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Cold Chain Solutions Cold Shipper Trials
Objective To observe & record existing Packing standards. To confirm efficacy (Temperature Retention).  To assess duration index of complete shipper. To assess weak links in cold chain. No changes made - to packaging material. to placement of chill packs. to methodology or processes followed.
The Protocol Select one each of thermocol shippers. Load shippers with sample contents. Package per existing practices. Add gel packs (maintain 2 to 8 °C). Store shippers for 96 hours in ambient. Record temperature using data loggers. Open Shippers (13th Sept) and analyse records. Equipment Used ThermocolBoxes (2 Nos) Chill Pack Freezer  (1 Nos) Data-Loggers (6pcs, 3  per box) Chill Packs (15 nos, 300ml each) Spectral temperature sensor. Shipper & contents Temperature Recorders Cold Packs – thermal charge
Trial Methodology 2 1 3 Package Prepared Shipper Sealed  Cold Packs’ Temperature Checked 6 4 5 Cold Packs placed, Loggers Placed
Trial Records Standard Thermocol Shipper loaded: Two layers of product, total ___units – mass ___gms. Bottom with 24 units, top layer with 16 units. Cardboard spacer sheet used. Cold Packs used measured initial at -10 to -17.5 °C. Cold Packs were wrapped in plastic sheet. Cold Packs placed on one side of shipped cargo box. Total 10 cold packs were placed (for 2 to 8 °C use). Temperature loggers placed next to product units. One between product, one between outer wall and product. Loggers programmed to measure every 5 mins. Shipper taped and strapped. Shipper placed on top floor (with ambient at 33.4 °C).
Two Boxes A Temp Datalogger B Cold Packs in Plastic Wrap Temp Datalogger B A Large Thermocol Box ,[object Object]
10 cold packs
2 Temp loggers (both inside)Small Thermocol Box ,[object Object]
5 cold packs
2 Temp loggers (1 in + 1 out),[object Object]
Result-Analysis [A] Box A – 10 cold packs, ambient 33.4°C, 40 units: Sensor 1: Internal temps between 20.8°C to 28.4°C. Product >25°C after 10-Sep, 1841 hrs (26.8hrs) Sensor 2: Internal temps between 17.3°C to 28.4°C. Product >25°C after 11-Sep, 1123 hrs (43.4hrs) No pull down to below 8 °C experienced. External ambient was between 26°C to 34°C. +1100 temperature samples (12 every hour) recorded. Conclusion: Box type & number of cold packs insufficient for intention. With pre-cooled product, results would improve. With harsher ambient, results would be worse.
Box A – Temp Graph Internal Product temperature logger
Result-Analysis [B] Box B – 5 cold packs, ambient <30°C, 1 ltr water: Sensor 1: Internal temps between 12.1°C to 28.7°C. Product >25°C after 11-Sep, 0718hrs (39.3hrs) Sensor 2: External temps between 25.7°C to 29.3°C. No pull down to below 8 °C experienced. +1100 temperature samples (12 every hour) recorded. Conclusion: Box type & number of cold packs insufficient. With pre-cooled product, results would improve. With harsher ambient, results would be worse.

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Pharma Packaging Trials

  • 1. Cold Chain Solutions Cold Shipper Trials
  • 2. Objective To observe & record existing Packing standards. To confirm efficacy (Temperature Retention). To assess duration index of complete shipper. To assess weak links in cold chain. No changes made - to packaging material. to placement of chill packs. to methodology or processes followed.
  • 3. The Protocol Select one each of thermocol shippers. Load shippers with sample contents. Package per existing practices. Add gel packs (maintain 2 to 8 °C). Store shippers for 96 hours in ambient. Record temperature using data loggers. Open Shippers (13th Sept) and analyse records. Equipment Used ThermocolBoxes (2 Nos) Chill Pack Freezer (1 Nos) Data-Loggers (6pcs, 3 per box) Chill Packs (15 nos, 300ml each) Spectral temperature sensor. Shipper & contents Temperature Recorders Cold Packs – thermal charge
  • 4. Trial Methodology 2 1 3 Package Prepared Shipper Sealed Cold Packs’ Temperature Checked 6 4 5 Cold Packs placed, Loggers Placed
  • 5. Trial Records Standard Thermocol Shipper loaded: Two layers of product, total ___units – mass ___gms. Bottom with 24 units, top layer with 16 units. Cardboard spacer sheet used. Cold Packs used measured initial at -10 to -17.5 °C. Cold Packs were wrapped in plastic sheet. Cold Packs placed on one side of shipped cargo box. Total 10 cold packs were placed (for 2 to 8 °C use). Temperature loggers placed next to product units. One between product, one between outer wall and product. Loggers programmed to measure every 5 mins. Shipper taped and strapped. Shipper placed on top floor (with ambient at 33.4 °C).
  • 6.
  • 8.
  • 10.
  • 11. Result-Analysis [A] Box A – 10 cold packs, ambient 33.4°C, 40 units: Sensor 1: Internal temps between 20.8°C to 28.4°C. Product >25°C after 10-Sep, 1841 hrs (26.8hrs) Sensor 2: Internal temps between 17.3°C to 28.4°C. Product >25°C after 11-Sep, 1123 hrs (43.4hrs) No pull down to below 8 °C experienced. External ambient was between 26°C to 34°C. +1100 temperature samples (12 every hour) recorded. Conclusion: Box type & number of cold packs insufficient for intention. With pre-cooled product, results would improve. With harsher ambient, results would be worse.
  • 12. Box A – Temp Graph Internal Product temperature logger
  • 13. Result-Analysis [B] Box B – 5 cold packs, ambient <30°C, 1 ltr water: Sensor 1: Internal temps between 12.1°C to 28.7°C. Product >25°C after 11-Sep, 0718hrs (39.3hrs) Sensor 2: External temps between 25.7°C to 29.3°C. No pull down to below 8 °C experienced. +1100 temperature samples (12 every hour) recorded. Conclusion: Box type & number of cold packs insufficient. With pre-cooled product, results would improve. With harsher ambient, results would be worse.
  • 14. Box B – Temp Graph
  • 15. Result Summary Regular validation of efficacy is required. Thermocol shipper specifications [insulation grade] suspect. Cold packs mass and numbers used insufficient. Ineffective placement of cold packs – new packaging method to be validated. Regular checks in hot oven and real time to be deployed. Pre-qualification of design and process required. Effective cold chain integrity is inconclusive.
  • 16. Improve your Cold chain Integrity