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GENERAL DUCTILE IRON MANUFACTURING PROCESS



        Process                                  Process Description                              What to look for



Purpose
Purpose of this document is to provide general information of foundry practices normally being followed
by Iron casting manufacturers globally.




                                                Prepared By: A T Ansari
GENERAL DUCTILE IRON MANUFACTURING PROCESS



       Process                              Process Description           What to look for


Typical process flow for casting manufacturing




                                            Prepared By: A T Ansari
GENERAL DUCTILE IRON MANUFACTURING PROCESS



      Process                                   Process Description                                What to look for

                         Various raw materials are being used in foundry processes to form
                         end result cast, our focus will be on major ones as listed below.
                         a. Pig iron                                                          Storage of Raw materials,
Raw material receipt &   b. Steel Scrap                                                       Identification and
 Receipt inspection:     c. CRCA scrap                                                        traceability, receipt
                         d. Ferro alloys                                                      inspection facilities
                         e. Green Sand
                         f. Resin coated sand


                                                                                              Method of metallic pattern
                         Pattern and core box can be made by using various materials,
                                                                                              manufacturing, Life of
                         such as
Pattern and core box                                                                          toolings made from
                         a. Metallic
       making                                                                                 wooden & chemical
                         b. Wooden
                                                                                              compound. System of
                         c. Chemical compounds e.g. Araldite
                                                                                              tooling management.


                         What is core? ==> Core is a component made of molding
                         material, used to create desired cavity / intricate shapes in        Where are the core
                         casting. Core can be also made up by using various materials &       prints?
                         methods, major processes as listed below.


                         a. By use of metallic core box and resin coated sand – Tooling is Core box temperature,
                         heated, as soon as resin coated sand comes in contact of heat,    HTS / LOI of resin coated
                         sand grains form a bounding in desired shape.                     sand


                         b. By CO2 Process – Uses proportionate mixture of raw silica
                             y                       p p
                         sand and sodium silicate, after ramming/shooting the mixture into
                                                                                           Ratio of Sodium silicate,
                         the core box CO2 is passed thru, here CO2 acts as catalyst and
                                                                                           vents and passing of CO2
                         sand bounded to form a core. Wooden tooling can be used in this
    Core making
                         process.


                         c. By Cold box process – Uses proportionate mixture of raw
                         silica sand, part 1 (resin) and part 2 (hardener), Shoots this  Ratios of resin and
                         mixture into core box and then Amine gas is passed thru, here   hardener, type of Amine.
                         Amine gas acts as catalyst to form hardened and strengthen core


                         d. By No Bake process – Uses proportionate mixture of raw silica
                         sand, part 1 and part 2 (These part 1 and part 2 are not same as
                                                                                              Ratio of part 1 and part 2,
                         used in Cold box process, chemical composition is different),
                                                                                              air set time
                         Shoots this mixture into core box. This process is time based, after
                         some time core gets rock solid and can be ejected from core box.




                                               Prepared By: A T Ansari
GENERAL DUCTILE IRON MANUFACTURING PROCESS



       Process                                  Process Description                                 What to look for

                         What is Mold? ==> A mold or mould is a hollowed-out block, a
                         framework or shape used to make an object of complementary             Sand to metal ratio
                         shape from a liquid metal.

                         a. All the above mentioned processes in core making can be             As applicable as per
                         utilized for molding also.                                             above.

       Molding
                         b. Green Sand Molding – This is most commonly used molding
                         process, the term "green sand" is known principally because of the
                                                                                            Moisture content, Green
                         moisture content within the sand. The sand undergoes a "mulling"
                                                                                            compression strength
                         process in which various clay and chemical additives that act as
                                                                                            (GCS),
                         binders are blended with the sand, which results in a compound
                         which is suitable for the sand molding process.


