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Basic Radiation Safety Office of Environmental Health and Safety
5425 Woodward Ste 300 Detroit, MI 48202 Office: 313.577.1200 Fax:313.993.4079 www.oehs.wayne.edu
What is OEHS? The Office of Environmental Health and Safety serves to protect the health and safety of the students, faculty and staff of Wayne State University.  The Office operates as the University’s extension of the regulatory agencies that monitor use of hazardous materials and ensures that a safe and compliant workplace is maintained.  Please call our office any time you have a question or concern about the acquisition, use, storage or disposal of any hazardous substance at the University.
Health Physics / Radiation Safety The Health Physics staff are specialists in radiological health and safety, and are ready to provide assistance so you may work safely with radioactive material.  Please contact us if you have questions or concerns about radioactive materials on campus. Lance Franklin Radiation Safety Officer 577-1200 [email_address] Wendy Barrows Health Physics Specialist 577-0019  ac5502@wayne.edu Michael Huberts Health Physics Specialist 577-9505 [email_address] Ryan Boyd Health Physics Assistant 577-9518 [email_address]
Hazardous Waste ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
Nuclear Regulatory Commission –  Type A  Broad Scope Radioactive Materials license.  Allows researchers to use a wide range of radioisotopes , but requires strict compliance with Federal Laws.  NRC regulates reactor produced radioactive  materials   ie P-32, H-3, C-14, etc Michigan Department of Community Health –  Radiation Generating Machine license.  Allows researchers to use x-ray producing machines.  State of Michigan regulates  machines   ie XRD, EM, Diagnotsic X-Ray, etc Regulatory Control and Responsibility Governmental
Regulatory Control and Responsibility ,[object Object],[object Object],University
Regulatory Control and Responsibility Laboratory ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],The Approval Holder / PI ! You are!
Radiation Worker Rights View the university’s licenses, inspection reports, and copies of the regulations You may contact the   US Nuclear Regulatory Commission without fear of retaliation by your Approval Holder or anyone at Wayne State University. Receive adequate training and have • • questions answered satisfactorily •
Worker Training Basic Radiation Safety Training must be taken annually First time - in class Annually -  online Radiation Generating Machine Training – Online Special Training by request Lab-specific training is provided by your PI   • • •
Basic Radiation Safety Part 1 Radiation Theory
What is Radiation? ,[object Object],Ionizing Non-ionizing
The Importance of Energy Ionizing radiation has enough energy to remove electrons from atoms E (hv) > E B Non-ionizing radiation may only excite electrons into excited states E (hv) < E B
Sources of Radiation X-Ray  -   Electron transition from one level to a lower level, or from slowing of a moving electron (bremsstrahlung) Gamma  - Radioactive decay emission originating from the nucleus.  Alpha  – Helium nucleus from decay from massive atom Beta –  particle emitted during n  p or p  n decay Neutron  – neutral particle emitted during fission
Gamma and X-ray Radiation   Tissue ,[object Object],[object Object],[object Object],[object Object],[object Object]
Alpha Particle Radiation (a) Tissue ,[object Object],[object Object],[object Object],[object Object],Alphas are internally highly toxic
Beta Particle Radiation  (  Tissue ,[object Object],[object Object],[object Object],[object Object],Lead shielding causes Bremsstrahlung x-ray production
Neutron (n) ,[object Object],[object Object],[object Object],[object Object],Tissue
Radioactive Decay   ,[object Object],[object Object],[object Object],Radioisotopes are chemically indistinguishable from stable isotopes of the same element.
