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Using RAE Systems
Colorimetric Gas Detection
    Tubes and Pumps
Important
            Cautions When
             Using Tubes
   Failure to wear protective equipment may lead to
    cuts and other severe injuries to eyes and hands
         Wear safety glasses and gloves when opening or
         handling tubes with sharp edges
   Always test the pump for leaks immediately
    before using it for a series of measurements
         Failure to test the pump for leakage may lead to
         dangerously inaccurate readings
Important Cautions
       When Using Tubes
   Avoid contact with tube contents in case of
    accidental breakage

         Exposure to tube contents can result in significant
         health hazards

   Dispose of spent tubes according to local
    regulations

         Review information listed in the Gas Detection
         Tube Data Sheet to identify materials that may
         require special disposal procedures.
The LP-1200 piston-type
                hand-pump description



        Draws fixed volume of gas, either 50 or 100 mL
        Vacuum seal formed by a greased plunger gasket
        Tapered inlet accommodates wide range of tubes
        Inlet filter protects the shaft from particulates
        Handle houses an end-of-flow indicator
        Built-in counter keeps track of the number of strokes


Operation of RAE Tubes and Pumps
RAE Colorimetric Tube
                 Description and Packaging




        Each box contains 10 tubes
        Instructions on back of box
        Arrow indicates direction of insertion and airflow
        Concentration scale and gas type printed on tube
        Number of strokes, total sample volume and units of
         measure also printed on tube
Operation of RAE Tubes and Pumps
Tube Data Sheet
                           Description
      Each box packaged with a Tube Data Sheet that
       gives detailed information on tube performance
      Partial data sheet sample:




Operation of RAE Tubes and Pumps
Testing the Hand-
            Pump for Leaks
   Insert unopened tube in hand-pump inlet
   Pull one-full stroke on plunger
   Wait two-minutes
   While holding the pump and plunger, rotate the
    plunger to release
   Allow the plunger to be drawn gently back into the
    pump shaft
   The plunger should return to within three millimeters
    of its original position
Measurement
                          Procedure
          Step One:
              Break both ends of a new detection tube using the tip
               breaker on the side of the pump


                       Step Two:
                        – Insert the tube, arrow towards the pump




Operation of RAE Tubes and Pumps
Measurement
                            Procedure
   Step Three:
       Select the sample volume desired and align the red dot on the
        plunger with the red dot on the pump shaft
Measurement
                                    Procedure
     Step Four:
           Pull the handle sharply until it locks (50 or 100 mL)
           Wait for the sampling time indicated on the data sheet to
            allow the air to be drawn through the tube




Operation of RAE Tubes and Pumps
Measurement
                                       Procedure
    Step Five:

          Flow is complete when the end-
           of-flow indicator returns to its full
           brightness.
          For additional strokes go to
                      step six, otherwise
           read the tube.




                               End-of-flow indicator



Operation of RAE Tubes and Pumps
Measurement
   Step Six:
                             Procedure
       For additional pump strokes, rotate the handle ¼ turn.




     – Push the plunger in without
       removing the tube.

     – Then repeat Step 4.
Measurement
                                     Procedure
          Step Seven:
              Empty broken glass bits
               from tube-tip reservoir as
               often as is necessary




Operation of RAE Tubes and Pumps
Reading Tubes
      The reading is the furthest point along the color change
      If the leading edge is diagonal or diffuse, use the average of the
       minimum and maximum values
      The three tubes shown below are all read as 6.5%




Operation of RAE Tubes and Pumps
Reading Tubes
   Read tube immediately after gas sampling, as colors
    may change, fade, or disperse with time

   If a non-standard number of pump strokes was used
    for sampling, multiply the reading by the correction
    factor given on the Tube Data Sheet

   If humidity and temperature corrections are
    necessary as indicated on the Data Sheets, multiply
    the observed readings by the given correction
    factor(s) (CF) to obtain the true concentration
Sampling Volumes
                  and Ranges
   Standard Sampling Volume and Ranges
       Standard stroke requirements are printed on each tube
       Gas concentrations can be measured by the scale printed
        on the tube
   Extended Sampling Volumes and Ranges
       Varying the number of strokes (volume) allows
        measurement of lower and higher concentrations than
        printed
       Varying the stroke means that the printed scale reading
        must be multiplied by a correction factor (CF)
Cross-Sensitivity
                        Cautions
   Colorimetric tubes are, by nature, selective;
   However, some compounds interfere with certain
    measurements
              Each Tube Data Sheet lists possible interfering
               compounds, but others may also exist