                         a. By using Cupola + Induction furnace – In this method melting is
                                                                                                Melting rate of cupola,
                         done in cupola and then metal transferred to electric induction
                                                                                                holding furnace capacity,
                         furnace, where liquid metal can be hold at required temperature
                                                                                                operating controls,
                         and necessary chemistry can be adjusted. This method is called
                                                                                                support facilities
                         as “Duplex Melting”.
        Melting

                         b. By using Electric induction furnace – In this method melting is     Frequency type, capacity,
                         done in induction furnace it self and ready material tapped for        operating controls,
                         pouring if CI or given for Mg treatment if SGCI.                       support facilities


                         a. High sulphur generally occurs in metal melted in acidic cupolas,
                         which if not lowered, necessitates the use of increased amount of Sulphur content prior to
                         spheroidizing alloy. Desulphurization can be done by commonly       desulphurization
                         used methods, s ch as
                          sed methods such as…

                         i. Injection of calcium carbide into the melt – The fine calcium
                         carbide is injected through a refractory tube, using dry nitrogen   Ratio of Calcium Carbide
                         gas as the carrying agent. The calcium sulfide formed floats to the and Nitrogen gas
                         surface of the melt as readily removable dross.

   Desulphurization
                         ii. Soda ash additions are also used to reduce sulphur levels.         Ratio of Soda ash

                         iii. Lime is also used for desulphurization, alone or in conjunction
                                                                                                Ratio of Lime.
                         with other materials.
                         iv. Shaking ladle – A recent innovation, uses lime. Shaking the
                                                                                                Ratio of lime and ladle
                         ladle increases contact of lime and metal, resulting in sulphur
                                                                                                shaking time
                         levels reduced.

                         b. Desulphurization generally not required when “Electric              Sulphur levels of metal
                         induction furnace” used for melting.                                   from induction furnace

Holding and Chemistry a. Superheat the metal taken from cupola.                                 Holding temperature, time
adjustment – Induction b. Adjust the chemistry required to achieve metallurgical and            taken for chemistry
       furnace         physical properties.                                                     adjustment, deslagging




                                                Prepared By: A T Ansari
GENERAL DUCTILE IRON MANUFACTURING PROCESS



       Process                                 Process Description                                  What to look for
                        Why magnesium treatment: Ductile iron, also known as spheroidal
                        graphite (s.g.) iron or nodular iron, is made by treating liquid iron
                        of suitable composition with magnesium before casting. This
                        promotes the precipitation of graphite in the form of discrete
                        nodules instead of interconnected flakes. The nodular iron so         Amount of metal to be
                        formed has high ductility, allowing castings to be used in critical   treated in any type of
                        applications such as Crankshafts, steering knuckles, differential     treatment.
                        carriers, brake callipers, hubs, brackets, valves, water pipes, pipe
                        fittings and many others.

                        Types of Mg treatment as mentioned below…
                    i. Sandwich method
                    Sandwich ladle: the treatment alloy is contained in a recess in the
                                                                                        Ratio of nodulizer and
                    bottom of a rather tall ladle and covered with steel scrap. The
                                                                                        steel punching
                    method is suitable for use only with treatment alloys containing
Magnesium Treatment less than 10%
                    ii. Tundish cover method
                    Tundish cover: this is a development of the treatment ladle in
                                                                                        Diameter of tundish hole
                    which a specially designed cover for the ladle improves Mg
                    recovery and almost eliminates glare and fume
                        iii. Plunging method
                        Plunger: the alloy is plunged into the ladle using a refractory
                                                                                                Plunging system.
                        plunger bell usually combined with a ladle cover and fume
                        extraction
                        iv. Mechanical feeder.
                        Cored wire treatment: wire containing Mg, FeSi, Ca is fed               Diameter of wire and its
                        mechanically into liquid metal in a covered treatment ladle at a        chemical composition
                        special station
                        Treatment in the mould (Inmold): MgFeSi alloy is placed in a
                                                                                                size of inmold chamber,
                                                                                                               chamber
                        chamber moulded into the running system, the iron is continuously
                                                                                                amount of nodulizer
                        treated as it flows over the alloy
                        Why Inoculation - Although the magnesium treatment is
                        responsible for the development of spheroidal graphite, quality
                        ductile iron also requires use of inoculants. Inoculation or post-
                        inoculation refers to the practice of making addition to the melt
                        which will increase the number of spheroids formed during
                        solidification.
     Inoculation        The amount of inoculant needed is governed by several factors.
                        The following rules guide the use of inoculation:
                        Low carbon equivalent irons require greater amounts of inoculant.
                        Grey cast irons with less than 0.06% sulphur are difficult to
                        inoculate, specially formulated products may be required.
                        For a given iron, the thinner the section of casting, the greater the
                        inoculation required.




