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Background 
An empirical formula describes the simplest ratio for of each type of atom that a compound contains, whereas the molecular 
formula gives the actual number of atoms in that compound. The empirical formula of a compound can be derived by finding 
the number of moles of the elements in a sample compound and then determining the simplest ratio between them. The 
molar ratio represents the simplest ratio for the number of moles of each element in a particular compound rather than the 
total number of moles in the compound. 
In this lab we will form copper oxide using two methods. The first method is simply to heat dry copper powder until it 
combines with oxygen in the air. Comparing the mass of copper to the mass of copper oxide allows us to determine the ratio 
of copper to oxygen in the compound. 
The second method uses an aqueous solution of copper(II) sulfate (CuSO 4 
) combined with sodium hydroxide (NaOH) which 
yields a copper hydroxide precipitate. This precipitate is then heated until a decomposition reaction yields water vapor and 
copper oxide. Since we know exactly how much copper sulfate we begin with, is possible to calculate the molar quantity of 
copper oxide that is formed and then determine its empirical formula.
Procedures 
Experiment 1 
1. Place a clean crucible from the Containers shelf onto the workbench. 
2. Place a balance and Bunsen burner from the Instruments shelf onto the workbench. 
3. Move the crucible onto the balance and record the mass of the crucible in your notes. 
4. Move the crucible onto the workbench and add 10 g of copper (Cu) from the Materials shelf into it. 
5. Move crucible onto the balance and record the combined mass of the crucible plus copper in your notes. Does the 
number make sense? 
6. Move the crucible onto the Bunsen burner. Double-click the crucible to open its properties. Select Show Contents and 
click OK. (This cut-away gives you a view of the Crucible's contents.) 
7. Turn on the Bunsen burner and set the flame to low. To turn on the burner, click on the black knob. (Clicking multiple 
times will increase the intensity of the flame until it is turned off.) 
8. Start the Timer by clicking on the clock icon in the lower left of the window frame. 
9. The copper will react with the oxygen in the air. You will see the contents of the crucible change color, signifying that the 
reaction is complete. Watch the crucible for an additional 30 – 60 seconds to verify that no further reactions occur. 
(You may want to use the + or – zoom buttons in the lower right of the screen for a closer view.) 
10. Move the crucible onto the workbench to cool and turn off the Bunsen burner. 
11. Weigh the crucible and its contents. Record the total mass. (Remember to press Save Notes so you don't lose your 
calculations.) 
Did the mass of the crucible's contents increase or decrease? 
12. Clear the workbench by dragging your containers to the recycling bin beneath the workbench. 
Experiment 2 
1. Place a 50 mL beaker from the Containers shelf onto the balance. Record the mass. 
2. Move the beaker onto the workbench and add 5 g of copper sulfate pentahydrate (CuSO *5H O) from the Materials 
shelf. 
4 2 
3. Weigh the beaker and record the combined mass of the beaker and its contents in your notes. 
4. Dissolve the copper sulfate pentahydrate by adding 30 mL of water to the beaker. 
Note: In a conventional wet lab, you would remove the container from the balance before you add any chemicals or 
solutions. Filling the container separately prevents any spills, sprays, or splashes that might affect your measurements 
when they land on the balance.
Luckily our virtual labs are spill-, spray-, and splash-free, so we skip that step to save time. 
5. Add 10 mL of 6M sodium hydroxide (NaOH) to the beaker. Observe the beaker for signs of a reaction and record your 
observations in your Lab Notes. 
(You may want to use the + or – zoom buttons in the lower right of the screen for a closer view.) 
6. Place a clean beaker from the Containers shelf onto the workbench. 
7. Decant the first beaker by moving it onto the empty beaker. Select the Decant option from the pop-up window and click 
OK. You should see the liquid transfer to the beaker. The solid will remain behind in the original beaker. 
8. Place a clean test tube from the Containers shelf onto the workbench. 
9. Determine the mass of the empty test tube by placing it on the balance. Record the mass in your notes. 
10. Transfer the solid precipitate from the beaker into the test tube by placing the beaker onto the test tube and selecting 
Pour All. 
11. Move the test tube on the Bunsen burner and click the black knob to the lowest setting. Start a timer. 
12. Over time the solid will decompose into copper oxygen in the air and water is released into the air as water vapor. You 
will then see the contents of the test tube change, signifying that the reaction is complete. Watch the crucible for an 
additional 30 – 60 seconds to verify that no further reactions occur. 
