of MPAW process like peak current, back current, pulse , pulse width, flow rate of shielding
gas, plow rate of purging gas, flow rate of plasma gas, welding speed etc. From the works
carried out by numerous researchers on usage of pulsing current on various welding processes
(N.Karunakaran et al., 2011, S.Babu et al., 2008, M.Balasubramanian et al.,2008) it was
understood that peak current, back current, pulse and pulse width are the dominating
parameters which effect the weld quality. However in the present work the optimal established
values are obtained by conducting trail experiments on various combinations of selected
process parameters as per Response Surface Method (RSM) by considering four factors, five
levels, rotatable central composite design matrix. The values of process parameters used in this
study are the optimal values obtained from RSM.

             Peak Current          = 7 Amperes
             Back Current          = 4 Amperes
             Pulse                 = 40 pulse/sec
             Pulse Width           = 50%

               Table 1: Fixed pulsed MPAW process parameters and their values.
                    Power source                         Secheron Micro Plasma Arc Machine (Model:
                                                                    PLASMAFIX 50E)
                      Polarity                                            DCEN
                Mode of operation                                      Pulse mode
                     Electrode                                2% thoriated tungsten electrode
                Electrode Diameter                                         1mm
                    Plasma gas                                     Argon & Hydrogen
               Plasma gas flow rate                                       6 Lpm
                   Shielding gas                                          Argon
              Shielding gas flow rate                                    0.4 Lpm
                    Purging gas                                           Argon
               Purging gas flow rate                                     0.4 Lpm
              Copper Nozzle diameter                                       1mm
              Nozzle to plate distance                                     1mm
                  Welding speed                                        260mm/min
                  Torch Position                                         Vertical
                  Operation type                                        Automatic

*Corresponding author (Kondapalli Siva Prasad). Tel/Fax: +91-9849212391. E-mail
addresses:kspanits@gmail.com.     2011. International Transaction Journal of Engineering,
Management, & Applied Sciences & Technologies.       Volume 2 No.4.      ISSN 2228-9860.
                                                                                                439
eISSN 1906-9642. Online Available at http://TuEngr.com/V02/437-446.pdf
The fixed pulsed MPAW process parameters and their values are presented in Table 1.

     Austenitic stainless steel sheets of type SS 304L 100×50×0.25 mm as shown in Figure 1
are welded autogenously with square butt joint without edge preparation (K.Siva Prasad et al.,
2011). The chemical composition of SS 304L was given in Table 2.

                            Table 2: Chemical composition of SS304L (weight %).
   C           Si          Mn           P          S        Cr            Ni         Mo   Ti     N
 0.021        0.35         1.27       0.030      0.001      18.10        8.02        --   --   0.053




                                       Figure 1: Typical weld joint.

     After preparation of weld joint, visual inspection was carried out to detect surface defects
and X-ray was taken to know internal defects like cracks, improper fusion etc. After clearing
X-ray the welded samples were prepared to carry out various tests mentioned in the succeeding
paragraphs.


3. Measurement of Output Responses 

3.1 Weld Bead Geometry 
     Sample preparation and mounting was done as per ASTM E 3-1 standard. The samples
were cut from the welded specimens and mounting using Bakelite powder. After standard
matallurgial polishing process, Oxalic acid is used as the etchant to reveal weld bead geometry.
The weld pool geometries were measured using Metallurgical Microscope, Make :Dewinter
Technologie, Model No. DMI-CROWN-II. A typical weld bead geometry is shown in Figure
2.
     440             Kondapalli Siva Prasad, Ch.Srinivasa Rao, and D.Nageswara Rao
Figure 2: Typical weld bead geometry.

     Photo macrograph of typical weld specimens showing the bead profile at 100X
magnification is presented in Figure 3a & 3b. The values of weld bead geometry for SS304L are
presented in Table 3.