Half-Life ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],A(t)=A o e  – λ t  ½ = e  – λ t 1/2   ln(2)/ λ  = t ½   After n half-lives  A = A o 2- n Half –Life Calculation Example: You order 200 uCi of I-125 in January.  In June of the same year you decide that you want to use the material.  Will you have enough to use? T 1/2  = 60 days t = 6 months ~ 180 days =  3 T 1/2  A = A o  2 -n   =  A = 200 * 2 -3   = 25 uCi A = Ao *1/2 *1/2 *1/2  =  25 uCi Or λ  = ln(2)/ T 1/2   A = Ao e  –  λ t   = 25 uCi
Units of Activity Historical unit  defined as the activity of 1 gram of Radium-226.  Still used today due to more convenient values  Bequerel (Bq)   Curie (Ci) SI unit defined as 1 disintegration per second (dps).  More useful unit, but very unwieldy values. Designated as official unit . 1 Ci  =  3.7 x 10 10  Bq (dps) i.e. 250 microCuries (uCi)  =  925 MegaBequerels (MBq)
Units of Exposure Roentgen (R)   -  The amount of ionization produced in a volume of air by gamma or x-rays Corresponds air at standard temperature and pressure (273K and 760 mm Hg).  The usefulness of the Roentgen in the practice of radiation safety is limited, because it is only defined for x-rays and gamma radiation in air.
Units of Dose and Dose Equivalent SI: Gray (Gy) = J/kg rad = 100 erg/g SI: Sievert (Sv) rem   Dose (D)  is a measure of the absorbed energy per unit mass of material 1 Gy = 100 rad Dose Equivalent (H)  is the product of the absorbed dose and the biological efficacy in tissue 1 Sv = 100 rem
Quality Factor / W R ,[object Object],[object Object],[object Object],[object Object],[object Object],H = D x Q i.e.  1 Gy dose delivered with neutron radiation; what is dose equivalent? D x Q = 1 Gy x 10 = H =  10 Sv  =  1000 rem
Acute High-Dose Effects ,[object Object],[object Object],[object Object],It is nearly impossible for you to receive these acute doses at Wayne State
Chronic Low-Level Exposure ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
Background Radiation Background in Michigan is 360 mRem/year
Basic Radiation Safety Part 2 Radiation Protection
A s  L ow  A s  R easonably  A chievable ,[object Object],A L A R A •  Time •  Distance •  Shielding •  Contamination Control
Protective Measures   Time ,[object Object],[object Object],i.e.  A worker performing an experiment in a 300 mrem/hour gamma radiation field completes the work in 20 minutes.  What is the dose received by the worker? 300 mrem/hr  x  0.33 hr = 100 mrem
Protective Measures   Distance Intensity of radiation is inversely proportional to the square of the distance – inverse square law I    1/d 2 I 2  = I 1  x (d 1 /d 2 ) 2 i.e.   A worker is 1 meter from a 200 mrem point source.  What is the dose at 2 m?  3m? I 1  x (d 1 /d 2 ) 2  = 200 x (1/2) 2  = I 2  = 50 mrem 200 x (1/3) 2  = I 2  =  22.2 mrem I 2 *d 2 2  = I 1 *d 1 2
Protective Measures   Shielding Alpha  – no shielding Beta  – none or Plexiglas, No Pb X, Gamma – Lead, thick or thin Neutron  – Concrete, parafin
Protective Measures  Contamination Control ,[object Object],[object Object],[object Object],[object Object],[object Object],Protective equipment, like lab coats, gloves and goggles, provide a contamination barrier between you and the radioactive material
Occupational worker limits ,[object Object],[object Object],[object Object],[object Object],[object Object],The NRC utilizes the Linear, No-Threshold Theory, which assumes all exposure to radiation above natural background will have some detrimental health effect . Risk for radiation workers is equivalent to risk associated with any other hazardous material worker
Pregnant Workers   Declared Decision is up to woman May be temporarily assigned non-radiation  duties until end of gestation May un-declare her pregnancy at any time Limits: Employer may  not  limit occupational exposure below worker • • • Undeclared 500 mRem over gestation <50 mRem per month • •
Personal Dosimeters  TLD ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],Dosimetry records (Form 5) are available for review at the Office of Environmental Health and Safety.