                                              Prepared By: A T Ansari
GENERAL DUCTILE IRON MANUFACTURING PROCESS



       Process                                  Process Description                                 What to look for
                         Electric melted irons require more inoculation than cupola melted
                         irons. Electric melting will also produce low sulphur contents. High
                         steel scrap charges will require more inoculation. Where
                         inoculated iron is held for more than a few minutes after
                         inoculation, there is a need of a higher level of treatment. It is
                         therefore difficult to give an accurate estimate of the amount of
                         inoculant which is required for every situation. In general,
                         inoculant additions of 0.1–0.5% by weight of metal will be
                         satisfactory for grey cast irons, higher additions are needed for
                         ductile (SG) irons. Care must be taken not to over-inoculate grey
                         irons, otherwise problems will arise with shrinkage porosity due to
                         too high a nucleation level. Many grades of inoculants contain
                         high Si content, so that by adding 0.5% of inoculant, the silicon
                         content of the iron will be raised by as much as 0.3%, this must be
                         allowed for by adjusting the Si analysis of the furnace metal.
                         The most widely used inoculation for ductile iron is ferrosilicon      Size and quantity of
                         alloys. The most widely used grade is 85 percent silicon.              inoculant
                         i. Ladle inoculation                                                   Inoculation in bottom of
      Inoculation        Conventional method where inoculant either kept in ladle before        ladle or during tapping,
                         tapping or put in the ladle during tapping the metal from furnace.     size and type of inoculant
                         ii. Stream inoculation
                         The inoculant used in late stream inoculators must have a number
                         of important features:
                         It must be a powerful inoculant.                                       System of stream
                         It must be finely divided to ensure free-flowing properties and        inoculation, size and type
                         rapid solution.                                                        of inoculation, start and
                         It must be very accurately graded, without superfine material          end time of stream,
                         which would blow away, or large particles which jam the gate           amount of inoculant
                         mechanism.
                         It must dissolve rapidly and cleanly to avoid the presence of
                         undissolved inoculant particles in the castings.
                      iii. Mold inoculation
                      There are several ways in which mould inoculation can be
                                                                                                Design for mold
                      performed: powdered inoculant can be placed in the pouring bush;
                                                                                                inoculation, size of mold
                      or it can be placed at the bottom of the sprue. A more reliable
                                                                                                inoculation
                      method is to use sachets or precast slugs of inoculant in the
                      pouring bush or in the running system
                      Pouring is activity to pour cleaned and inoculated liquid metal into      Pouring temperature,
                      mold with specific temperature range within specific time.                pouring time, deslagging
                      Natural cooling of casting for designed time is necessary to
 Pouring and cooling achieve required hardness, microstructure and physical
                      properties.
                                                                                                Cooling time
                      The cooling time not only allows the castings to solidify completely
                      but also reduces internal stresses within the casting caused by
                      differential cooling of sections of varying thickness.
                      The shakeout separates the castings from the sand. It may be a
                      vibrating grid or a rotating drum, the latter also having a cooling
                      function since water is sprayed onto the sand in the drum. The
                      shakeout is provided with copious air extraction, to prevent dust
                                                                                                System of shake out and
Shake out & Knock out from entering the foundry. This also removes some fines from the
                                                                                                knock out
                      sand and so plays an important part in the control of the sand
                      system.
                      In knock-off or knock out casting separation done from runners
                      and riser.




                                               Prepared By: A T Ansari
GENERAL DUCTILE IRON MANUFACTURING PROCESS



     Process                                 Process Description                             What to look for
                     Shot blasting comes under category of Abrasive Blasting, abrasive
                     material in this case is steel shots.

                     Abrasive blasting is the operation of cleaning or preparing a
                     surface by forcibly propelling a stream of abrasive material against
  Shot blasting                                                                           Cycle time
                     it. Usually explained as the use of a material against another
                     material to make it smoother, remove surface contaminants or to
                     roughen a surface. It is also the appropriate term for what is
                     known as glass bead blasting, sandblasting, sand carving,
                     sodablasting or shot blasting.