                              100X                                          100X


       Figure 3a: Front Width                    Figure 3b: Sectional View across the weld

                              Table 3: Weld bead parameters of SS304L.
                     Weld bead parameter                          Dimension in Microns
                     Front Width (Microns)                            1509.859
                     Back Width (Microns)                             1394.383
                     Front Height (Microns)                             51.903
                     Back Height (Microns)                              34.312

3.2 Micro Hardness 
     Vickers Micro hardness was done as per ASTM E384. The samples were cut from the
welded specimens and Vickers Micro Hardness values across the weld joint at an interval of
0.3mm using Digital Micro Hardness testing Machine, make METSUZAWA CO LTD,
JAPAN, Model No: MMT-X7 and the values recorded are presented in Table 4.

     Table 4:    The variation of hardness values across the weld joint at 0.3mm interval.
 Location               1         2        3        4         5         6           7       8     9
 Vickers Micro
 Hardness             189       202      197       194      199        189         193   186     188
 (VHN)

*Corresponding author (Kondapalli Siva Prasad). Tel/Fax: +91-9849212391. E-mail
addresses:kspanits@gmail.com.     2011. International Transaction Journal of Engineering,
Management, & Applied Sciences & Technologies.       Volume 2 No.4.      ISSN 2228-9860.
                                                                                                441
eISSN 1906-9642. Online Available at http://TuEngr.com/V02/437-446.pdf
In the above table points 1,2,8,9 are on the base metal at Heat Affected Zone, points 4, 5, 6
across the Weld Zone and points 3,7 indicates at Fusion Zone and are represented in Figure 4 .
The variation of hardness across the weld joint is represented in Figure 5.



                                                           1 2 3         4    5        6         7 8 9




               Figure 4: Location of hardness measuring points in weld joint.


                                                205
                Vickers Microhardess values (VHN)




                                                                202
                                                200
                                                                                      199
                                                                       197
                                                195
                                                                             194                     193
                                                190
                                                          189                                  189               188
                                                185                                                        186

                                                180

                                                175
                                                      1     2      3     4        5        6     7     8     9

                                                                        Location on the weld

    Figure 5: Variation of Hardness values at an interval of 0.3mm across the weld joint.

    From Figure 4 it is understood that the weld zone is having higher hardness values
compared to parent metal.


3.3 Microstructure 
    For Microstructure measurement ASTM E 407 was followed for Etching along with ASM
Metal Hand Book, Volume 9. For revealing the Microstructure the weld samples are mounted
using Bakelite and polishing was done according to standard Metallurgical procedure. Oxalic

    442               Kondapalli Siva Prasad, Ch.Srinivasa Rao, and D.Nageswara Rao
Acid was used as an etchant. For revealing the Microstructure, Electrolytic Etching was done.
The Microstructure was measured using Metallurgical Microscope, Make: Carl Zeiss, Model
No: Axiovert 40 at a magnification of 100X. The Microstructure of parent metal zone, weld
metal zone and fusion zone are shown in Figure 6.




               Weld Zone                                                       Parent metal Zone




                       Figure 6: Indicating Parent, Fusion and Metal zone.

3.4 Grain Size 
     For Grain Size measurement ASTM E112 was followed. Polishing was done according to
standard Metallurgical procedure and Etching was done as per ASTM E407. For revealing the
grain size Electrolytic was done using Nitric Acid for about 1 minute. Using Metallurgical
Microscope, Make: Carl Zeiss, Model No: Axiovert 40 at a magnification of 200X grain
structures was captured and compared with ASTM standard grain Size. Figures 7 and 8
indicate the grain structure at weld joint and Parent metal zone.




    Figure 7: Grain structure at weld joint.          Figure 8: Grain structure at Parent metal.


     From Figures 7 and 8, one can only compare with the standard ASTM grain size number.
By comparison method it was observed that for parent metal the ASTM grain size number is 8.5
and near to the fusion zone the ASTM grain size number is 8.
*Corresponding author (Kondapalli Siva Prasad). Tel/Fax: +91-9849212391. E-mail
addresses:kspanits@gmail.com.     2011. International Transaction Journal of Engineering,
Management, & Applied Sciences & Technologies.       Volume 2 No.4.      ISSN 2228-9860.
                                                                                            443
eISSN 1906-9642. Online Available at http://TuEngr.com/V02/437-446.pdf
In order to get the exact grain size one has to go for advanced measuring devices like
Scanning Electron Microscope (SEM).The grain size of parent metal in heat affected zone is
around 45.432µm and near to the fusion zone it is around 43.854µm. The SEM images showing
the grain size at the fusion zone is presented in Figure 9.




