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COLD CREAMS
Dr. Prashant L. Pingale
Associate Professor,
Dept. of Pharmaceutics,
GES’s Sir Dr. M. S. Gosavi College of Pharm. Edu. and Research,
Nashik-422005
An emulsion of water and certain fats, usually
including beeswax and various scent agents,
designed to smooth skin and remove makeup.
The name derives from the cool feeling that the
cream leaves on the skin.
2
• Cold cream produces cooling effect becoz slow
evaporation of water present in the emulsion.
• In olden days the cold cream was prepared from
animal fats & vegetable oils but
– Vegetable oils: rancid so replaced by mineral oils
which gives more stable product.
3
• Mechanism of action on skin:
– o/w type of emulsion but after application on skin,
sufficient water evaporates to permit phase inversion
to w/o type.
4
Formulation:
• Formula 1
• Bees wax ---- 5%
• Liquid paraffin ---- 45%
• White soft paraffin ----10%
• Hard paraffin ---- 7%
• Borax ---- 0.2%
• Water ---- 32.8%
• Perfume ---- q.s
• Formula 2
• Bees wax ---- 16%
• Liquid paraffin ---- 50%
• Borax ---- 0.8%
• Water ---- 33.2%
• Perfume ---- q.s
5
General procedure
– Weigh all ingredients in reqd qty.
– Melt the wax and other ings. in their decreasing order
of m.p. on water bath
– Dissolve borax in water at 70-750C
– Add both phase together i.e. oil & water
– Add reqd qty of preservative & perfume
– Transfer the cream to container while hot.
6
• Storage:
– Stored in a well closed container at a temperature not exceeds 250C.
– Stored in a cool place.
• Labeling:
– Label should indicate following:
• Name of active ingredient(s)
• Quantity (in mg. , gm., or %)
• Net content
• Batch
• Mfg. Date
• Exp. Date
• Manufactured by
• Marketed by
• Storage condition
• Direction
• Special instruction if any
7
Evaluation parameters
– Consistency (viscosity)
– Skin irritation test
– Net content in the container
– Test for microbial growth
– Rancidity
– Color & physical appearance test
8
Marketed Products
• Pond’s cold cream
• Ayur herbal cold cream
• Emani cold cream
• Aloe vera cold cream
9
VANISHING CREAMS
• Creams spread easily & seem to disappear rapidly when rubbed
on skin are termed as vanishing creams.
• These are an o/w type of emulsions which when applied to the
skin leave an almost invisible layer on it so called vanishing
creams.
• These creams can be quickly washed off with water due to the
presence of o/w emulsifiers
DEFINITION
11
• These creams are prepared by emulsification of stearic acid &
water by means of alkalies like NaOH, KOH, borax, triethanolamine
etc..
• Synonym: greaseless cream
• An oil-in-water emulsion containing potassium, ammonium, or
sodium stearate with water and holding in emulsified form more or
less free stearic acid;
General Discussion
12
• It also contains a hygroscopic ingredient such as glycerol, and a
small amount of a fatty ingredient;
• It leaves a protective, invisible film of stearic acid on the skin.
• The main ingredients are:
• Stearic acid which gives pearly white shining appearance to the
cream, after application gives thin white film of free stearic
acid.
13
• Stearic acid (550C)-- protective
• High quality is used bcoz to provide an oil phase, which melts
above body tempt.
• Provides non-greasy film
• Produce very attractive appearance
• KOH or NaOH :- to neutralize free fatty acid
• NaOH makes a harder cream than KOH.
• Triethanolamine is also used instead which makes preparation
easy & viable nature.
• borax is used to make white creams but product has tendency
to grain (small piece)
FORMULATION
14
• Glycerin 10% of total
• Used to maintain consistency
• Enhance spreading ability
• Water in large qty. so preservative required to
prevent microbial growth
• Methyl parahydroxy benzoate (0.12%)
• Propyl parahydroxy benzoate (0.12%) in combination
• Perfume
• Sandalwood, lavender oil, linalol, rose, geraniol etc…
15
• Stearic acid ---- 20%
• Cetyl alcohol ---- 0.5%
• Triethanolamine ---- 1.2%
• NaOH ---- 0.36%
• Glycerin ---- 8%
• Water ---- 69.94%
• Preservative ---- q.s.
• Perfume ---- q.s.
• Procedure:
– Weigh all ingredients & heat or melt Ist part ingredients (from 1to 3) in a
container
– Heat or melt IInd part ingredients in a beaker
– Add IInd part mixture to Ist part with continuous stirring
– Cool with continuous stirring
– Add perfume when tempt. is about 350 C.
