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ME 101: Materials Science and Technology
ME101: Materials Science and
Technology








Hardness is not necessarily an indication of
strength , although for some materials such as
steel, a harder steel is a stronger steel.
Measure of a material’s ability to resist surface
indentation or scratching
A difficult property to describe in terms of first
principles Þ value depends greatly on
method of testing.
Different testing methods Þ different scales and
values
ME101: Materials Science and
Technology






Brinell Hardness Test: 10mm diameter ball
with a load of 500, 1000 or 3000kg
Rockwell Hardness Test: A cone shape
indenter; the depth of penetration is measured.
Vickers Hardness Test: Pyramid shape indenter

ME101: Materials Science and
Technology
F

Brinell’s Hardness
ME101: Materials Science and
Technology
P from 500 - 3000 kg
D= 10 mm

D
d

BHN =( 2 P )

{

πD D −



ME101: Materials Science and
Technology

(

)

}

D 2 −d 2 


ME101: Materials Science and
Technology
1.
2.
3.

Press a 10mm (3/8") diameter ball into
material with a known amount of load.
Measure diameter of the indentation.
BHN =
Load
=
2L
Surface Area πD[D-(D2-d2)1/2]
1. L = Load placed on ball, usually 3000 kg , but 1500 kg, and

500 kg can also be used.

2. D = Diameter of steel ball ( = 10 mm)
3. d = diameter of dent, measured by looking thru a Brinell

microscope.

ME101: Materials Science and
Technology
Plastic

Mild steel

Elastic
H
Copper

H = Ae-BT

d/D(%E)
ME101: Materials Science and
Technology
Tensile Strength (MPa)

Tensile Strength = 3.4 BHN

Correlations between the
Brinell hardness number (BHN)
and tensile strength of carbon
steels.
ME101: Materials Science and
Technology

Hardness (HB)


Sample must be ten times thicker than the
indentation depth (sample usually should be at least
3/8" thick).



Test is most accurate if the indentation depth is 2.5 5.0 mm. Adjust load to achieve this.



Test is no good if BHN > 650

ME101: Materials Science and
Technology







Widely used and well
accepted
Large ball gives good
average reading with
a single test.
Accurate
Easy to learn and use







Destructive
Non-portable
High initial cost
($5,000)
Error due to operator
reading Brinell
Microscope (10%
max)

ME101: Materials Science and
Technology
ME101: Materials Science and
Technology
Machine measures depth of penetration and computes
hardness

ME101: Materials Science and
Technology




Select Scale - load and
indentor depending on
the scale
Press a point into
material





- Diamond Point (Brale)
- 1/16" ball
- 1/8" ball
- ¼” ball

ME101: Materials Science and
Technology
Load levels and indenter sizes for Rockwell hardness tests.
Symbol
Indenter
Normal Scales
RB, 1/16 ball*
RC, cone +
RA, cone
RD, cone
RE, 1/8 ball
RF, 1/16 ball
RG, 1/16 ball
Superficial Sales
R15N, cone+
R30N, cone
R45N, cone
R15T, 1/16 ball
R30T, 1/16 ball
R45T, 1/16 ball

Minor(Pre-)
Load, kg

Coefficients in
R = C1 – C2 t

Major(Total)
Load, kg

C1

C2mm-1

10
10
10
10
10
10
10

100
150
60
100
100
60
150

130
100
100
100
130
130
130

500
500
500
500
500
500
500

3
3
3
3
3
3

15
30
45
15
30
45

100
100
100
100
100
100

1000
1000
1000
1000
1000
1000

ME101: Materials Science and
Technology





Sample must be ten times thicker than the
indentation depth (sample usually should
be at least 1/8" thick).
Need 3 tests (minimum) to avoid
inaccuracies due to impurities, hard spots.
Test is most accurate if the Rockwell
Hardness is between 0 and 100. Adjust
scale to achieve this.
For Steel:
If HRa > 60, use HRc scale
If HRa < 60, use HRb scale

ME101: Materials Science and
Technology







Widely used and well
accepted
Little operator
subjectivity
Accurate
Fast





Destructive
Non-Portable
Initial cost ($5,000)