                                   Figure 9: SEM image of SS304L.


3.5 Tensile Properties 
    The tensile property of the sample was carried out according to ASTM E8. Specimen was
cut using wire cut Electro Discharge Machine. Tensing was carried out on a 100KN universal
tensile testing machine. The results indicate that the values obtained are better than the parent
metal; hence the weld joint is good. The tensile properties of parent metal and welded specimen
are shown in Table 5.

                                       Table 5: Tensile properties.
                                                        Parent
                                                                     Welded specimen
                                                         metal
                     Yield Strength (MPa)               254.95              271
                     Ultimate Strength (Mpa)            677.67              705
                     % Elongation
                                                        52.56               59.5
                     (50mm gauge length


    From Table 5 it is very clear that the tensile properties of the weld specimen is better than
the parent metal.




    444             Kondapalli Siva Prasad, Ch.Srinivasa Rao, and D.Nageswara Rao
4. Conclusions 
     The study reveals that the sound weld joint is obtained by choosing proper values of Peak
current, Back current, Pulse and Pulse as the important process variables. The weld joint
obtained is free from surface defects and fused properly. The hardness values of the weld zone
are comparatively better than the parent metal zone which indicates better strength of the weld
joint. The microstructure of the weld joint indicates the presence of ferrite particles. Fine grains
are obtained in the weld zone and fusion zone because of using pulsed current. The grain size of
parent metal in heat affected zone is around 45.432µm and near to the fusion zone it is around
43.854µm, which reveals that weld zone is stronger than parent metal. The tensile properties of
welded sample are better than parent metal, which indicates better strength of the weld joint.


5. Acknowledgements 

     We express our sincere thanks to Shri. R.Gopla Krishnan, Director, M/s Metallic Bellows
(I) Pvt Ltd, Chennai, INDIA and Andhra University, Visakhapatnam, INDIA for their support
to carry out experimentation. A very special thank you is due to Assistant Professor Dr.
Apiwat Muttamara for insightful comments, helping clarify and improve the manuscript.


6. References 
G. Madusudhan Reddy, A. A. Gokhale and K.Prasad Rao (1997), Weld microstructure
     refinement in a 1441 grade aluminium-lithium alloy , Journal of Material Science,
     Vol.32,pp.4117.

K. Prasad Rao (2001), Proc of the national Conference on Recent Trends in Material Processing
       (RAMP, Annamalai University, India, 2001) p.176.

Kondapalli Siva Prasad, Ch. Srinivasa Rao, D. Nageswara Rao (2011),Prediction of Weld Pool
      Geometry in Pulsed Current Micro Plasma Arc Welding of SS304L Stainless Steel
      Sheets, International Transaction Journal of Engineering, Management, & Applied
      Sciences & Technologies, Vol.2(3), 325-336.

M. Balasubramanian, V.Jayabalan and V.Balasubramanian (2006), Optimizing the Pulsed
      Current Gas Tungsten Arc Welding Parameters, J Mater Sci Technol, Vol.22,
      Number.6, pp.821.

M. Balasubramanian, V.Jayabalan and V.Balasubramanian (2008), Developing mathematical
      models to predict grain size and hardness of argon tungsten pulse current arc welded
      titanium alloy, Journal of Materials Processing Technology, Vol.196,pp.222-229.

*Corresponding author (Kondapalli Siva Prasad). Tel/Fax: +91-9849212391. E-mail
addresses:kspanits@gmail.com.     2011. International Transaction Journal of Engineering,
Management, & Applied Sciences & Technologies.       Volume 2 No.4.      ISSN 2228-9860.
                                                                                            445
eISSN 1906-9642. Online Available at http://TuEngr.com/V02/437-446.pdf
M. Balasubramanian, V.Jayabalan, V.Balasubramanian (2010), Effect of process parameters of
       pulsed current tungsten inert gas welding on weld pool geometry of titanium welds,
       Acta Metall.Sin.(Engl. Lett.) ,Vol.23 ,No.4,pp 312-320.