Dosimetry for users of beta emitting isotopes ,[object Object],[object Object],[object Object],Examples:  32 P,  36 Cl,  90 Sr
Dosimetry for users of beta emitting isotopes ,[object Object],[object Object],Examples:  35 S,  14 C,  3 H
Dosimetry for users of gamma emitting isotopes ,[object Object],[object Object],[object Object],Example:  125 I
Dosimetry for users of gamma emitting isotopes ,[object Object],[object Object],Examples:  111 In,  51 Cr,  22 Na
Proper use of Dosimeters ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
Internal Hazards ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],Use fume hood Be cautious with sharps
Ingestion WSU Food Policy ,[object Object],[object Object],[object Object],[object Object],Floor to ceiling enclosures must separate food areas from hazardous materials areas
Bioassays ,[object Object],[object Object],[object Object],[object Object],[object Object],Because many radioisotopes are only internal radiation hazards, external dosimetry is not an effective method for monitoring occupational exposure.  For this reason, you may be asked to provide a urine sample for bioassay. Individuals working with unbound  125 I, must come between six and seventy-two hours after each radioiodonation for a thyroid bioassay.  • •
Basic Radiation Safety Part 3   Radiation Detection Equipment
Radiation Detection ,[object Object],You cannot detect ionizing radiation •  Survey Meters •  Liquid Scintillation Counters
Survey Meters Ludlum Model 3 Geiger Counter with pancake and LEG probes Required in most labs ( 32 P  125 I) Detects contamination quickly Indicates the effectiveness of shielding Must be calibrated annually Geiger-Mueller (GM) Crystal Scintillation (LEG) Ion Chamber (QT Pie) • • • • Not for  3 H or  35 S
Pancake and End Window Probes Ion chamber - Volume of gas with biased electrodes.  Radiation creates ion which induces “current” to show up as an event Survey Meters
Gamma and X ray Survey Probes (LEG) Low energy gamma 1x1 gamma probe Low energy gamma (LEG) scintillation detectors -  Sodium iodide (NaI) crystal encased in a metal cylinder, mounted on a photomultiplier tube.  These are more sensitive and will have a higher background than other probes Recommended for detection of  125 I. http:// www.uos.harvard.edu/ehs/radsafety/sur_how.shtml Survey Meters
Ion Chamber Survey Meter ,[object Object],[object Object],[object Object],[object Object],[object Object],Survey Meters
Using a Meter: BCBS ,[object Object],[object Object],[object Object],Survey Meters
Reading Your Meter ,[object Object],[object Object],Meters are calibrated by Health Physics staff annually.  If your meter is out of date call us at 577-1200 Survey Meters
Other Settings ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],scale setting change Survey Meters
Performing a Survey ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],Survey Meters
Liquid Scintillation Counters (LSC) ,[object Object],[object Object],[object Object],[object Object],[object Object]
Radiation Safety Video ,[object Object]
Basic Radiation Safety Part 4 Laboratory Application
Performing a Wipe Test Wipe Test  – Wipe surface with filter paper, fold wipe-side in, and insert into scintillation vial.  Add ~10mL of scintillation cocktail and count the sample in the LSC.  Record all results including nil results
Contamination Surveys ,[object Object],[object Object],A survey is an evaluation of dose potential in a work area based on all aspects of radiation use, not just monitoring for radiation contamination Surveying = Monitoring
[object Object],[object Object],Contamination Surveys A blank copy of this form is available as Appendix M in the Radiation Safety Manual and Lab Guide
Use Log and After-Use Surveys ,[object Object],[object Object],[object Object],[object Object],[object Object],H-3 0906B 09/02/06 500 09/08/06 Thymidine 09/02/06 J. Schmoe 500 22 09/04/06 J. Schmoe 250  250 21  30  22  28 H  F1  fl 09/04/06  J. Schmoe 250  0 26  20  39  40 H  F1  fl  A blank copy of this form is available as Appendix O in the Radiation Safety Manual and Lab Guide
Survey Record If a lab has radioactive material, a monthly survey must be completed in at least the storage location Any survey location must be accompanied by a survey of the adjacent floor See form instructions 10/10/06 Science 123 Dr Franklin Schmoe, Joe Grad Asst X 500 uCi 2 mCi IIIIIIIIIII IIIIIIIIIII H-3 P-32 Ludlum 3 / 123 Science Beckman 8600 / 123 Science 25 44 52 106 107 115 12 99 249 100 B1 fl F2 H B1 fl F2 H H-3 contamination in Hood – cleaned, repeat survey performed 56 H Re-wipe Joe Schmoe 44 115 fl fl 55 110 fl fl A blank copy of this form is available as Appendix N in the Radiation Safety Manual and Lab Guide