ME101: Materials Science and
Technology
1)

If -20 < HRc < 40
BHN = 1,420,000
(100 – HRc)2

2)

3)

If 40 < HRc < 100
If 35 < HRb < 100

BHN = 25,000__
(100 - HRc)
BHN = 7,300____
(130 - HRb)

ME101: Materials Science and
Technology
DPH/VHN/VPH/VH = 2PSin(θ/2)/L2

P

P: applied load in kg, 5-120 kg
L: average diagonal length, mm
(typically from a few µm to 1 mm)

θ

θ: angle between opposite faces of
indenter; ≡ 136°
L

Range: 5 (extremely soft metals) 1500 (extremely hard materials)

1.854P
HV =
2
L

A
Vickers Hardness = F/A =
3σ

ME101: Materials Science and
Technology








Continuous hardness from soft (5 DPH) to hard
materials (1500 DPH)
DPH independent on load value unlike BHN
Careful surface preparation required
Slow due to careful measurement
Small indentation compared to BHN
Pin cushion and Barrel indentations possible

ME101: Materials Science and
Technology
ME101: Materials Science and
Technology







Knoop hardness Test: Pyramid shape
indenter
Scleroscope: rebound height
Durometer: The resistance to penetration
(elastic deformation)
Relationship between Hardness and
Strength

TS = K h ( HB )

where K h = 500 in lb/in

ME101: Materials Science and
Technology

= 3.45 in MPa

2


Micro Hardness Tests


Major : Minor = 7 : 1



P :
Ap :
L :
C :





14.2P
HK =
2
L

Applied load = 25 gf- 300 gf
Unrecovered Proj. area of indentations, mm 2
Length of long diagonal, mm
A constant supplied by the manufacturer
(C=0.07028 for 172° 30' between
long edges and 130° 0' between short edges)


ME101: Materials Science and
Technology






Accurate
Useful for elongated and
anisotropic constituents.
Requires load to be
normal to surface plane
parallel surfaces.
Can be done on
mounted specimens






Slow
Sensitive to surface
condition
Subject to error in
diagonal measurement

ME101: Materials Science and
Technology
Microhardness variation in a 9Cr-1 Mo steel weldment as a function of position.
Note the structural changes and the corresponding changes in hardness as the
fusion line is traversed.
ME101: Materials Science and
Technology
ME101: Materials Science and
Technology






The Shore (Durometer) test provides an empirical hardness
value that doesn't correlate to other properties or
fundamental characteristics.
Shore Hardness, using either the Shore A or Shore D scale,
is the preferred method for rubbers/elastomers and is also
commonly used for 'softer' plastics such as polyolefins,
fluoropolymers, and vinyls. The Shore A scale is used for
'softer' rubbers while the Shore D scale is used for 'harder'
ones.
Because of the resilience of rubbers and plastics, the
hardness reading may change over time - so the
indentation time is sometimes reported along with the
hardness number. The ASTM test number is ASTM D2240
number
while the analogous ISO test method is ISO 868.
ME101: Materials Science and
Technology
ME101: Materials Science and
Technology
ME101: Materials Science and
Technology
ME101: Materials Science and
Technology
The Brinell’s Hardness Test of an alloy steel was measured
to be 355. What is the diameter of the indentation if a load
of 2000 kg was used. Also compute the tensile strength of the
material.
D= 10 mm
d = 2.65 mm
Tensile Strength = 1207 MPa

ME101: Materials Science and
Technology
The Brinell hardness of an alloy steel is 355. Compute the
diameter of the indentation if a load of 200 kg was used and estimate the
Solution
corresponding tensile strength of the material.