N. Karunakaran, V.Balasubramanian (2011), Effect of pulsed current on temperature
      distribution, weld bead profiles and characteristics of gas tungsten arc welded
      aluminium alloy joints, Transactions of Nonferrous Metals Society of China, Vol.21,
      pp.278-286.

Plasma Welding: more accurate, better control at lower currents (1999), Modern Application
      News.

S.Babu, R.Senthil Kumar, V.Balasubramanian (2008), Optimizing pulsed current gas tungsten
      arc welding parameters of AA6061 aluminium alloy using Hooke and Jeeves algorithm,
      Transactions of Nonferrous Metals Society of China, Vol.18, pp.1028-1036.



           K.Siva Prasad is an Assistant Professor of Department of Mechanical Engineering at Anil Neerukonda
           Institute of Technology & Sciences, Visakhapatnam, India. He received his Bachelors degree from Osmania
           University, India and Master Degree from JNTU, Hyderabad, India. He is also a part time scholar at Andhra
           University. He is a member of various professional bodies like ISTE, FPSI, ISHRAE etc. His area of research
           is micro welding processes.

           Dr. Ch.Srinivasa Rao is an Associate Professor in the Mechanical Engineering Department at Andhra
           University, Visakhapatnam, India. He obtained his PhD degree from Andhra University, Visakhapatnam, India.
           He has published his research papers in various International Journals and conferences proceedings. He is a
           member of various professional bodies like ISTE, IE etc. His area of interest is manufacturing sciences, rapid
           prototyping and robotics.

           Dr. D.Nageswara Rao is a Professor in the Mechanical Engineering Department at Andhra University,
           Visakhapatnam, India. He obtained his PhD degree from Indian Institute of Technology Delhi, India. He is the
           coordinator for Centre for Nanotechnology at Andhra University. He has successfully completed various
           projects sponsored by DST, UGC, AICTE, NRB etc. His area of research is manufacturing sciences and
           nanotechnology.


Peer Review: This article has been internationally peer-reviewed and accepted for publication
               according to the guidelines given at the journal’s website.




    446           Kondapalli Siva Prasad, Ch.Srinivasa Rao, and D.Nageswara Rao

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A Study on Weld Quality Characteristics of Pulsed Current Micro Plasma Arc Welding of SS304L Sheets

