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Spectrolytic GmbH
Portable milk analysers
providing laboratory
accuracy
2
Milk analysis
3
• Milk analysis is becoming more important for efficiency and herd management reasons.
• Being able to measure, in real time, key parameters of the milk can be used to optimise
feeding, detect illnesses and improve overall performance.
• Milk adulteration is also a growing problem worldwide where previously good milk is
contaminated with additives.
• In 2008 a Chinese milk manufacturer was charged for adding Melamine which falsely elevates
the protein contents in infant powder milk, as a result 13,000 babies were taken ill for kidney
inflammation and bladder carcinoma.
• Spectrolytic provides a compact and accurate solution for real time milk analysis application
based on analysing the mid-infrared absorption spectrum of a milk sample.
Introduction
4
What is mid-infrared spectroscopy
• A broad band emitter shines light through a samples
• The molecules in the sample will absorb certain wavelength of the light whist others pass through the
sample
• The wavelength of the light that is absorbed by the sample can be linked to certain molecular
structures that unequivocally identifies the molecules.
• Typically light in the wavelength range from 2.000nm to 12.000nm (mid infrared wavelength region)
provides the highest absorption signal whiles still providing a unique molecular identifier
• Monitoring the changes in the absorption spectrum of a sample over time provides information about
the concentration of relevant molecules in the sample.
Sample
5001000150020002500300035004000
0
10
20
30
40
50
60
wavenumber (cm-1
)
transmission(%)
Broad band emitter Absorption spectrum
5
Transmission &ATR Spectrometer Principles
multi-element
IR-Emitter
ATR
LVF
Pyroelectric
linearray
oil
multi-element
IR-emitter
cuvette LVF pyroelectric line
sensor
-Light is emitted from broad band source
-Light penetrates cuvette with sample fluid/gas
-Certain wavelength get absorbed by sample
-Light is separated into its spectral components by
Linear Variable Filter (LVF)
-Signals (as function of wavelength) are detected with sensor
-Light is emitted from broad band source
-Light is coupled into an ATR crystal
-Sample fluid is placed on top of ATR crystal
-Light bounces in a controlled way through ATR crystal
and interacts with the sample on its surface
-Certain wavelength get absorbed by sample
-Light is separated into its spectral components by
Linear Variable Filter (LVF)
-Signals (as function of wavelength) are detected with sensor
6
Introduction
Milk samples Spectrometer Data Analysis Interpretation
0.5 1 1.5
0.5
1
1.5
measured YpredictedY
predicted vs. measured - Oil1 - TAN - MIR
Milk sample is
poured onto
the spectrometer
Spectrometer to
record a spectrum
Spectrometer
analyses data and
compares against
laboratory standard
Feedback about milk quality
within 2 minutes
Simple to use, accurate and quick
7
Product Portfolio
Transmission Spectrometer
Spectral range:
 LVF1: 5.5-11µm (1808-909cm-1)
 LVF2: 2.5-5µm (4000-2000cm-1)
Voltage supply:
12-33V / 3W
Communication interfaces:
Ethernet, CANopen, USB
Aditional ports:
16GPIOs, I²C, SPI, UART
Cuvette:
demountable, 15-250µm spacer
ATR Spectrometer
Spectral range:
 LVF1: 5.5-11µm (1808-909cm-1)
 LVF2: 2.5-5µm (4000-2000cm-1)
Voltage supply:
5V / 3W
Communication interfaces:
Ethernet, Bluetooth, USB
ATR:
 ZnSe, 9 reflections
 ZnS, 9 reflections
 Diamond, 9 reflections
Additions:
 Through flow plate
 Options for fixed installation
Lab in a box
Truly portable solution
for instant analysis.
Simplified software
called “Express mode”
Battery operated
No need for additional
wet chemistry
Homogeniser available
8
Milk analysis parameters
Standard error : 0.04
Standard error : 0.09
Standard Error: 0.3
Results Products used
Lactose
Protein
Total Solids
9
Milk adulteration
Standard error : 0.23g/kg
Standard error : 0.64g/kg
Urea contamination >20g/l
All contamination levels are
easily detectable
Results Products used
10
Quantitative milk analysis
Component Accuracy /RMSE %
Fat 0.40
Protein 0.09
Lactose 0.04
SNF 0.09
Total Solids 0.28
Urea 1.0g/kg
Melamime 0.23g/kg
Glucose 0.64g/kg
Note: Other parameters can also be detected. Please contact Spectrolytic for detailed discussions
11
• Spectrolytic’s portable milk analyser provides fast and accurate prediction.
• Data can be represented in a qualitative or quantitative format
• Express mode software user interface can be configured to be used by untrained
personnel.