                     These are the common processes in any foundry. In these
Grinding, trimming   processes fins and burrs removed from casting with help of bench Tools for fettling.
                     grinders and portable grinders.

                     Primary Inspection
                     This is a type of visual inspection and carried out immediately
                     after knock out, in some special cases it is done after shot blasting
                     also as defect are more visible after shot blasting.
                     Secondary Inspection
                     This is combination of visual and dimensional inspection after all
                     grinding and fettling, when casting is ready for dispatch or
                     machining.

                     Physical testing
   Inspections
                     These are destructive tests, often for to saving the casting and
                     cost, these tests are done on test bars of same metal according to
                     applicable standards. Two main test which are generally
                     conducted are Tensile test and Impact test.

                     Non Destructive testing (NDT)
                     These are the tests carried out directly on the part without causing
                     any damage to casting or product. Major NDT techniques are
                     ultrasonic tests, Magnetic particle inspection and liquid penetrant
                     test.




                                           Prepared By: A T Ansari

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General Foundry Guidelines

  • 1. GENERAL DUCTILE IRON MANUFACTURING PROCESS Process Process Description What to look for Purpose Purpose of this document is to provide general information of foundry practices normally being followed by Iron casting manufacturers globally. Prepared By: A T Ansari
  • 2. GENERAL DUCTILE IRON MANUFACTURING PROCESS Process Process Description What to look for Typical process flow for casting manufacturing Prepared By: A T Ansari
  • 3. GENERAL DUCTILE IRON MANUFACTURING PROCESS Process Process Description What to look for Various raw materials are being used in foundry processes to form end result cast, our focus will be on major ones as listed below. a. Pig iron Storage of Raw materials, Raw material receipt & b. Steel Scrap Identification and Receipt inspection: c. CRCA scrap traceability, receipt d. Ferro alloys inspection facilities e. Green Sand f. Resin coated sand Method of metallic pattern Pattern and core box can be made by using various materials, manufacturing, Life of such as Pattern and core box toolings made from a. Metallic making wooden & chemical b. Wooden compound. System of c. Chemical compounds e.g. Araldite tooling management. What is core? ==> Core is a component made of molding material, used to create desired cavity / intricate shapes in Where are the core casting. Core can be also made up by using various materials & prints? methods, major processes as listed below. a. By use of metallic core box and resin coated sand – Tooling is Core box temperature, heated, as soon as resin coated sand comes in contact of heat, HTS / LOI of resin coated sand grains form a bounding in desired shape. sand b. By CO2 Process – Uses proportionate mixture of raw silica y p p sand and sodium silicate, after ramming/shooting the mixture into Ratio of Sodium silicate, the core box CO2 is passed thru, here CO2 acts as catalyst and vents and passing of CO2 sand bounded to form a core. Wooden tooling can be used in this Core making process. c. By Cold box process – Uses proportionate mixture of raw silica sand, part 1 (resin) and part 2 (hardener), Shoots this Ratios of resin and mixture into core box and then Amine gas is passed thru, here hardener, type of Amine. Amine gas acts as catalyst to form hardened and strengthen core d. By No Bake process – Uses proportionate mixture of raw silica sand, part 1 and part 2 (These part 1 and part 2 are not same as Ratio of part 1 and part 2, used in Cold box process, chemical composition is different), air set time Shoots this mixture into core box. This process is time based, after some time core gets rock solid and can be ejected from core box. Prepared By: A T Ansari