  • 1. 2011 International Transaction Journal of Engineering, Management, & Applied Sciences & Technologies. International Transaction Journal of Engineering, Management, & Applied Sciences & Technologies http://www.TuEngr.com, http://go.to/Research A Study on Weld Quality Characteristics of Pulsed Current Micro Plasma Arc Welding of SS304L Sheets a* b b Kondapalli Siva Prasad , Ch.Srinivasa Rao , and D. Nageswara Rao a Department of Mechanical Engineering, Anil Neerukonda Institute of Technology & Sciences, Visakhapatnam, INDIA b Department of Mechanical Engineering, Andhra University, Visakhapatnam, INDIA ARTICLEINFO A B S T RA C T Article history: Micro Plasma Arc Welding plays a vital role in attaining Received 17 June 2011 good weld quality in various engineering applications like bellows, Received in revised form 23 September 2011 diaphragms etc. The main objective of the present work is to use Accepted 25 September 2011current pulsing technique while welding SS304L sheets. The paper Available online focuses on studying the influence of various Micro Plasma Arc 25 September 2011 Welding process parameters like peak current, back current, pulse Keywords: and pulse width on the weld quality characteristics like weld pool Weld Quality, geometry, microstructure, grain size, hardness and tensile Pulsed current, properties. The results reveals that the usage of pulsing current, Micro Plasma Arc Welding, grain refinement has taken place in weld fusion zone, because of SS304L which improvement in weld quality characteristics have been observed. 2011 International Transaction Journal of Engineering, Management, & Applied Sciences & Technologies. 1. Introduction  Welding thin sheets is quite different from welding thick sections, because during welding of thin sheets many problems are experienced. These problems are usually linked with heat input. Fusion welding generally involves joining of metals by application of heat for melting of metals to be joined. Almost all the conventional arc welding processes offer high heat input, which in turn leads to various problems such as burn through or melt trough, distortion, *Corresponding author (Kondapalli Siva Prasad). Tel/Fax: +91-9849212391. E-mail addresses:kspanits@gmail.com. 2011. International Transaction Journal of Engineering, Management, & Applied Sciences & Technologies. Volume 2 No.4. ISSN 2228-9860. 437 eISSN 1906-9642. Online Available at http://TuEngr.com/V02/437-446.pdf
  • 2. porosity, buckling warping & twisting of welded sheets, grain coarsening , evaporation of useful elements present in coating of the sheets, joint gap variation during welding, fume generation form coated sheets etc. Use of proper welding process, procedure and technique is one tool to address this issue (M.Balasubramanian et al., 2010). MPAW is a good process for joining thin sheet, but it suffers high equipment cost compared to GTAW. However it is more economical when compare with Laser Beam welding and Electron Beam Welding processes. The plasma welding process was introduced to the welding industry in 1964 as a method of bringing better control to the arc welding process in lower current ranges (Modern Application News, 1999). Today, plasma retains the original advantages it brought to the industry by providing an advanced level of control and accuracy to produce high quality welds in both miniature and pre precision applications and to provide long electrode life for high production requirements at all levels of amperage. Plasma welding is equally suited to manual and automatic applications. It is used in a variety of joining operations ranging from welding of miniature components to seam welding to high volume production welding and many others. Pulsed current MPAW involves cycling the welding current at selected regular frequency. The maximum current is selected to give adequate penetration and bead contour, while the minimum is set at a level sufficient to maintain a stable arc (K.Prasad Rao, 2001 & G.Madusudhan Reddy et al., 1993). This permits arc energy to be used effectively to fuse a spot of controlled dimensions in a short time producing the weld as a series of overlapping nuggets. By contrast, in constant current welding, the heat required to melt the base material is supplied only during the peak current pulses allowing the heat to dissipate into the base material leading to narrower heat affected zone (HAZ) (M.Balasubramanian et al., 2006). Advantages include improved bead contours, greater tolerance to heat sink variations, lower heat input requirements,, reduced residual stresses and distortion, refinement of fusion zone microstructure and reduced with of HAZ. There are four independent parameters that influence the process are peak current, back current, pulse and pulse width. From earlier works, it has been observed that much work is not reported so far to investigate the effect of pulsed current MPAW process parameters particularly joining thin sheets. Hence an attempt has been made to study important pulsed MPAW process parameters. This work presents the influence of weld input parameters like Peak Current, Back Current, Pulse and Pulse Width on weld quality characteristics of MPAW welded SS 304L joint. 438 Kondapalli Siva Prasad, Ch.Srinivasa Rao, and D.Nageswara Rao