– Mill it (uniform mixing)
Formula
16
• Storage:
– Stored in a well closed container at a temperature not exceeds 250C.
– Stored in a cool place.
• Labeling:
– Label should indicate following:
• Name of active ingredient(s)
• Quantity (in mg. , gm., or %)
• Net content
• Batch
• Mfg. Date
• Exp. Date
• Manufactured by
• Marketed by
• Storage condition
• Direction
• Special instruction if any
17
• Evaluation of vanishing creams:
– Rheology or viscosity
– Skin sensitivity or patch test
– Biological testing (antiseptic, hormones, vitamins etc..)
– Net content
18
• Marketed Products:
– Lakme,
– Max-factor,
– Ponds,
– Charmis.
19
CLEANSING
CREAMS
21
DEFINITION
 These are cosmetic preparations used to be applied
on skin for removing the facial makeup.
 They are also used to improve the healthy & good
appearance to the skin
 These are same as cold creams but contains detergent
for cleaning action.
 They contain other ingredients which helps to soften,
lubricate or protect the skin.
22
• Cleansing Cream is used to clean the face of makeup and the
dust before going to bed.
• The layers of makeup, dust and sweat remain as a coat on the
face and do not allow the skin breathe which may result in
wrinkles an dullness on skin.
• Cleansing Creams is made with a mixture of:
– stearic acid,
– mineral oil,
– lanolin,
– teropenol,
– tri-ethanomine,
– propylene glycol and
– perfume.
23
• Functions of cleansing cream:
– Used to
• Remove facial makeup,
• Surface grime,
• Oil,
• Dead cells &
• Crusts
24
Properties of cleansing cream:
The cleansing cream should possess the following:
 Be stable
 Good appearance
 Soften on application on skin
 Spread easily
 Not have oily or greasy feel during application
 No residue should remain after evaporation of water
 a thin emollient film should remain on the skin after its use
25
Types of cleansing cream:
• Three types:
– Liquefied cleansing cream
– Emulsified cream of o/w type
– Emulsified creams of w/o type
26
• Liquefied cleansing cream:
– Simple mixtures of mineral oils or synthetic fatty materials, with HC
waxes, paraffin wax etc..
– In modern formulations cetyl or stearyl alcohols are also included
– Example:
• Isopropyl myristate ---- 25%
• Liquid paraffin ---- 25%
• White soft paraffin ---- 30%
• Paraffin wax ---- 20%
– Procedure:
• Melt all ingredients in their decreasing order of m.p
• Cool with const. stirring until the product is little over solidifying point.
• Pour into final container & packed
27
• Emulsified cream of o/w type:
– Bees wax – borax cream is an example of this type
• Example:
– Bees wax ---- 12%
– Liquid paraffin ---- 53%
– Bentonite ---- 0.7%
– Borax ---- 0.7%
– Water ---- 33.2%
– IPA ---- 0.4%
• Procedure:
– Triturate bentonite, IPA & part of liquid paraffin
– Heat it with beeswax at 750C.
– Dissolve borax in water at 700C
– Add into oily phase with stirring
– Continue stirring till the tempt. Comes down to 40 – 450C.
– Pour into final container & labeled it.
28
• Emulsified creams of w/o type:
– These are stabilized by using non-ionic emulsifier
• Example:
– Liquid paraffin ---- 50%
– Paraffin wax ---- 5%
– Bentone ---- 0.7%
– Water ---- 43.9%
– IPA ---- 0.4%
• Procedure:
– Triturate bentonite, IPA & part of liquid paraffin to disperse bentone
– Gel is formed & heat it with paraffin wax & liquid paraffin to 750C
– Heat the water to 700C & mixed slowly with oil phase with stirring
– Continue the stirring till desired consistency is obtained
– Pour the emulsified into final container & packed
29
• Storage:
– Stored in a well closed container at a temperature not
exceeds 250C.
– Stored in a cool place.