Calculation of Activity CPM - BKG    NRC requires surveys to be written in units of DPM or uCi. CPM is a function of instrument efficiency Instrument efficiency   DPM     DPM = uCi  = 2.22 x 10 6  DPM/uCi CPM CPM CPM CPM
Contamination ,[object Object],[object Object],[object Object],[object Object]
Minor Incident ,[object Object],[object Object],[object Object],[object Object],[object Object]
[object Object],[object Object],[object Object],[object Object],[object Object],Minor Incident
Major Incident ,[object Object],[object Object],[object Object]
Major Incident ,[object Object],[object Object],[object Object],[object Object]
Emergency Procedures ,[object Object],[object Object],Radioactive material has been released, and one or more of the following has occurred: No University lab possesses enough radioactive material to cause immediate harm to a first responder
Radiation Lab Postings Warning Placard with radiation sticker – outside lab NRC-3 Form – visible in lab Radioactive materials sticker – on all storage, use and waste areas and containers ie Refrigerators, freezers, cabinets, sinks, benches, hoods, centrifuges, etc.  • • Three postings must be clearly visible in or at the entrance to your lab If you cannot locate any of these call OEHS immediately for a replacement at 577-1200 * •
Changing RAM Location Use/Storage ,[object Object],[object Object],[object Object],[object Object]
Labeling and Identifying ,[object Object],[object Object],[object Object],[object Object],Any radioactive material or waste must be labeled as such and identified.  ie radionuclide, lot number, assay date etc. If there is radiation above background in or on something, it  must  be labeled or decontaminated. It is not acceptable to label items known to be free of contamination with a radioactive warning
Moving Radioactive Material ,[object Object],[object Object],[object Object],[object Object],[object Object]
All radioactive material must be secured from tampering or removal by unauthorized persons. Material Security Lock the lab door in your absence Loss of material must be reported to the RSO immediately • •
Radioactive Waste ,[object Object],[object Object],[object Object],[object Object]
Radioactive Waste Tag ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
Radioactive Waste Pick-up ,[object Object],[object Object],[object Object],[object Object]
Mixed Waste ,[object Object],[object Object]
Radioactive Waste  Do’s ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]
Radioactive waste  Don’ts Do NOT mix potentially dangerous  chemicals Do NOT discard sharps into regular waste Do NOT dispose of liquid waste into solid waste boxes Do NOT dump liquid waste down the drains Do NOT overfill waste containers (>¾) Do NOT mix incompatible chemicals Do NOT mix isotopes Do NOT remove radioactive waste without OEHS approval • • • • • • • •
Basic Radiation Safety Exam Monday 1:00 ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]

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Basic Radiation Safety

  • 1. Basic Radiation Safety Office of Environmental Health and Safety
  • 2. 5425 Woodward Ste 300 Detroit, MI 48202 Office: 313.577.1200 Fax:313.993.4079 www.oehs.wayne.edu
  • 3. What is OEHS? The Office of Environmental Health and Safety serves to protect the health and safety of the students, faculty and staff of Wayne State University. The Office operates as the University’s extension of the regulatory agencies that monitor use of hazardous materials and ensures that a safe and compliant workplace is maintained. Please call our office any time you have a question or concern about the acquisition, use, storage or disposal of any hazardous substance at the University.
  • 4. Health Physics / Radiation Safety The Health Physics staff are specialists in radiological health and safety, and are ready to provide assistance so you may work safely with radioactive material. Please contact us if you have questions or concerns about radioactive materials on campus. Lance Franklin Radiation Safety Officer 577-1200 [email_address] Wendy Barrows Health Physics Specialist 577-0019 ac5502@wayne.edu Michael Huberts Health Physics Specialist 577-9505 [email_address] Ryan Boyd Health Physics Assistant 577-9518 [email_address]
  • 5.