  • 3. 2. Experimental Procedure  Experiments are conducted using the Pulsed Micro Plasma Arc Welding (MPAW) process. Industrial pure and commercial grade argon gases are used for shielding and back purging, respectively. Automatic voltage control available in the welding equipment is used. Fixture variation effects are not considered as the same setup has been used throughout the experiment. There are many influential process parameters which effect the weld quality characteristics of MPAW process like peak current, back current, pulse , pulse width, flow rate of shielding gas, plow rate of purging gas, flow rate of plasma gas, welding speed etc. From the works carried out by numerous researchers on usage of pulsing current on various welding processes (N.Karunakaran et al., 2011, S.Babu et al., 2008, M.Balasubramanian et al.,2008) it was understood that peak current, back current, pulse and pulse width are the dominating parameters which effect the weld quality. However in the present work the optimal established values are obtained by conducting trail experiments on various combinations of selected process parameters as per Response Surface Method (RSM) by considering four factors, five levels, rotatable central composite design matrix. The values of process parameters used in this study are the optimal values obtained from RSM. Peak Current = 7 Amperes Back Current = 4 Amperes Pulse = 40 pulse/sec Pulse Width = 50% Table 1: Fixed pulsed MPAW process parameters and their values. Power source Secheron Micro Plasma Arc Machine (Model: PLASMAFIX 50E) Polarity DCEN Mode of operation Pulse mode Electrode 2% thoriated tungsten electrode Electrode Diameter 1mm Plasma gas Argon & Hydrogen Plasma gas flow rate 6 Lpm Shielding gas Argon Shielding gas flow rate 0.4 Lpm Purging gas Argon Purging gas flow rate 0.4 Lpm Copper Nozzle diameter 1mm Nozzle to plate distance 1mm Welding speed 260mm/min Torch Position Vertical Operation type Automatic *Corresponding author (Kondapalli Siva Prasad). Tel/Fax: +91-9849212391. E-mail addresses:kspanits@gmail.com. 2011. International Transaction Journal of Engineering, Management, & Applied Sciences & Technologies. Volume 2 No.4. ISSN 2228-9860. 439 eISSN 1906-9642. Online Available at http://TuEngr.com/V02/437-446.pdf
  • 4. The fixed pulsed MPAW process parameters and their values are presented in Table 1. Austenitic stainless steel sheets of type SS 304L 100×50×0.25 mm as shown in Figure 1 are welded autogenously with square butt joint without edge preparation (K.Siva Prasad et al., 2011). The chemical composition of SS 304L was given in Table 2. Table 2: Chemical composition of SS304L (weight %). C Si Mn P S Cr Ni Mo Ti N 0.021 0.35 1.27 0.030 0.001 18.10 8.02 -- -- 0.053 Figure 1: Typical weld joint. After preparation of weld joint, visual inspection was carried out to detect surface defects and X-ray was taken to know internal defects like cracks, improper fusion etc. After clearing X-ray the welded samples were prepared to carry out various tests mentioned in the succeeding paragraphs. 3. Measurement of Output Responses  3.1 Weld Bead Geometry  Sample preparation and mounting was done as per ASTM E 3-1 standard. The samples were cut from the welded specimens and mounting using Bakelite powder. After standard matallurgial polishing process, Oxalic acid is used as the etchant to reveal weld bead geometry. The weld pool geometries were measured using Metallurgical Microscope, Make :Dewinter Technologie, Model No. DMI-CROWN-II. A typical weld bead geometry is shown in Figure 2. 440 Kondapalli Siva Prasad, Ch.Srinivasa Rao, and D.Nageswara Rao