BHN = ( 2 P )

{

π D D −



(

)

D2 − d 2 



}

Substituting the values from the problem statement yields :

355 = ( 2 ) ( 2000 )

{

10π 10 −



(

)

10 2 − d 2 



}

which after some algebra gives d = 2.65mm

ME101: Materials Science and
Technology
5mm
ME101: Materials Science and
Technology


Indentation Hardness used for steel




It is indicative of ultimate tensile strength




as opposed to scratch or rebound hardness
Atoms move out of the way to create indentation

Two main types: Brinell and Rockwell







A spherical indenter (1 cm diameter) is shot
with 29 kN force at the target
Frequently the indenter is steel, but for harder
materials it is replaced with a tungsten carbide
sphere
The diameter of the indentation is recorded
The indentation diameter can be correlated
with the volume of the indentation.
B N=
H

(

2
P

)

π − ( −d )
DD D
2

2





ASTM and ISO use the HB value. It can be
HBS (Hardness, Brinell, Steel) or the HBW
(Hardness, Brinell, Tungsten)
HBW = 0.102 BHN
Sometimes written as HBW 10/3000
(Tungsten, 10 mm diameter, 3,000 kg force)
Material
Softwood (e.g., pine)
Hardwood
Aluminum
Copper
Mild steel
18-8 (304) stainless steel annealed
Glass
Hardened tool steel
Rhenium diboride

Hardness
1.6 HBS 10/100
2.6–7.0 HBS 1.6 10/100
15 HB
35 HB
120 HB
200 HB
1550 HB
1500–1900 HB
4600 HB
Scale Code

Load

Indenter

Use

120° diamond cone

Tungsten
carbide

A

HRA 60 kgf

B

Al, brass, and
HRB 100 kgf 1/16 in diameter steel sphere soft steels

C
D

HRC 150 kgf 120° diamond cone
HRD 100 kgf 120° diamond cone

E

HRE 100 kgf 1/8 in diameter steel sphere

F

HRF 60 kgf

G

HRG 150 kgf 1/16 in diameter steel sphere

1/16 in diameter steel sphere

Harder steels
HBW
10/3000

HRA 60KG

HRB 100KG

HRC 150KG

Tensile
Strength
(Approx)

638

80.8

-

59.2

329,000

578

79.1

-

56

297,000

461

74.9

-

48.5

235,000

375

70.6

-

40.4

188,000

311

66.9

-

33.1

155,000

241

61.8

100

22.8

118,000

207

-

94.6

16

100,000

179

-

89

-

87,000

149

-

80.8

-

73,000

111

-

65.7

-

56,000

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Presentation on Hardness Testing