  • 4. GENERAL DUCTILE IRON MANUFACTURING PROCESS Process Process Description What to look for What is Mold? ==> A mold or mould is a hollowed-out block, a framework or shape used to make an object of complementary Sand to metal ratio shape from a liquid metal. a. All the above mentioned processes in core making can be As applicable as per utilized for molding also. above. Molding b. Green Sand Molding – This is most commonly used molding process, the term "green sand" is known principally because of the Moisture content, Green moisture content within the sand. The sand undergoes a "mulling" compression strength process in which various clay and chemical additives that act as (GCS), binders are blended with the sand, which results in a compound which is suitable for the sand molding process. a. By using Cupola + Induction furnace – In this method melting is Melting rate of cupola, done in cupola and then metal transferred to electric induction holding furnace capacity, furnace, where liquid metal can be hold at required temperature operating controls, and necessary chemistry can be adjusted. This method is called support facilities as “Duplex Melting”. Melting b. By using Electric induction furnace – In this method melting is Frequency type, capacity, done in induction furnace it self and ready material tapped for operating controls, pouring if CI or given for Mg treatment if SGCI. support facilities a. High sulphur generally occurs in metal melted in acidic cupolas, which if not lowered, necessitates the use of increased amount of Sulphur content prior to spheroidizing alloy. Desulphurization can be done by commonly desulphurization used methods, s ch as sed methods such as… i. Injection of calcium carbide into the melt – The fine calcium carbide is injected through a refractory tube, using dry nitrogen Ratio of Calcium Carbide gas as the carrying agent. The calcium sulfide formed floats to the and Nitrogen gas surface of the melt as readily removable dross. Desulphurization ii. Soda ash additions are also used to reduce sulphur levels. Ratio of Soda ash iii. Lime is also used for desulphurization, alone or in conjunction Ratio of Lime. with other materials. iv. Shaking ladle – A recent innovation, uses lime. Shaking the Ratio of lime and ladle ladle increases contact of lime and metal, resulting in sulphur shaking time levels reduced. b. Desulphurization generally not required when “Electric Sulphur levels of metal induction furnace” used for melting. from induction furnace Holding and Chemistry a. Superheat the metal taken from cupola. Holding temperature, time adjustment – Induction b. Adjust the chemistry required to achieve metallurgical and taken for chemistry furnace physical properties. adjustment, deslagging Prepared By: A T Ansari
  • 5. GENERAL DUCTILE IRON MANUFACTURING PROCESS Process Process Description What to look for Why magnesium treatment: Ductile iron, also known as spheroidal graphite (s.g.) iron or nodular iron, is made by treating liquid iron of suitable composition with magnesium before casting. This promotes the precipitation of graphite in the form of discrete nodules instead of interconnected flakes. The nodular iron so Amount of metal to be formed has high ductility, allowing castings to be used in critical treated in any type of applications such as Crankshafts, steering knuckles, differential treatment. carriers, brake callipers, hubs, brackets, valves, water pipes, pipe fittings and many others. Types of Mg treatment as mentioned below… i. Sandwich method Sandwich ladle: the treatment alloy is contained in a recess in the Ratio of nodulizer and bottom of a rather tall ladle and covered with steel scrap. The steel punching method is suitable for use only with treatment alloys containing Magnesium Treatment less than 10% ii. Tundish cover method Tundish cover: this is a development of the treatment ladle in Diameter of tundish hole which a specially designed cover for the ladle improves Mg recovery and almost eliminates glare and fume iii. Plunging method Plunger: the alloy is plunged into the ladle using a refractory Plunging system. plunger bell usually combined with a ladle cover and fume extraction iv. Mechanical feeder. Cored wire treatment: wire containing Mg, FeSi, Ca is fed Diameter of wire and its mechanically into liquid metal in a covered treatment ladle at a chemical composition special station Treatment in the mould (Inmold): MgFeSi alloy is placed in a size of inmold chamber, chamber chamber moulded into the running system, the iron is continuously amount of nodulizer treated as it flows over the alloy Why Inoculation - Although the magnesium treatment is responsible for the development of spheroidal graphite, quality ductile iron also requires use of inoculants. Inoculation or post- inoculation refers to the practice of making addition to the melt which will increase the number of spheroids formed during solidification. Inoculation The amount of inoculant needed is governed by several factors. The following rules guide the use of inoculation: Low carbon equivalent irons require greater amounts of inoculant. Grey cast irons with less than 0.06% sulphur are difficult to inoculate, specially formulated products may be required. For a given iron, the thinner the section of casting, the greater the inoculation required. Prepared By: A T Ansari