  • 6. Nuclear Regulatory Commission – Type A Broad Scope Radioactive Materials license. Allows researchers to use a wide range of radioisotopes , but requires strict compliance with Federal Laws. NRC regulates reactor produced radioactive materials ie P-32, H-3, C-14, etc Michigan Department of Community Health – Radiation Generating Machine license. Allows researchers to use x-ray producing machines. State of Michigan regulates machines ie XRD, EM, Diagnotsic X-Ray, etc Regulatory Control and Responsibility Governmental
  • 7.
  • 8.
  • 9. Radiation Worker Rights View the university’s licenses, inspection reports, and copies of the regulations You may contact the US Nuclear Regulatory Commission without fear of retaliation by your Approval Holder or anyone at Wayne State University. Receive adequate training and have • • questions answered satisfactorily •
  • 10. Worker Training Basic Radiation Safety Training must be taken annually First time - in class Annually - online Radiation Generating Machine Training – Online Special Training by request Lab-specific training is provided by your PI • • •
  • 11. Basic Radiation Safety Part 1 Radiation Theory
  • 12.
  • 13. The Importance of Energy Ionizing radiation has enough energy to remove electrons from atoms E (hv) > E B Non-ionizing radiation may only excite electrons into excited states E (hv) < E B
  • 14. Sources of Radiation X-Ray - Electron transition from one level to a lower level, or from slowing of a moving electron (bremsstrahlung) Gamma - Radioactive decay emission originating from the nucleus. Alpha – Helium nucleus from decay from massive atom Beta – particle emitted during n p or p n decay Neutron – neutral particle emitted during fission
  • 15.
  • 16.
  • 17.
  • 18.
  • 19.
  • 20.
  • 21. Units of Activity Historical unit defined as the activity of 1 gram of Radium-226. Still used today due to more convenient values Bequerel (Bq) Curie (Ci) SI unit defined as 1 disintegration per second (dps). More useful unit, but very unwieldy values. Designated as official unit . 1 Ci = 3.7 x 10 10 Bq (dps) i.e. 250 microCuries (uCi) = 925 MegaBequerels (MBq)
  • 22. Units of Exposure Roentgen (R) - The amount of ionization produced in a volume of air by gamma or x-rays Corresponds air at standard temperature and pressure (273K and 760 mm Hg). The usefulness of the Roentgen in the practice of radiation safety is limited, because it is only defined for x-rays and gamma radiation in air.
  • 23. Units of Dose and Dose Equivalent SI: Gray (Gy) = J/kg rad = 100 erg/g SI: Sievert (Sv) rem Dose (D) is a measure of the absorbed energy per unit mass of material 1 Gy = 100 rad Dose Equivalent (H) is the product of the absorbed dose and the biological efficacy in tissue 1 Sv = 100 rem
  • 24.
  • 25.
  • 26.
  • 27. Background Radiation Background in Michigan is 360 mRem/year
  • 28. Basic Radiation Safety Part 2 Radiation Protection
  • 29.
  • 30.
  • 31. Protective Measures Distance Intensity of radiation is inversely proportional to the square of the distance – inverse square law I  1/d 2 I 2 = I 1 x (d 1 /d 2 ) 2 i.e. A worker is 1 meter from a 200 mrem point source. What is the dose at 2 m? 3m? I 1 x (d 1 /d 2 ) 2 = 200 x (1/2) 2 = I 2 = 50 mrem 200 x (1/3) 2 = I 2 = 22.2 mrem I 2 *d 2 2 = I 1 *d 1 2
  • 32. Protective Measures Shielding Alpha – no shielding Beta – none or Plexiglas, No Pb X, Gamma – Lead, thick or thin Neutron – Concrete, parafin
  • 33.
  • 34.
