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Strategy for GPAT
By Payaam Vohra
Best Pharmacy
tips and tricks
All cology classification
All medchem class
All cognosy class
All anaylsis titrations and IMA
All ceutics formulations (IP ,PP)
All POC name reactions
Imp terminologies
Microbiology and biotech
Biopharmaceutics.
APP
Jurisprudence
Inorganic chem
Biochemistry
Miscellaneous topics
Things that will be covered during the sessions
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Parameters Tablets Capsules Parenterals Aerosols
Evaluation Hardness Uniformity of wt,
Uniformity of content
Dissolution Wt variation
Disintegration Friability
Morphological,Bloom
strength,Iron content-(15PPm),
Viscosity(25-45 mp),Base
adsorption, MC,Content
uniformi ,Wt variation
Sterility Pyrogenicity Leakage
(1% Methyelene
blue),Clarity,Particulate matter
Particle size
distrbituion,Identifciati
on,MC,Flash point
Flame ,Vap pree,foam
stability ,Spray
pattern,Density
Method Dry Wet Direct slugging
Chilsonator roller compa
Aseptic area Clean area Cold,Pressure Vaccum
filling
Excipients Binder 10-20% glidant diluents
disintegrants 5% Super
disintegrant adherants
antiadherant Lubricants
Colouring ,flavouring
sweetening
Gelatin , HPMC, Opacifying,
Diluents, Plasticizer, Absorbents
vehicles/solvents, tonicity
agents, buffers, solubilizing
agents (such co-solvents,
surfactants, complexing agents),
bulking agents,osmotic agent
antimicrobials/preservatives,
Viscosity modfifer, antioxidants,
chelating agents
Cryoprotectans Lyoprotectants
Propellant,Wetting,Hu
mectant, Antifoaming
Equipments Multipunch rotary die press Zanasi Eli lily, Rotosort
Rotofill,Accogel, Accogil
Dip tube Actuator
Canister Gasket
Miscellaneous Tablet defects,Sugar and
Enteric coated polymer
Type a and b gelatin ,
Glcyerin :gelatin
Preformulation consideration 140-180 psi pressure
at 130 F/ 70 degree
Capping Lamination Blushing ,Mottlling Blooming
Type A TYPE B
Pork skin Bovine bones
Acidic Basic
9 4.7
Capsule Ratio
HGC 0.4/1
Intermediate 0.6/1
Soft 0.8/1
Cascae impactor-Particle szie
Gas crgayp-Mositure content
Hygrometer-density
Tag open cup appratus- - 25 f
Propellant- Ir spectrsocopy
Rotosort-Unfilled capsules
Accogel-Powder in SGC
Accofill-Powder in HGC
Nacl-0.9 % w/v
Dextrose- 5% w/v
Antioxidants
BHT, BHA,Tocopherols
Monsanto
Erweka
Strong cobb
Schrolonguier
Pftizer
20 tablets - potency
30 tablets-Content of unifromity
10 mesh size 37+ 2 - Disintegration
20 mesh size 37+ 0.5- Dissolution
Roche friabolotr- 1%
Propellant 11-Trichloromonoflurourmethane
Propellant 12-dicholor difluroormethan
prope 114-dichloro tetrafluror ethane
FTM- aerobic and anaerboic 30-35 degree 7 days
SCDM-Aerobic fingi-20-25 degree -14 days
Base
adsotption
Capsule
size
Less filling
capacity
Density
Anti fungal, bacterial, Viral ,protozoal, Parasitic, Amoebic, Helminthic, Malarial, Cancer, Gout, Rheumatism,
Parkinson, Alzheimer, Depressant, Thyroid, Diabetic ,Anticoagulant
Mania Bipolar, Anxiety, Sedative Hypnotic, Local anesthetic, General anesthetic, erectile dysfunction, Pre anesthetic, Coagulants,
Fibrinolytics , Antithrombotic, Leprotic
Anti-inflammatory ,pyretic , analgesic, Cholinergic ,AC , adrenergic, AA, Myasthenia gravis , Alcohols, Skeletal muscle relaxants, Glaucoma,
Tubercular
Antiulcer, Anti arrhythmic ,Anginals,Hyperlipidaemics,CHF,DiureticsHypertension,Antibiotics ,Anabolic steroids, Insulin analogues,UTI
Antiasthma, Hormones ,(Estrogen progesterone Testosterone) ,oral contraceptives, Corticosteroids, Tranquilizers (Schizophrenia),Protein target
drugs
Laxative, Immunosuppressants and stimulants, Tocolytics, Oxytociosis, Hormones (ACTH STH MSH prolactin),STD,Mab ,Biosmilars