  • 5. Figure 2: Typical weld bead geometry. Photo macrograph of typical weld specimens showing the bead profile at 100X magnification is presented in Figure 3a & 3b. The values of weld bead geometry for SS304L are presented in Table 3. 100X 100X Figure 3a: Front Width Figure 3b: Sectional View across the weld Table 3: Weld bead parameters of SS304L. Weld bead parameter Dimension in Microns Front Width (Microns) 1509.859 Back Width (Microns) 1394.383 Front Height (Microns) 51.903 Back Height (Microns) 34.312 3.2 Micro Hardness  Vickers Micro hardness was done as per ASTM E384. The samples were cut from the welded specimens and Vickers Micro Hardness values across the weld joint at an interval of 0.3mm using Digital Micro Hardness testing Machine, make METSUZAWA CO LTD, JAPAN, Model No: MMT-X7 and the values recorded are presented in Table 4. Table 4: The variation of hardness values across the weld joint at 0.3mm interval. Location 1 2 3 4 5 6 7 8 9 Vickers Micro Hardness 189 202 197 194 199 189 193 186 188 (VHN) *Corresponding author (Kondapalli Siva Prasad). Tel/Fax: +91-9849212391. E-mail addresses:kspanits@gmail.com. 2011. International Transaction Journal of Engineering, Management, & Applied Sciences & Technologies. Volume 2 No.4. ISSN 2228-9860. 441 eISSN 1906-9642. Online Available at http://TuEngr.com/V02/437-446.pdf
  • 6. In the above table points 1,2,8,9 are on the base metal at Heat Affected Zone, points 4, 5, 6 across the Weld Zone and points 3,7 indicates at Fusion Zone and are represented in Figure 4 . The variation of hardness across the weld joint is represented in Figure 5. 1 2 3 4 5 6 7 8 9 Figure 4: Location of hardness measuring points in weld joint. 205 Vickers Microhardess values (VHN) 202 200 199 197 195 194 193 190 189 189 188 185 186 180 175 1 2 3 4 5 6 7 8 9 Location on the weld Figure 5: Variation of Hardness values at an interval of 0.3mm across the weld joint. From Figure 4 it is understood that the weld zone is having higher hardness values compared to parent metal. 3.3 Microstructure  For Microstructure measurement ASTM E 407 was followed for Etching along with ASM Metal Hand Book, Volume 9. For revealing the Microstructure the weld samples are mounted using Bakelite and polishing was done according to standard Metallurgical procedure. Oxalic 442 Kondapalli Siva Prasad, Ch.Srinivasa Rao, and D.Nageswara Rao
  • 7. Acid was used as an etchant. For revealing the Microstructure, Electrolytic Etching was done. The Microstructure was measured using Metallurgical Microscope, Make: Carl Zeiss, Model No: Axiovert 40 at a magnification of 100X. The Microstructure of parent metal zone, weld metal zone and fusion zone are shown in Figure 6. Weld Zone Parent metal Zone Figure 6: Indicating Parent, Fusion and Metal zone. 3.4 Grain Size  For Grain Size measurement ASTM E112 was followed. Polishing was done according to standard Metallurgical procedure and Etching was done as per ASTM E407. For revealing the grain size Electrolytic was done using Nitric Acid for about 1 minute. Using Metallurgical Microscope, Make: Carl Zeiss, Model No: Axiovert 40 at a magnification of 200X grain structures was captured and compared with ASTM standard grain Size. Figures 7 and 8 indicate the grain structure at weld joint and Parent metal zone. Figure 7: Grain structure at weld joint. Figure 8: Grain structure at Parent metal. From Figures 7 and 8, one can only compare with the standard ASTM grain size number. By comparison method it was observed that for parent metal the ASTM grain size number is 8.5 and near to the fusion zone the ASTM grain size number is 8. *Corresponding author (Kondapalli Siva Prasad). Tel/Fax: +91-9849212391. E-mail addresses:kspanits@gmail.com. 2011. International Transaction Journal of Engineering, Management, & Applied Sciences & Technologies. Volume 2 No.4. ISSN 2228-9860. 443 eISSN 1906-9642. Online Available at http://TuEngr.com/V02/437-446.pdf
  • 8. In order to get the exact grain size one has to go for advanced measuring devices like Scanning Electron Microscope (SEM).The grain size of parent metal in heat affected zone is around 45.432µm and near to the fusion zone it is around 43.854µm. The SEM images showing the grain size at the fusion zone is presented in Figure 9. Figure 9: SEM image of SS304L. 3.5 Tensile Properties  The tensile property of the sample was carried out according to ASTM E8. Specimen was cut using wire cut Electro Discharge Machine. Tensing was carried out on a 100KN universal tensile testing machine. The results indicate that the values obtained are better than the parent metal; hence the weld joint is good. The tensile properties of parent metal and welded specimen are shown in Table 5. Table 5: Tensile properties. Parent Welded specimen metal Yield Strength (MPa) 254.95 271 Ultimate Strength (Mpa) 677.67 705 % Elongation 52.56 59.5 (50mm gauge length From Table 5 it is very clear that the tensile properties of the weld specimen is better than the parent metal. 444 Kondapalli Siva Prasad, Ch.Srinivasa Rao, and D.Nageswara Rao