  • 35. Pregnant Workers Declared Decision is up to woman May be temporarily assigned non-radiation duties until end of gestation May un-declare her pregnancy at any time Limits: Employer may not limit occupational exposure below worker • • • Undeclared 500 mRem over gestation <50 mRem per month • •
  • 36.
  • 37.
  • 38.
  • 39.
  • 40.
  • 41.
  • 42.
  • 43.
  • 44.
  • 45. Basic Radiation Safety Part 3 Radiation Detection Equipment
  • 46.
  • 47. Survey Meters Ludlum Model 3 Geiger Counter with pancake and LEG probes Required in most labs ( 32 P 125 I) Detects contamination quickly Indicates the effectiveness of shielding Must be calibrated annually Geiger-Mueller (GM) Crystal Scintillation (LEG) Ion Chamber (QT Pie) • • • • Not for 3 H or 35 S
  • 48. Pancake and End Window Probes Ion chamber - Volume of gas with biased electrodes. Radiation creates ion which induces “current” to show up as an event Survey Meters
  • 49. Gamma and X ray Survey Probes (LEG) Low energy gamma 1x1 gamma probe Low energy gamma (LEG) scintillation detectors - Sodium iodide (NaI) crystal encased in a metal cylinder, mounted on a photomultiplier tube. These are more sensitive and will have a higher background than other probes Recommended for detection of 125 I. http:// www.uos.harvard.edu/ehs/radsafety/sur_how.shtml Survey Meters
  • 50.
  • 51.
  • 52.
  • 53.
  • 54.
  • 55.
  • 56.
  • 57. Basic Radiation Safety Part 4 Laboratory Application
  • 58. Performing a Wipe Test Wipe Test – Wipe surface with filter paper, fold wipe-side in, and insert into scintillation vial. Add ~10mL of scintillation cocktail and count the sample in the LSC. Record all results including nil results
  • 59.
  • 60.
  • 61.
  • 62. Survey Record If a lab has radioactive material, a monthly survey must be completed in at least the storage location Any survey location must be accompanied by a survey of the adjacent floor See form instructions 10/10/06 Science 123 Dr Franklin Schmoe, Joe Grad Asst X 500 uCi 2 mCi IIIIIIIIIII IIIIIIIIIII H-3 P-32 Ludlum 3 / 123 Science Beckman 8600 / 123 Science 25 44 52 106 107 115 12 99 249 100 B1 fl F2 H B1 fl F2 H H-3 contamination in Hood – cleaned, repeat survey performed 56 H Re-wipe Joe Schmoe 44 115 fl fl 55 110 fl fl A blank copy of this form is available as Appendix N in the Radiation Safety Manual and Lab Guide
  • 63. Calculation of Activity CPM - BKG NRC requires surveys to be written in units of DPM or uCi. CPM is a function of instrument efficiency Instrument efficiency DPM DPM = uCi = 2.22 x 10 6 DPM/uCi CPM CPM CPM CPM
  • 64.
  • 65.
  • 66.
  • 67.
  • 68.
  • 69.
  • 70. Radiation Lab Postings Warning Placard with radiation sticker – outside lab NRC-3 Form – visible in lab Radioactive materials sticker – on all storage, use and waste areas and containers ie Refrigerators, freezers, cabinets, sinks, benches, hoods, centrifuges, etc. • • Three postings must be clearly visible in or at the entrance to your lab If you cannot locate any of these call OEHS immediately for a replacement at 577-1200 * •
  • 71.
  • 72.
  • 73.
  • 74. All radioactive material must be secured from tampering or removal by unauthorized persons. Material Security Lock the lab door in your absence Loss of material must be reported to the RSO immediately • •
  • 75.
  • 76.
  • 77.
  • 78.
  • 79.
  • 80. Radioactive waste Don’ts Do NOT mix potentially dangerous chemicals Do NOT discard sharps into regular waste Do NOT dispose of liquid waste into solid waste boxes Do NOT dump liquid waste down the drains Do NOT overfill waste containers (>¾) Do NOT mix incompatible chemicals Do NOT mix isotopes Do NOT remove radioactive waste without OEHS approval • • • • • • • •
  • 81.