              Interfering compounds can increase or decrease
               the reading

              Be aware of potential interferences!
Maintenance of the LP-
        1200 Piston Hand Pump
   Tube Tip Reservoir
       Remove the tube tip reservoir
        cover as needed to empty the
        broken glass reservoir that is in
        the pump end fitting



            Tube-tip reservoir cover
Maintenance of the LP-
        1200 Piston Hand Pump
   Pump Inlet and Filter
       The rubber pump inlet can
        become worn with use and
        result in leaks
       Unscrew pump inlet nut and
        replace the rubber inlet
       If the inlet is not replaced,
        inspect the inlet filter and
        replace or clean the filter as
        necessary
Maintenance of the LP-
        1200 Piston Hand Pump
   Plunger gasket may leak if worn or not well
    lubricated
       To replace gasket, unscrew pump end fitting                   on
        the handle side, and pull plunger out of               the
        pump shaft
       After replacing gasket, carefully push plunger          back
        into the shaft
       Use a fine screwdriver or tweezers to help ease the gasket into
        the shaft
       Lubricate inside of shaft with vacuum grease to ensure a good
        seal
       Caution: Do not over tighten the plunger gasket as it could
        cause a sudden loss of vacuum
Maintenance of the LP-
        1200 Piston Hand Pump
   Inlet Valve
       Inlet check-valve may cause leaks if worn or not lubricated
       Unscrew the end-fitting on the inlet side, and pull out the
        disk-shaped rubber-inlet check-valve
       Replace as necessary, adding a light coat of grease around
        the hole
Maintenance of the LP-
        1200 Piston Hand Pump
   Outlet Valve
       Replace outlet check-valve gasket if there is resistance on
        the return stroke
       Using the special tool or needle-nose pliers, unscrew the
        plunger tip from the plunger rod
       Replace O-ring and check-valve gasket as necessary, and
        reassemble
       Inspect gasket-ring in the inlet end-fitting, and replace if
        damaged before screwing the end-fitting back on

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Using RAE Systems Colorimetric Gas Detection Tubes and Pumps