  • 9. 4. Conclusions  The study reveals that the sound weld joint is obtained by choosing proper values of Peak current, Back current, Pulse and Pulse as the important process variables. The weld joint obtained is free from surface defects and fused properly. The hardness values of the weld zone are comparatively better than the parent metal zone which indicates better strength of the weld joint. The microstructure of the weld joint indicates the presence of ferrite particles. Fine grains are obtained in the weld zone and fusion zone because of using pulsed current. The grain size of parent metal in heat affected zone is around 45.432µm and near to the fusion zone it is around 43.854µm, which reveals that weld zone is stronger than parent metal. The tensile properties of welded sample are better than parent metal, which indicates better strength of the weld joint. 5. Acknowledgements  We express our sincere thanks to Shri. R.Gopla Krishnan, Director, M/s Metallic Bellows (I) Pvt Ltd, Chennai, INDIA and Andhra University, Visakhapatnam, INDIA for their support to carry out experimentation. A very special thank you is due to Assistant Professor Dr. Apiwat Muttamara for insightful comments, helping clarify and improve the manuscript. 6. References  G. Madusudhan Reddy, A. A. Gokhale and K.Prasad Rao (1997), Weld microstructure refinement in a 1441 grade aluminium-lithium alloy , Journal of Material Science, Vol.32,pp.4117. K. Prasad Rao (2001), Proc of the national Conference on Recent Trends in Material Processing (RAMP, Annamalai University, India, 2001) p.176. Kondapalli Siva Prasad, Ch. Srinivasa Rao, D. Nageswara Rao (2011),Prediction of Weld Pool Geometry in Pulsed Current Micro Plasma Arc Welding of SS304L Stainless Steel Sheets, International Transaction Journal of Engineering, Management, & Applied Sciences & Technologies, Vol.2(3), 325-336. M. Balasubramanian, V.Jayabalan and V.Balasubramanian (2006), Optimizing the Pulsed Current Gas Tungsten Arc Welding Parameters, J Mater Sci Technol, Vol.22, Number.6, pp.821. M. Balasubramanian, V.Jayabalan and V.Balasubramanian (2008), Developing mathematical models to predict grain size and hardness of argon tungsten pulse current arc welded titanium alloy, Journal of Materials Processing Technology, Vol.196,pp.222-229. *Corresponding author (Kondapalli Siva Prasad). Tel/Fax: +91-9849212391. E-mail addresses:kspanits@gmail.com. 2011. International Transaction Journal of Engineering, Management, & Applied Sciences & Technologies. Volume 2 No.4. ISSN 2228-9860. 445 eISSN 1906-9642. Online Available at http://TuEngr.com/V02/437-446.pdf
  • 10. M. Balasubramanian, V.Jayabalan, V.Balasubramanian (2010), Effect of process parameters of pulsed current tungsten inert gas welding on weld pool geometry of titanium welds, Acta Metall.Sin.(Engl. Lett.) ,Vol.23 ,No.4,pp 312-320. N. Karunakaran, V.Balasubramanian (2011), Effect of pulsed current on temperature distribution, weld bead profiles and characteristics of gas tungsten arc welded aluminium alloy joints, Transactions of Nonferrous Metals Society of China, Vol.21, pp.278-286. Plasma Welding: more accurate, better control at lower currents (1999), Modern Application News. S.Babu, R.Senthil Kumar, V.Balasubramanian (2008), Optimizing pulsed current gas tungsten arc welding parameters of AA6061 aluminium alloy using Hooke and Jeeves algorithm, Transactions of Nonferrous Metals Society of China, Vol.18, pp.1028-1036. K.Siva Prasad is an Assistant Professor of Department of Mechanical Engineering at Anil Neerukonda Institute of Technology & Sciences, Visakhapatnam, India. He received his Bachelors degree from Osmania University, India and Master Degree from JNTU, Hyderabad, India. He is also a part time scholar at Andhra University. He is a member of various professional bodies like ISTE, FPSI, ISHRAE etc. His area of research is micro welding processes. Dr. Ch.Srinivasa Rao is an Associate Professor in the Mechanical Engineering Department at Andhra University, Visakhapatnam, India. He obtained his PhD degree from Andhra University, Visakhapatnam, India. He has published his research papers in various International Journals and conferences proceedings. He is a member of various professional bodies like ISTE, IE etc. His area of interest is manufacturing sciences, rapid prototyping and robotics. Dr. D.Nageswara Rao is a Professor in the Mechanical Engineering Department at Andhra University, Visakhapatnam, India. He obtained his PhD degree from Indian Institute of Technology Delhi, India. He is the coordinator for Centre for Nanotechnology at Andhra University. He has successfully completed various projects sponsored by DST, UGC, AICTE, NRB etc. His area of research is manufacturing sciences and nanotechnology. Peer Review: This article has been internationally peer-reviewed and accepted for publication according to the guidelines given at the journal’s website. 446 Kondapalli Siva Prasad, Ch.Srinivasa Rao, and D.Nageswara Rao