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extraction2 2
1.
Liquid-Liquid Extraction techniques
2.
Use balance to weigh
solids
3.
TARE by pressing ->0/T<-
Test tube is supported in a beaker -> to subtract the weight of the glassware
4.
Add chemical to
glassware after removing it from the balance
5.
Record measurement
6.
Add organic solvent
7.
8.
Mix with pipette, aspirate
and expel
9.
Solid has dissolved in
organic solvent
10.
Add aqueous layer
11.
meniscus
12.
- Use pipette
to mix layers - Allow mixture to separate
13.
Layers are separated
14.
Label receiving test
tube
15.
Pipette Both test tubes
are held with the same hand transfer bottom layer transferred aqueous layer
16.
Precipitate solid from
aqueous layer
17.
solid formation
18.
Label receiving vessel
19.
ether layer compressed air
jet carefully turn on compressed air to get a gentle stream
20.
solid deposits on
the side of the test tube ether evaporates
21.
Clean up
22.
solids that are
insoluble in water (benzophenone) are rinsed with acetone into the flammable waste
23.
Discard used chemicals
in the appropriate waste collector
24.
Rinse all glassware
with hot water
25.
Place rinsed glassware
in proper basket
Notes de l'éditeur
slide n: wasn't there a slide showing that glassware was to be stored in the locker upside down on a piece of paper towel to allow it to drain?
label receiving vessel
soli deposits on the side of the tt, (benzophenone)
solids that are insoluble in water (benzophenone) are rinsed with acetone into the flammable waste
discard use chemicals in the appropriate waste collector
rinse all glassware with hot water
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