Antiemetic, Drugs of abuse, Hallucinogens, Nootropics Hematinic, Shock, Calcium level, Antipsychotics,Appetite regulators,
Autocoids(Histamine serotonin PG ),Nasal decongestant ,Expectorant ,Respiratory stimulnts,Digestants,Posioning (Lead arsenic Mercury)
Pharmacology MedChem
ADR
DRUG interactions
SAR
MOA
Tafts stearic, hammets Electronic, Hanstch analysis
Iodo
Iodi
Bromato Cerio Permangano Dichrom Iodato
Mohr Volhard Fajan
Gay
lussac
T
IMA Titrations
Acid base(Neutralization)
SA-SB
WA-WB
SA-WB
WA-SB
Redox
Precipitation
Complexometric
Gravimetric
Indicators
Primary and seconday
Colour change
For acidic Ph=7.9 pka =6.9 PH-PKA
For basic Ph=7.9 pka=8.9 PKA -PH
Solubility
Complexation
Preformulation
Kinetics
States of Matter
Incompatibliets
Thermodynamics
Acids and bases buffer
Antidotes
PP and Ip
Krebs glycolysis ETS
Acetate mevalonate
Proteins Amino acids
Carbohydrates
Lipids
Identification tests classification uses
Urea cycle
Vitamins
Enzymes
Few disorder( Black urine)
Acid saponification Iodine values
Synthesis and metbaolism of ACH adrenaline
Biochemistry
Potentiometry
Conductomtery
Polarography(Ilkovic
majorly) Differnce
between indicator
and Ref
Nephelturbidometry
Fluorimetry
UV IR NMR FLAME
AAS MASS
spectroscopy
Chromatography
Electrophoresis
Analysis
TLC paper Gc hplc gel affinity ion
exchange
gel
eclect
paper
elecet
capillar
y elec
principle detector detrctor principle ligand types zone types mb
procedu
re
injector injector gel
permati
on
spacer
arm
iec epm eof
devlop
tech
colum
oven
pump tev types
injecting injecting
carrier
gas
mp rese
temp
progra
Strategy for GPAT.pptx
Param
eters
IR FLAME AAS AES Nephel
o-
turbido
FLuo
rimtr
y
UV NMR MASS
Detecto
r
Sample
holder
Source
Graph
Sample
Ref
stand
Suspension
Emulsion
Micromeretics
Rheology
Solublity
Complexation
Interfacial tension
Ceutics
α (alpha)-cyclodextrin: 6 glucose subunits. β (beta)-cyclodextrin: 7
glucose subunits. γ (gamma)-cyclodextrin: 8 glucose subunits.
Strategy for GPAT.pptx
Steroids
proteins
Carbs
Tropane
Alkaloids
Antraquinoin glcyoi
Pale catechu
Flavanoids
Tannins
Sudan red 3 Volatile oil
Cuoaxam Cellulose
Ruthenium red Mucilage
Phloroglucinol con
hcl
Lignin
Extraction techniques(Soxhlation , Craigs, Infusion Decotion maceration
Shikimic acid
Cognosy
Category Name Therapeutic
activity
Miscellaneous Subcategory B.S Active
consituent
Family
Alkaloids Vinca Anti cancer Indole Leaf Vincristin Apocynacae
Glycosides Digitalis CHF leaf Digoxin
Tannins Catechu catechutannic
Resins Benzoin
Flavanoids Rutin Capillary per
Volatile oils Fennel
Cognsoy
Radioactive
Hematinic
Dentifrices (Fluoride)
Heat transfer (Fouriers and Kirchoffs law)
Limit tests Packagings
Buffer
Few Ophthalmic concepts
Inorganic chemistry
Alcohol Phenol aldehyde Ketone Amine acid Ester
Lucas Fecl3 Sodi nitorpru Carbylamine Na2CO3 Fruity smell
Victor mayer Bromine water Iodoform Nitrous acid Fluroesein
Picric acid Hinsberg Esterification
ELISA, Western, Southern blotting
Sterilization
Gram acid fast staining
Sterility testing
IMVIC
Vaccines
Fermentation
Enzyme immobilization
Immunity -MHC
Blood products
Analytical Validation
Microbiology and Biotech
•Fscher Indole Synthesis
•Walden Inversion
•Perkin Reaction Mechanism
•Diels-Alder Reaction Mechanism
•Michael Addition Mechanism
•Heck Reaction
•Mannich Reaction Mechanism
•Hydroboration oxidation reaction
•Claisen condensation
•Lindlar Catalyst
•Maillard Reaction
•Robinson Annulation
•Woodward Reaction
•Oppenauer Oxidation
POC name reactions
L
Lossen rearrangement
Marknoikov,
Peterson
Pechmann
Kharash mayo effect
Coulson moffit,
Rosenumund
Sasche moh,Paal knorr
,Haworth
,knoor pyrrole,,
Skraup synthesis
PIncole pinacolone
Bayers strain,
Saythzeff
A
Aldol