• Portable milk homogeniser is available achieving 2um particle homogenisation
of raw milk
Summary
Spectrolytic GmbH
Portable milk analyser
for quick and accurate
analysis
Dr.-Ing. Benjamin Wiesent
CEO
info@spectrolytic.com

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Milk Analysis Spectrolytic

  • 1. Spectrolytic GmbH Portable milk analysers providing laboratory accuracy
  • 3. 3 • Milk analysis is becoming more important for efficiency and herd management reasons. • Being able to measure, in real time, key parameters of the milk can be used to optimise feeding, detect illnesses and improve overall performance. • Milk adulteration is also a growing problem worldwide where previously good milk is contaminated with additives. • In 2008 a Chinese milk manufacturer was charged for adding Melamine which falsely elevates the protein contents in infant powder milk, as a result 13,000 babies were taken ill for kidney inflammation and bladder carcinoma. • Spectrolytic provides a compact and accurate solution for real time milk analysis application based on analysing the mid-infrared absorption spectrum of a milk sample. Introduction
  • 4. 4 What is mid-infrared spectroscopy • A broad band emitter shines light through a samples • The molecules in the sample will absorb certain wavelength of the light whist others pass through the sample • The wavelength of the light that is absorbed by the sample can be linked to certain molecular structures that unequivocally identifies the molecules. • Typically light in the wavelength range from 2.000nm to 12.000nm (mid infrared wavelength region) provides the highest absorption signal whiles still providing a unique molecular identifier • Monitoring the changes in the absorption spectrum of a sample over time provides information about the concentration of relevant molecules in the sample. Sample 5001000150020002500300035004000 0 10 20 30 40 50 60 wavenumber (cm-1 ) transmission(%) Broad band emitter Absorption spectrum
  • 5. 5 Transmission &ATR Spectrometer Principles multi-element IR-Emitter ATR LVF Pyroelectric linearray oil multi-element IR-emitter cuvette LVF pyroelectric line sensor -Light is emitted from broad band source -Light penetrates cuvette with sample fluid/gas -Certain wavelength get absorbed by sample -Light is separated into its spectral components by Linear Variable Filter (LVF) -Signals (as function of wavelength) are detected with sensor -Light is emitted from broad band source -Light is coupled into an ATR crystal -Sample fluid is placed on top of ATR crystal -Light bounces in a controlled way through ATR crystal and interacts with the sample on its surface -Certain wavelength get absorbed by sample -Light is separated into its spectral components by Linear Variable Filter (LVF) -Signals (as function of wavelength) are detected with sensor
  • 6. 6 Introduction Milk samples Spectrometer Data Analysis Interpretation 0.5 1 1.5 0.5 1 1.5 measured YpredictedY predicted vs. measured - Oil1 - TAN - MIR Milk sample is poured onto the spectrometer Spectrometer to record a spectrum Spectrometer analyses data and compares against laboratory standard Feedback about milk quality within 2 minutes Simple to use, accurate and quick
  • 7. 7 Product Portfolio Transmission Spectrometer Spectral range:  LVF1: 5.5-11µm (1808-909cm-1)  LVF2: 2.5-5µm (4000-2000cm-1) Voltage supply: 12-33V / 3W Communication interfaces: Ethernet, CANopen, USB Aditional ports: 16GPIOs, I²C, SPI, UART Cuvette: demountable, 15-250µm spacer ATR Spectrometer Spectral range:  LVF1: 5.5-11µm (1808-909cm-1)  LVF2: 2.5-5µm (4000-2000cm-1) Voltage supply: 5V / 3W Communication interfaces: Ethernet, Bluetooth, USB ATR:  ZnSe, 9 reflections  ZnS, 9 reflections  Diamond, 9 reflections Additions:  Through flow plate  Options for fixed installation Lab in a box Truly portable solution for instant analysis. Simplified software called “Express mode” Battery operated No need for additional wet chemistry Homogeniser available
  • 8. 8 Milk analysis parameters Standard error : 0.04 Standard error : 0.09 Standard Error: 0.3 Results Products used Lactose Protein Total Solids
  • 9. 9 Milk adulteration Standard error : 0.23g/kg Standard error : 0.64g/kg Urea contamination >20g/l All contamination levels are easily detectable Results Products used
  • 10. 10 Quantitative milk analysis Component Accuracy /RMSE % Fat 0.40 Protein 0.09 Lactose 0.04 SNF 0.09 Total Solids 0.28 Urea 1.0g/kg Melamime 0.23g/kg Glucose 0.64g/kg Note: Other parameters can also be detected. Please contact Spectrolytic for detailed discussions
  • 11. 11 • Spectrolytic’s portable milk analyser provides fast and accurate prediction. • Data can be represented in a qualitative or quantitative format • Express mode software user interface can be configured to be used by untrained personnel. • Portable milk homogeniser is available achieving 2um particle homogenisation of raw milk Summary
  • 12. Spectrolytic GmbH Portable milk analyser for quick and accurate analysis Dr.-Ing. Benjamin Wiesent CEO info@spectrolytic.com