• Labeling:
– Label should indicate following:
• Name of active ingredient(s)
• Quantity (in mg. , gm., or %)
• Net content
• Batch
• Mfg. Date
• Exp. Date
• Manufactured by
• Marketed by
• Storage condition
• Direction
• Special instruction if any
30
• Evaluation parameters:
– Consistency (viscosity)
– Skin irritation test
– Net content in the container
– Test for microbial growth
– Rancidity
– Color & physical appearance test
31
• Marketed Products:
– Clarins
– Dove
– Rutina
– Gala,
– Lakme,
– Anne french
– Max-factor

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Cold cream, vanishing cream and cleansing cream

  • 1. COLD CREAMS Dr. Prashant L. Pingale Associate Professor, Dept. of Pharmaceutics, GES’s Sir Dr. M. S. Gosavi College of Pharm. Edu. and Research, Nashik-422005
  • 2. An emulsion of water and certain fats, usually including beeswax and various scent agents, designed to smooth skin and remove makeup. The name derives from the cool feeling that the cream leaves on the skin. 2
  • 3. • Cold cream produces cooling effect becoz slow evaporation of water present in the emulsion. • In olden days the cold cream was prepared from animal fats & vegetable oils but – Vegetable oils: rancid so replaced by mineral oils which gives more stable product. 3
  • 4. • Mechanism of action on skin: – o/w type of emulsion but after application on skin, sufficient water evaporates to permit phase inversion to w/o type. 4
  • 5. Formulation: • Formula 1 • Bees wax ---- 5% • Liquid paraffin ---- 45% • White soft paraffin ----10% • Hard paraffin ---- 7% • Borax ---- 0.2% • Water ---- 32.8% • Perfume ---- q.s • Formula 2 • Bees wax ---- 16% • Liquid paraffin ---- 50% • Borax ---- 0.8% • Water ---- 33.2% • Perfume ---- q.s 5
  • 6. General procedure – Weigh all ingredients in reqd qty. – Melt the wax and other ings. in their decreasing order of m.p. on water bath – Dissolve borax in water at 70-750C – Add both phase together i.e. oil & water – Add reqd qty of preservative & perfume – Transfer the cream to container while hot. 6
  • 7. • Storage: – Stored in a well closed container at a temperature not exceeds 250C. – Stored in a cool place. • Labeling: – Label should indicate following: • Name of active ingredient(s) • Quantity (in mg. , gm., or %) • Net content • Batch • Mfg. Date • Exp. Date • Manufactured by • Marketed by • Storage condition • Direction • Special instruction if any 7
  • 8. Evaluation parameters – Consistency (viscosity) – Skin irritation test – Net content in the container – Test for microbial growth – Rancidity – Color & physical appearance test 8
  • 9. Marketed Products • Pond’s cold cream • Ayur herbal cold cream • Emani cold cream • Aloe vera cold cream 9
  • 11. • Creams spread easily & seem to disappear rapidly when rubbed on skin are termed as vanishing creams. • These are an o/w type of emulsions which when applied to the skin leave an almost invisible layer on it so called vanishing creams. • These creams can be quickly washed off with water due to the presence of o/w emulsifiers DEFINITION 11
  • 12. • These creams are prepared by emulsification of stearic acid & water by means of alkalies like NaOH, KOH, borax, triethanolamine etc.. • Synonym: greaseless cream • An oil-in-water emulsion containing potassium, ammonium, or sodium stearate with water and holding in emulsified form more or less free stearic acid; General Discussion 12
  • 13. • It also contains a hygroscopic ingredient such as glycerol, and a small amount of a fatty ingredient; • It leaves a protective, invisible film of stearic acid on the skin. • The main ingredients are: • Stearic acid which gives pearly white shining appearance to the cream, after application gives thin white film of free stearic acid. 13
  • 14. • Stearic acid (550C)-- protective • High quality is used bcoz to provide an oil phase, which melts above body tempt. • Provides non-greasy film • Produce very attractive appearance • KOH or NaOH :- to neutralize free fatty acid • NaOH makes a harder cream than KOH. • Triethanolamine is also used instead which makes preparation easy & viable nature. • borax is used to make white creams but product has tendency to grain (small piece) FORMULATION 14
  • 15. • Glycerin 10% of total • Used to maintain consistency • Enhance spreading ability • Water in large qty. so preservative required to prevent microbial growth • Methyl parahydroxy benzoate (0.12%) • Propyl parahydroxy benzoate (0.12%) in combination • Perfume • Sandalwood, lavender oil, linalol, rose, geraniol etc… 15
  • 16. • Stearic acid ---- 20% • Cetyl alcohol ---- 0.5% • Triethanolamine ---- 1.2% • NaOH ---- 0.36% • Glycerin ---- 8% • Water ---- 69.94% • Preservative ---- q.s. • Perfume ---- q.s. • Procedure: – Weigh all ingredients & heat or melt Ist part ingredients (from 1to 3) in a container – Heat or melt IInd part ingredients in a beaker – Add IInd part mixture to Ist part with continuous stirring – Cool with continuous stirring – Add perfume when tempt. is about 350 C. – Mill it (uniform mixing) Formula 16
  • 17. • Storage: – Stored in a well closed container at a temperature not exceeds 250C. – Stored in a cool place. • Labeling: – Label should indicate following: • Name of active ingredient(s) • Quantity (in mg. , gm., or %) • Net content • Batch • Mfg. Date • Exp. Date • Manufactured by • Marketed by • Storage condition • Direction • Special instruction if any 17
  • 18. • Evaluation of vanishing creams: – Rheology or viscosity – Skin sensitivity or patch test – Biological testing (antiseptic, hormones, vitamins etc..) – Net content 18
  • 19. • Marketed Products: – Lakme, – Max-factor, – Ponds, – Charmis. 19
  • 21. 21 DEFINITION  These are cosmetic preparations used to be applied on skin for removing the facial makeup.  They are also used to improve the healthy & good appearance to the skin  These are same as cold creams but contains detergent for cleaning action.  They contain other ingredients which helps to soften, lubricate or protect the skin.