Arndt-Eistert Synthesis
B
Baeyer-Villiger oxidation
Bartoli indole synthesis
Beckmann rearrangement
Birch reduction
Bamford steven
C
Cannizzaro reaction
Claisen condensation
Claisen rearrangement
Clemmensen reduction
Cope rearrangement
Corey House synthesis
Curtius rearrangement
D
Dakin-West reaction
Doebner miller synthesis
Dieckmann condensation
Diels-Alder reaction
Darzen reaction
F
Finkelstein reaction
Fischer esterification
Fischer indole synthesis
Friedel-Crafts acylation and alkylation
Fries rearrangement
Favosrki
Fittig
Friendlander
Hybridization
Acidity and basicity
OP directing activating and deactivating
SN1 SN2 E1 E2
Isomerism
BCS class
HAP
Reference books and which topic to
refer from which book
Images adopted from Solution pharmacy
Compartment modelling
Linear and causes on non linearity
Reynolds number Bernoullis theorem
Receptor types
ADME
BPPK and PE
Name Principle Uses Type Disadvantage Miscellaneous
Ball mill Size reduction
Fractional Distillation
Perforated Centrifugation
Falling film Evaporation
Plate and frame Filtration
Elutriation tank Size sepration
Sigma blade Mixing
crystallization
Fluidized Bed Drying
Venturimeter Flow of fluid
D AND C
MTP
ICH
NDPS
IPR( GI,CCOPYRIGHT TRADEMARK,PATENT
PHARMACY ACT
DRUG AND MAGIC REMEDIES
TOILET PREPRATIONS
IP Publciations
Hatch Waxmann act
Drug discovery and developemtn phasses clinical trials
Jurisprudence
Strategy for GPAT.pptx
1) GLASS
2) PLASTIC
3) RUBBER
Strategy for GPAT.pptx

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Strategy for GPAT.pptx

  • 1. Strategy for GPAT By Payaam Vohra
  • 2. Best Pharmacy tips and tricks All cology classification All medchem class All cognosy class All anaylsis titrations and IMA All ceutics formulations (IP ,PP) All POC name reactions Imp terminologies Microbiology and biotech Biopharmaceutics. APP Jurisprudence Inorganic chem Biochemistry Miscellaneous topics Things that will be covered during the sessions
  • 3. No 3D Model? No Problem! Microsoft makes it easy to insert a 3D Model! Simply go to the Insert Ribbon and click on the 3D Models option. Choose the option for online sources gallery (shown at the right). Select the model you wish to insert. 3D Models is a subscription-only feature. If you have a subscription, the next slide shows you how it works in a new presentation. Parameters Tablets Capsules Parenterals Aerosols Evaluation Hardness Uniformity of wt, Uniformity of content Dissolution Wt variation Disintegration Friability Morphological,Bloom strength,Iron content-(15PPm), Viscosity(25-45 mp),Base adsorption, MC,Content uniformi ,Wt variation Sterility Pyrogenicity Leakage (1% Methyelene blue),Clarity,Particulate matter Particle size distrbituion,Identifciati on,MC,Flash point Flame ,Vap pree,foam stability ,Spray pattern,Density Method Dry Wet Direct slugging Chilsonator roller compa Aseptic area Clean area Cold,Pressure Vaccum filling Excipients Binder 10-20% glidant diluents disintegrants 5% Super disintegrant adherants antiadherant Lubricants Colouring ,flavouring sweetening Gelatin , HPMC, Opacifying, Diluents, Plasticizer, Absorbents vehicles/solvents, tonicity agents, buffers, solubilizing agents (such co-solvents, surfactants, complexing agents), bulking agents,osmotic agent antimicrobials/preservatives, Viscosity modfifer, antioxidants, chelating agents Cryoprotectans Lyoprotectants Propellant,Wetting,Hu mectant, Antifoaming Equipments Multipunch rotary die press Zanasi Eli lily, Rotosort Rotofill,Accogel, Accogil Dip tube Actuator Canister Gasket Miscellaneous Tablet defects,Sugar and Enteric coated polymer Type a and b gelatin , Glcyerin :gelatin Preformulation consideration 140-180 psi pressure at 130 F/ 70 degree