13. Move the test tube on the workbench to cool. (Do not skip this step.) 
14. Weigh the test tube and record the mass in your Lab Notes. (Remember to save your notes.)
Notes

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Lab4

  • 1. Background An empirical formula describes the simplest ratio for of each type of atom that a compound contains, whereas the molecular formula gives the actual number of atoms in that compound. The empirical formula of a compound can be derived by finding the number of moles of the elements in a sample compound and then determining the simplest ratio between them. The molar ratio represents the simplest ratio for the number of moles of each element in a particular compound rather than the total number of moles in the compound. In this lab we will form copper oxide using two methods. The first method is simply to heat dry copper powder until it combines with oxygen in the air. Comparing the mass of copper to the mass of copper oxide allows us to determine the ratio of copper to oxygen in the compound. The second method uses an aqueous solution of copper(II) sulfate (CuSO 4 ) combined with sodium hydroxide (NaOH) which yields a copper hydroxide precipitate. This precipitate is then heated until a decomposition reaction yields water vapor and copper oxide. Since we know exactly how much copper sulfate we begin with, is possible to calculate the molar quantity of copper oxide that is formed and then determine its empirical formula.
  • 2. Procedures Experiment 1 1. Place a clean crucible from the Containers shelf onto the workbench. 2. Place a balance and Bunsen burner from the Instruments shelf onto the workbench. 3. Move the crucible onto the balance and record the mass of the crucible in your notes. 4. Move the crucible onto the workbench and add 10 g of copper (Cu) from the Materials shelf into it. 5. Move crucible onto the balance and record the combined mass of the crucible plus copper in your notes. Does the number make sense? 6. Move the crucible onto the Bunsen burner. Double-click the crucible to open its properties. Select Show Contents and click OK. (This cut-away gives you a view of the Crucible's contents.) 7. Turn on the Bunsen burner and set the flame to low. To turn on the burner, click on the black knob. (Clicking multiple times will increase the intensity of the flame until it is turned off.) 8. Start the Timer by clicking on the clock icon in the lower left of the window frame. 9. The copper will react with the oxygen in the air. You will see the contents of the crucible change color, signifying that the reaction is complete. Watch the crucible for an additional 30 – 60 seconds to verify that no further reactions occur. (You may want to use the + or – zoom buttons in the lower right of the screen for a closer view.) 10. Move the crucible onto the workbench to cool and turn off the Bunsen burner. 11. Weigh the crucible and its contents. Record the total mass. (Remember to press Save Notes so you don't lose your calculations.) Did the mass of the crucible's contents increase or decrease? 12. Clear the workbench by dragging your containers to the recycling bin beneath the workbench. Experiment 2 1. Place a 50 mL beaker from the Containers shelf onto the balance. Record the mass. 2. Move the beaker onto the workbench and add 5 g of copper sulfate pentahydrate (CuSO *5H O) from the Materials shelf. 4 2 3. Weigh the beaker and record the combined mass of the beaker and its contents in your notes. 4. Dissolve the copper sulfate pentahydrate by adding 30 mL of water to the beaker. Note: In a conventional wet lab, you would remove the container from the balance before you add any chemicals or solutions. Filling the container separately prevents any spills, sprays, or splashes that might affect your measurements when they land on the balance.
  • 3. Luckily our virtual labs are spill-, spray-, and splash-free, so we skip that step to save time. 5. Add 10 mL of 6M sodium hydroxide (NaOH) to the beaker. Observe the beaker for signs of a reaction and record your observations in your Lab Notes. (You may want to use the + or – zoom buttons in the lower right of the screen for a closer view.) 6. Place a clean beaker from the Containers shelf onto the workbench. 7. Decant the first beaker by moving it onto the empty beaker. Select the Decant option from the pop-up window and click OK. You should see the liquid transfer to the beaker. The solid will remain behind in the original beaker. 8. Place a clean test tube from the Containers shelf onto the workbench. 9. Determine the mass of the empty test tube by placing it on the balance. Record the mass in your notes. 10. Transfer the solid precipitate from the beaker into the test tube by placing the beaker onto the test tube and selecting Pour All. 11. Move the test tube on the Bunsen burner and click the black knob to the lowest setting. Start a timer. 12. Over time the solid will decompose into copper oxygen in the air and water is released into the air as water vapor. You will then see the contents of the test tube change, signifying that the reaction is complete. Watch the crucible for an additional 30 – 60 seconds to verify that no further reactions occur. 13. Move the test tube on the workbench to cool. (Do not skip this step.) 14. Weigh the test tube and record the mass in your Lab Notes. (Remember to save your notes.)