  • 22. 22 • Cleansing Cream is used to clean the face of makeup and the dust before going to bed. • The layers of makeup, dust and sweat remain as a coat on the face and do not allow the skin breathe which may result in wrinkles an dullness on skin. • Cleansing Creams is made with a mixture of: – stearic acid, – mineral oil, – lanolin, – teropenol, – tri-ethanomine, – propylene glycol and – perfume.
  • 23. 23 • Functions of cleansing cream: – Used to • Remove facial makeup, • Surface grime, • Oil, • Dead cells & • Crusts
  • 24. 24 Properties of cleansing cream: The cleansing cream should possess the following:  Be stable  Good appearance  Soften on application on skin  Spread easily  Not have oily or greasy feel during application  No residue should remain after evaporation of water  a thin emollient film should remain on the skin after its use
  • 25. 25 Types of cleansing cream: • Three types: – Liquefied cleansing cream – Emulsified cream of o/w type – Emulsified creams of w/o type
  • 26. 26 • Liquefied cleansing cream: – Simple mixtures of mineral oils or synthetic fatty materials, with HC waxes, paraffin wax etc.. – In modern formulations cetyl or stearyl alcohols are also included – Example: • Isopropyl myristate ---- 25% • Liquid paraffin ---- 25% • White soft paraffin ---- 30% • Paraffin wax ---- 20% – Procedure: • Melt all ingredients in their decreasing order of m.p • Cool with const. stirring until the product is little over solidifying point. • Pour into final container & packed
  • 27. 27 • Emulsified cream of o/w type: – Bees wax – borax cream is an example of this type • Example: – Bees wax ---- 12% – Liquid paraffin ---- 53% – Bentonite ---- 0.7% – Borax ---- 0.7% – Water ---- 33.2% – IPA ---- 0.4% • Procedure: – Triturate bentonite, IPA & part of liquid paraffin – Heat it with beeswax at 750C. – Dissolve borax in water at 700C – Add into oily phase with stirring – Continue stirring till the tempt. Comes down to 40 – 450C. – Pour into final container & labeled it.
  • 28. 28 • Emulsified creams of w/o type: – These are stabilized by using non-ionic emulsifier • Example: – Liquid paraffin ---- 50% – Paraffin wax ---- 5% – Bentone ---- 0.7% – Water ---- 43.9% – IPA ---- 0.4% • Procedure: – Triturate bentonite, IPA & part of liquid paraffin to disperse bentone – Gel is formed & heat it with paraffin wax & liquid paraffin to 750C – Heat the water to 700C & mixed slowly with oil phase with stirring – Continue the stirring till desired consistency is obtained – Pour the emulsified into final container & packed
  • 29. 29 • Storage: – Stored in a well closed container at a temperature not exceeds 250C. – Stored in a cool place. • Labeling: – Label should indicate following: • Name of active ingredient(s) • Quantity (in mg. , gm., or %) • Net content • Batch • Mfg. Date • Exp. Date • Manufactured by • Marketed by • Storage condition • Direction • Special instruction if any
  • 30. 30 • Evaluation parameters: – Consistency (viscosity) – Skin irritation test – Net content in the container – Test for microbial growth – Rancidity – Color & physical appearance test
  • 31. 31 • Marketed Products: – Clarins – Dove – Rutina – Gala, – Lakme, – Anne french – Max-factor