  • 4. Capping Lamination Blushing ,Mottlling Blooming Type A TYPE B Pork skin Bovine bones Acidic Basic 9 4.7 Capsule Ratio HGC 0.4/1 Intermediate 0.6/1 Soft 0.8/1
  • 5. Cascae impactor-Particle szie Gas crgayp-Mositure content Hygrometer-density Tag open cup appratus- - 25 f Propellant- Ir spectrsocopy Rotosort-Unfilled capsules Accogel-Powder in SGC Accofill-Powder in HGC Nacl-0.9 % w/v Dextrose- 5% w/v Antioxidants BHT, BHA,Tocopherols
  • 6. Monsanto Erweka Strong cobb Schrolonguier Pftizer 20 tablets - potency 30 tablets-Content of unifromity 10 mesh size 37+ 2 - Disintegration 20 mesh size 37+ 0.5- Dissolution Roche friabolotr- 1% Propellant 11-Trichloromonoflurourmethane Propellant 12-dicholor difluroormethan prope 114-dichloro tetrafluror ethane
  • 7. FTM- aerobic and anaerboic 30-35 degree 7 days SCDM-Aerobic fingi-20-25 degree -14 days Base adsotption Capsule size Less filling capacity Density
  • 8. Anti fungal, bacterial, Viral ,protozoal, Parasitic, Amoebic, Helminthic, Malarial, Cancer, Gout, Rheumatism, Parkinson, Alzheimer, Depressant, Thyroid, Diabetic ,Anticoagulant Mania Bipolar, Anxiety, Sedative Hypnotic, Local anesthetic, General anesthetic, erectile dysfunction, Pre anesthetic, Coagulants, Fibrinolytics , Antithrombotic, Leprotic Anti-inflammatory ,pyretic , analgesic, Cholinergic ,AC , adrenergic, AA, Myasthenia gravis , Alcohols, Skeletal muscle relaxants, Glaucoma, Tubercular Antiulcer, Anti arrhythmic ,Anginals,Hyperlipidaemics,CHF,DiureticsHypertension,Antibiotics ,Anabolic steroids, Insulin analogues,UTI Antiasthma, Hormones ,(Estrogen progesterone Testosterone) ,oral contraceptives, Corticosteroids, Tranquilizers (Schizophrenia),Protein target drugs Laxative, Immunosuppressants and stimulants, Tocolytics, Oxytociosis, Hormones (ACTH STH MSH prolactin),STD,Mab ,Biosmilars Antiemetic, Drugs of abuse, Hallucinogens, Nootropics Hematinic, Shock, Calcium level, Antipsychotics,Appetite regulators, Autocoids(Histamine serotonin PG ),Nasal decongestant ,Expectorant ,Respiratory stimulnts,Digestants,Posioning (Lead arsenic Mercury) Pharmacology MedChem
  • 9. ADR DRUG interactions SAR MOA Tafts stearic, hammets Electronic, Hanstch analysis
  • 10. Iodo Iodi Bromato Cerio Permangano Dichrom Iodato Mohr Volhard Fajan Gay lussac T IMA Titrations Acid base(Neutralization) SA-SB WA-WB SA-WB WA-SB Redox Precipitation Complexometric Gravimetric Indicators Primary and seconday Colour change
  • 11. For acidic Ph=7.9 pka =6.9 PH-PKA For basic Ph=7.9 pka=8.9 PKA -PH
  • 13. Krebs glycolysis ETS Acetate mevalonate Proteins Amino acids Carbohydrates Lipids Identification tests classification uses Urea cycle Vitamins Enzymes Few disorder( Black urine) Acid saponification Iodine values Synthesis and metbaolism of ACH adrenaline Biochemistry
  • 14. Potentiometry Conductomtery Polarography(Ilkovic majorly) Differnce between indicator and Ref Nephelturbidometry Fluorimetry UV IR NMR FLAME AAS MASS spectroscopy Chromatography Electrophoresis Analysis TLC paper Gc hplc gel affinity ion exchange gel eclect paper elecet capillar y elec principle detector detrctor principle ligand types zone types mb procedu re injector injector gel permati on spacer arm iec epm eof devlop tech colum oven pump tev types injecting injecting carrier gas mp rese temp progra
  • 16. Param eters IR FLAME AAS AES Nephel o- turbido FLuo rimtr y UV NMR MASS Detecto r Sample holder Source Graph Sample Ref stand
  • 17. Suspension Emulsion Micromeretics Rheology Solublity Complexation Interfacial tension Ceutics α (alpha)-cyclodextrin: 6 glucose subunits. β (beta)-cyclodextrin: 7 glucose subunits. γ (gamma)-cyclodextrin: 8 glucose subunits.