  • 1. ME 101: Materials Science and Technology
  • 2. ME101: Materials Science and Technology
  • 3.     Hardness is not necessarily an indication of strength , although for some materials such as steel, a harder steel is a stronger steel. Measure of a material’s ability to resist surface indentation or scratching A difficult property to describe in terms of first principles Þ value depends greatly on method of testing. Different testing methods Þ different scales and values ME101: Materials Science and Technology
  • 4.    Brinell Hardness Test: 10mm diameter ball with a load of 500, 1000 or 3000kg Rockwell Hardness Test: A cone shape indenter; the depth of penetration is measured. Vickers Hardness Test: Pyramid shape indenter ME101: Materials Science and Technology
  • 6. P from 500 - 3000 kg D= 10 mm D d BHN =( 2 P ) { πD D −   ME101: Materials Science and Technology ( ) } D 2 −d 2   
  • 7. ME101: Materials Science and Technology
  • 8. 1. 2. 3. Press a 10mm (3/8") diameter ball into material with a known amount of load. Measure diameter of the indentation. BHN = Load = 2L Surface Area πD[D-(D2-d2)1/2] 1. L = Load placed on ball, usually 3000 kg , but 1500 kg, and 500 kg can also be used. 2. D = Diameter of steel ball ( = 10 mm) 3. d = diameter of dent, measured by looking thru a Brinell microscope. ME101: Materials Science and Technology
  • 9. Plastic Mild steel Elastic H Copper H = Ae-BT d/D(%E) ME101: Materials Science and Technology
  • 10. Tensile Strength (MPa) Tensile Strength = 3.4 BHN Correlations between the Brinell hardness number (BHN) and tensile strength of carbon steels. ME101: Materials Science and Technology Hardness (HB)
  • 11.  Sample must be ten times thicker than the indentation depth (sample usually should be at least 3/8" thick).  Test is most accurate if the indentation depth is 2.5 5.0 mm. Adjust load to achieve this.  Test is no good if BHN > 650 ME101: Materials Science and Technology
  • 12.     Widely used and well accepted Large ball gives good average reading with a single test. Accurate Easy to learn and use     Destructive Non-portable High initial cost ($5,000) Error due to operator reading Brinell Microscope (10% max) ME101: Materials Science and Technology
  • 13. ME101: Materials Science and Technology
  • 14. Machine measures depth of penetration and computes hardness ME101: Materials Science and Technology
  • 15.   Select Scale - load and indentor depending on the scale Press a point into material     - Diamond Point (Brale) - 1/16" ball - 1/8" ball - ¼” ball ME101: Materials Science and Technology
  • 16. Load levels and indenter sizes for Rockwell hardness tests. Symbol Indenter Normal Scales RB, 1/16 ball* RC, cone + RA, cone RD, cone RE, 1/8 ball RF, 1/16 ball RG, 1/16 ball Superficial Sales R15N, cone+ R30N, cone R45N, cone R15T, 1/16 ball R30T, 1/16 ball R45T, 1/16 ball Minor(Pre-) Load, kg Coefficients in R = C1 – C2 t Major(Total) Load, kg C1 C2mm-1 10 10 10 10 10 10 10 100 150 60 100 100 60 150 130 100 100 100 130 130 130 500 500 500 500 500 500 500 3 3 3 3 3 3 15 30 45 15 30 45 100 100 100 100 100 100 1000 1000 1000 1000 1000 1000 ME101: Materials Science and Technology
  • 17.    Sample must be ten times thicker than the indentation depth (sample usually should be at least 1/8" thick). Need 3 tests (minimum) to avoid inaccuracies due to impurities, hard spots. Test is most accurate if the Rockwell Hardness is between 0 and 100. Adjust scale to achieve this. For Steel: If HRa > 60, use HRc scale If HRa < 60, use HRb scale ME101: Materials Science and Technology
  • 18.     Widely used and well accepted Little operator subjectivity Accurate Fast    Destructive Non-Portable Initial cost ($5,000) ME101: Materials Science and Technology
  • 19. 1) If -20 < HRc < 40 BHN = 1,420,000 (100 – HRc)2 2) 3) If 40 < HRc < 100 If 35 < HRb < 100 BHN = 25,000__ (100 - HRc) BHN = 7,300____ (130 - HRb) ME101: Materials Science and Technology
  • 20. DPH/VHN/VPH/VH = 2PSin(θ/2)/L2 P P: applied load in kg, 5-120 kg L: average diagonal length, mm (typically from a few µm to 1 mm) θ θ: angle between opposite faces of indenter; ≡ 136° L Range: 5 (extremely soft metals) 1500 (extremely hard materials) 1.854P HV = 2 L A Vickers Hardness = F/A = 3σ ME101: Materials Science and Technology
  • 21.       Continuous hardness from soft (5 DPH) to hard materials (1500 DPH) DPH independent on load value unlike BHN Careful surface preparation required Slow due to careful measurement Small indentation compared to BHN Pin cushion and Barrel indentations possible ME101: Materials Science and Technology
  • 22. ME101: Materials Science and Technology