  • 6. GENERAL DUCTILE IRON MANUFACTURING PROCESS Process Process Description What to look for Electric melted irons require more inoculation than cupola melted irons. Electric melting will also produce low sulphur contents. High steel scrap charges will require more inoculation. Where inoculated iron is held for more than a few minutes after inoculation, there is a need of a higher level of treatment. It is therefore difficult to give an accurate estimate of the amount of inoculant which is required for every situation. In general, inoculant additions of 0.1–0.5% by weight of metal will be satisfactory for grey cast irons, higher additions are needed for ductile (SG) irons. Care must be taken not to over-inoculate grey irons, otherwise problems will arise with shrinkage porosity due to too high a nucleation level. Many grades of inoculants contain high Si content, so that by adding 0.5% of inoculant, the silicon content of the iron will be raised by as much as 0.3%, this must be allowed for by adjusting the Si analysis of the furnace metal. The most widely used inoculation for ductile iron is ferrosilicon Size and quantity of alloys. The most widely used grade is 85 percent silicon. inoculant i. Ladle inoculation Inoculation in bottom of Inoculation Conventional method where inoculant either kept in ladle before ladle or during tapping, tapping or put in the ladle during tapping the metal from furnace. size and type of inoculant ii. Stream inoculation The inoculant used in late stream inoculators must have a number of important features: It must be a powerful inoculant. System of stream It must be finely divided to ensure free-flowing properties and inoculation, size and type rapid solution. of inoculation, start and It must be very accurately graded, without superfine material end time of stream, which would blow away, or large particles which jam the gate amount of inoculant mechanism. It must dissolve rapidly and cleanly to avoid the presence of undissolved inoculant particles in the castings. iii. Mold inoculation There are several ways in which mould inoculation can be Design for mold performed: powdered inoculant can be placed in the pouring bush; inoculation, size of mold or it can be placed at the bottom of the sprue. A more reliable inoculation method is to use sachets or precast slugs of inoculant in the pouring bush or in the running system Pouring is activity to pour cleaned and inoculated liquid metal into Pouring temperature, mold with specific temperature range within specific time. pouring time, deslagging Natural cooling of casting for designed time is necessary to Pouring and cooling achieve required hardness, microstructure and physical properties. Cooling time The cooling time not only allows the castings to solidify completely but also reduces internal stresses within the casting caused by differential cooling of sections of varying thickness. The shakeout separates the castings from the sand. It may be a vibrating grid or a rotating drum, the latter also having a cooling function since water is sprayed onto the sand in the drum. The shakeout is provided with copious air extraction, to prevent dust System of shake out and Shake out & Knock out from entering the foundry. This also removes some fines from the knock out sand and so plays an important part in the control of the sand system. In knock-off or knock out casting separation done from runners and riser. Prepared By: A T Ansari
  • 7. GENERAL DUCTILE IRON MANUFACTURING PROCESS Process Process Description What to look for Shot blasting comes under category of Abrasive Blasting, abrasive material in this case is steel shots. Abrasive blasting is the operation of cleaning or preparing a surface by forcibly propelling a stream of abrasive material against Shot blasting Cycle time it. Usually explained as the use of a material against another material to make it smoother, remove surface contaminants or to roughen a surface. It is also the appropriate term for what is known as glass bead blasting, sandblasting, sand carving, sodablasting or shot blasting. These are the common processes in any foundry. In these Grinding, trimming processes fins and burrs removed from casting with help of bench Tools for fettling. grinders and portable grinders. Primary Inspection This is a type of visual inspection and carried out immediately after knock out, in some special cases it is done after shot blasting also as defect are more visible after shot blasting. Secondary Inspection This is combination of visual and dimensional inspection after all grinding and fettling, when casting is ready for dispatch or machining. Physical testing Inspections These are destructive tests, often for to saving the casting and cost, these tests are done on test bars of same metal according to applicable standards. Two main test which are generally conducted are Tensile test and Impact test. Non Destructive testing (NDT) These are the tests carried out directly on the part without causing any damage to casting or product. Major NDT techniques are ultrasonic tests, Magnetic particle inspection and liquid penetrant test. Prepared By: A T Ansari