  • 19. Steroids proteins Carbs Tropane Alkaloids Antraquinoin glcyoi Pale catechu Flavanoids Tannins Sudan red 3 Volatile oil Cuoaxam Cellulose Ruthenium red Mucilage Phloroglucinol con hcl Lignin Extraction techniques(Soxhlation , Craigs, Infusion Decotion maceration Shikimic acid Cognosy
  • 20. Category Name Therapeutic activity Miscellaneous Subcategory B.S Active consituent Family Alkaloids Vinca Anti cancer Indole Leaf Vincristin Apocynacae Glycosides Digitalis CHF leaf Digoxin Tannins Catechu catechutannic Resins Benzoin Flavanoids Rutin Capillary per Volatile oils Fennel Cognsoy
  • 21. Radioactive Hematinic Dentifrices (Fluoride) Heat transfer (Fouriers and Kirchoffs law) Limit tests Packagings Buffer Few Ophthalmic concepts Inorganic chemistry Alcohol Phenol aldehyde Ketone Amine acid Ester Lucas Fecl3 Sodi nitorpru Carbylamine Na2CO3 Fruity smell Victor mayer Bromine water Iodoform Nitrous acid Fluroesein Picric acid Hinsberg Esterification
  • 22. ELISA, Western, Southern blotting Sterilization Gram acid fast staining Sterility testing IMVIC Vaccines Fermentation Enzyme immobilization Immunity -MHC Blood products Analytical Validation Microbiology and Biotech
  • 23. •Fscher Indole Synthesis •Walden Inversion •Perkin Reaction Mechanism •Diels-Alder Reaction Mechanism •Michael Addition Mechanism •Heck Reaction •Mannich Reaction Mechanism •Hydroboration oxidation reaction •Claisen condensation •Lindlar Catalyst •Maillard Reaction •Robinson Annulation •Woodward Reaction •Oppenauer Oxidation POC name reactions
  • 24. L Lossen rearrangement Marknoikov, Peterson Pechmann Kharash mayo effect Coulson moffit, Rosenumund Sasche moh,Paal knorr ,Haworth ,knoor pyrrole,, Skraup synthesis PIncole pinacolone Bayers strain, Saythzeff A Aldol Arndt-Eistert Synthesis B Baeyer-Villiger oxidation Bartoli indole synthesis Beckmann rearrangement Birch reduction Bamford steven C Cannizzaro reaction Claisen condensation Claisen rearrangement Clemmensen reduction Cope rearrangement Corey House synthesis Curtius rearrangement D Dakin-West reaction Doebner miller synthesis Dieckmann condensation Diels-Alder reaction Darzen reaction F Finkelstein reaction Fischer esterification Fischer indole synthesis Friedel-Crafts acylation and alkylation Fries rearrangement Favosrki Fittig Friendlander
  • 25. Hybridization Acidity and basicity OP directing activating and deactivating SN1 SN2 E1 E2 Isomerism BCS class
  • 26. HAP Reference books and which topic to refer from which book Images adopted from Solution pharmacy
  • 27. Compartment modelling Linear and causes on non linearity Reynolds number Bernoullis theorem Receptor types ADME BPPK and PE Name Principle Uses Type Disadvantage Miscellaneous Ball mill Size reduction Fractional Distillation Perforated Centrifugation Falling film Evaporation Plate and frame Filtration Elutriation tank Size sepration Sigma blade Mixing crystallization Fluidized Bed Drying Venturimeter Flow of fluid
  • 28. D AND C MTP ICH NDPS IPR( GI,CCOPYRIGHT TRADEMARK,PATENT PHARMACY ACT DRUG AND MAGIC REMEDIES TOILET PREPRATIONS IP Publciations Hatch Waxmann act Drug discovery and developemtn phasses clinical trials Jurisprudence