  • 1. Using RAE Systems Colorimetric Gas Detection Tubes and Pumps
  • 2. Important Cautions When Using Tubes  Failure to wear protective equipment may lead to cuts and other severe injuries to eyes and hands Wear safety glasses and gloves when opening or handling tubes with sharp edges  Always test the pump for leaks immediately before using it for a series of measurements Failure to test the pump for leakage may lead to dangerously inaccurate readings
  • 3. Important Cautions When Using Tubes  Avoid contact with tube contents in case of accidental breakage Exposure to tube contents can result in significant health hazards  Dispose of spent tubes according to local regulations Review information listed in the Gas Detection Tube Data Sheet to identify materials that may require special disposal procedures.
  • 4. The LP-1200 piston-type hand-pump description  Draws fixed volume of gas, either 50 or 100 mL  Vacuum seal formed by a greased plunger gasket  Tapered inlet accommodates wide range of tubes  Inlet filter protects the shaft from particulates  Handle houses an end-of-flow indicator  Built-in counter keeps track of the number of strokes Operation of RAE Tubes and Pumps
  • 5. RAE Colorimetric Tube Description and Packaging  Each box contains 10 tubes  Instructions on back of box  Arrow indicates direction of insertion and airflow  Concentration scale and gas type printed on tube  Number of strokes, total sample volume and units of measure also printed on tube Operation of RAE Tubes and Pumps
  • 6. Tube Data Sheet Description  Each box packaged with a Tube Data Sheet that gives detailed information on tube performance  Partial data sheet sample: Operation of RAE Tubes and Pumps
  • 7. Testing the Hand- Pump for Leaks  Insert unopened tube in hand-pump inlet  Pull one-full stroke on plunger  Wait two-minutes  While holding the pump and plunger, rotate the plunger to release  Allow the plunger to be drawn gently back into the pump shaft  The plunger should return to within three millimeters of its original position
  • 8. Measurement Procedure  Step One:  Break both ends of a new detection tube using the tip breaker on the side of the pump Step Two: – Insert the tube, arrow towards the pump Operation of RAE Tubes and Pumps
  • 9. Measurement Procedure  Step Three:  Select the sample volume desired and align the red dot on the plunger with the red dot on the pump shaft
  • 10. Measurement Procedure  Step Four:  Pull the handle sharply until it locks (50 or 100 mL)  Wait for the sampling time indicated on the data sheet to allow the air to be drawn through the tube Operation of RAE Tubes and Pumps
  • 11. Measurement Procedure  Step Five:  Flow is complete when the end- of-flow indicator returns to its full brightness.  For additional strokes go to step six, otherwise read the tube. End-of-flow indicator Operation of RAE Tubes and Pumps
  • 12. Measurement  Step Six: Procedure  For additional pump strokes, rotate the handle ¼ turn. – Push the plunger in without removing the tube. – Then repeat Step 4.
  • 13. Measurement Procedure  Step Seven:  Empty broken glass bits from tube-tip reservoir as often as is necessary Operation of RAE Tubes and Pumps
  • 14. Reading Tubes  The reading is the furthest point along the color change  If the leading edge is diagonal or diffuse, use the average of the minimum and maximum values  The three tubes shown below are all read as 6.5% Operation of RAE Tubes and Pumps
  • 15. Reading Tubes  Read tube immediately after gas sampling, as colors may change, fade, or disperse with time  If a non-standard number of pump strokes was used for sampling, multiply the reading by the correction factor given on the Tube Data Sheet  If humidity and temperature corrections are necessary as indicated on the Data Sheets, multiply the observed readings by the given correction factor(s) (CF) to obtain the true concentration
  • 16. Sampling Volumes and Ranges  Standard Sampling Volume and Ranges  Standard stroke requirements are printed on each tube  Gas concentrations can be measured by the scale printed on the tube  Extended Sampling Volumes and Ranges  Varying the number of strokes (volume) allows measurement of lower and higher concentrations than printed  Varying the stroke means that the printed scale reading must be multiplied by a correction factor (CF)
  • 17. Cross-Sensitivity Cautions  Colorimetric tubes are, by nature, selective;  However, some compounds interfere with certain measurements  Each Tube Data Sheet lists possible interfering compounds, but others may also exist  Interfering compounds can increase or decrease the reading  Be aware of potential interferences!
  • 18. Maintenance of the LP- 1200 Piston Hand Pump  Tube Tip Reservoir  Remove the tube tip reservoir cover as needed to empty the broken glass reservoir that is in the pump end fitting Tube-tip reservoir cover
  • 19. Maintenance of the LP- 1200 Piston Hand Pump  Pump Inlet and Filter  The rubber pump inlet can become worn with use and result in leaks  Unscrew pump inlet nut and replace the rubber inlet  If the inlet is not replaced, inspect the inlet filter and replace or clean the filter as necessary
  • 20. Maintenance of the LP- 1200 Piston Hand Pump  Plunger gasket may leak if worn or not well lubricated  To replace gasket, unscrew pump end fitting on the handle side, and pull plunger out of the pump shaft  After replacing gasket, carefully push plunger back into the shaft  Use a fine screwdriver or tweezers to help ease the gasket into the shaft  Lubricate inside of shaft with vacuum grease to ensure a good seal  Caution: Do not over tighten the plunger gasket as it could cause a sudden loss of vacuum
  • 21. Maintenance of the LP- 1200 Piston Hand Pump  Inlet Valve  Inlet check-valve may cause leaks if worn or not lubricated  Unscrew the end-fitting on the inlet side, and pull out the disk-shaped rubber-inlet check-valve  Replace as necessary, adding a light coat of grease around the hole
  • 22. Maintenance of the LP- 1200 Piston Hand Pump  Outlet Valve  Replace outlet check-valve gasket if there is resistance on the return stroke  Using the special tool or needle-nose pliers, unscrew the plunger tip from the plunger rod  Replace O-ring and check-valve gasket as necessary, and reassemble  Inspect gasket-ring in the inlet end-fitting, and replace if damaged before screwing the end-fitting back on