  • 23.     Knoop hardness Test: Pyramid shape indenter Scleroscope: rebound height Durometer: The resistance to penetration (elastic deformation) Relationship between Hardness and Strength TS = K h ( HB ) where K h = 500 in lb/in ME101: Materials Science and Technology = 3.45 in MPa 2
  • 24.  Micro Hardness Tests  Major : Minor = 7 : 1  P : Ap : L : C :    14.2P HK = 2 L Applied load = 25 gf- 300 gf Unrecovered Proj. area of indentations, mm 2 Length of long diagonal, mm A constant supplied by the manufacturer (C=0.07028 for 172° 30' between long edges and 130° 0' between short edges)  ME101: Materials Science and Technology
  • 25.     Accurate Useful for elongated and anisotropic constituents. Requires load to be normal to surface plane parallel surfaces. Can be done on mounted specimens    Slow Sensitive to surface condition Subject to error in diagonal measurement ME101: Materials Science and Technology
  • 26. Microhardness variation in a 9Cr-1 Mo steel weldment as a function of position. Note the structural changes and the corresponding changes in hardness as the fusion line is traversed. ME101: Materials Science and Technology
  • 27. ME101: Materials Science and Technology
  • 28.    The Shore (Durometer) test provides an empirical hardness value that doesn't correlate to other properties or fundamental characteristics. Shore Hardness, using either the Shore A or Shore D scale, is the preferred method for rubbers/elastomers and is also commonly used for 'softer' plastics such as polyolefins, fluoropolymers, and vinyls. The Shore A scale is used for 'softer' rubbers while the Shore D scale is used for 'harder' ones. Because of the resilience of rubbers and plastics, the hardness reading may change over time - so the indentation time is sometimes reported along with the hardness number. The ASTM test number is ASTM D2240 number while the analogous ISO test method is ISO 868. ME101: Materials Science and Technology
  • 29. ME101: Materials Science and Technology
  • 30. ME101: Materials Science and Technology
  • 31. ME101: Materials Science and Technology
  • 32. The Brinell’s Hardness Test of an alloy steel was measured to be 355. What is the diameter of the indentation if a load of 2000 kg was used. Also compute the tensile strength of the material. D= 10 mm d = 2.65 mm Tensile Strength = 1207 MPa ME101: Materials Science and Technology
  • 33. The Brinell hardness of an alloy steel is 355. Compute the diameter of the indentation if a load of 200 kg was used and estimate the Solution corresponding tensile strength of the material. BHN = ( 2 P ) { π D D −   ( ) D2 − d 2    } Substituting the values from the problem statement yields : 355 = ( 2 ) ( 2000 ) { 10π 10 −   ( ) 10 2 − d 2    } which after some algebra gives d = 2.65mm ME101: Materials Science and Technology
  • 35.  Indentation Hardness used for steel   It is indicative of ultimate tensile strength   as opposed to scratch or rebound hardness Atoms move out of the way to create indentation Two main types: Brinell and Rockwell
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  • 37.     A spherical indenter (1 cm diameter) is shot with 29 kN force at the target Frequently the indenter is steel, but for harder materials it is replaced with a tungsten carbide sphere The diameter of the indentation is recorded The indentation diameter can be correlated with the volume of the indentation.
  • 38. B N= H ( 2 P ) π − ( −d ) DD D 2 2
  • 39.    ASTM and ISO use the HB value. It can be HBS (Hardness, Brinell, Steel) or the HBW (Hardness, Brinell, Tungsten) HBW = 0.102 BHN Sometimes written as HBW 10/3000 (Tungsten, 10 mm diameter, 3,000 kg force)
  • 40. Material Softwood (e.g., pine) Hardwood Aluminum Copper Mild steel 18-8 (304) stainless steel annealed Glass Hardened tool steel Rhenium diboride Hardness 1.6 HBS 10/100 2.6–7.0 HBS 1.6 10/100 15 HB 35 HB 120 HB 200 HB 1550 HB 1500–1900 HB 4600 HB
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  • 43. Scale Code Load Indenter Use 120° diamond cone Tungsten carbide A HRA 60 kgf B Al, brass, and HRB 100 kgf 1/16 in diameter steel sphere soft steels C D HRC 150 kgf 120° diamond cone HRD 100 kgf 120° diamond cone E HRE 100 kgf 1/8 in diameter steel sphere F HRF 60 kgf G HRG 150 kgf 1/16 in diameter steel sphere 1/16 in diameter steel sphere Harder steels
  • 44. HBW 10/3000 HRA 60KG HRB 100KG HRC 150KG Tensile Strength (Approx) 638 80.8 - 59.2 329,000 578 79.1 - 56 297,000 461 74.9 - 48.5 235,000 375 70.6 - 40.4 188,000 311 66.9 - 33.1 155,000 241 61.8 100 22.8 118,000 207 - 94.6 16 100,000 179 - 89 - 87,000 149 - 80.8 - 73,000 111 - 65.7 - 56,000