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Leiden Cryogenics B.V.
The Dilution Refrigerators
of
Leiden Cryogenics
SmB – 8 May 2014
Arlette de Waard
Leiden Cryogenics B.V.
Founder - Giorgio Frossati
Plastic heat exchanger.
T=5.5mK Grenoble, 1976
Silver heat exchanger.
T=2mK Grenoble 1978-1982
CRYO1: WORLD RECORD for the
lowest continuous temperature
(T=1.85 mK). Leiden, 1982-1998
Silver Sinter
Heat Exchangers
Plastic
dilution
refrigerators
All welded
dilution
refrigerators
Magnetic field
independent
dielectric
thermometers
Plastic
Pomeranchuk
Cells
Non-metal
pressure
transducer
PhD Grenoble: Ultra Low Temperature Research
World record lowest temperature for 25 years
Leiden Cryogenics B.V.
MiniGRAIL (my PhD)
Gravitational Radiation Antenna In Leiden
CuAl sphere – M=1400kg, Tmin=50mK
Leiden Cryogenics B.V.
The Company
Founded in 1992 by Giorgio Frossati. Professor at the Kamerlingh
Onnes Laboratory, Leiden University from 1980-2006.
Workshops:
Kenauweg - Assembling
- Fabrication prototypes
- Cryogenic tests
Ananasweg - Production hall
Number of employees 17
Physicist 4
Electronical engineer 1
Mechanical engineer 12
Most of the engineers were trained at the
Leiden Instrument Making School, founded by
Kamerlingh Onnes
Leiden Cryogenics B.V.
The Company
Founded in 1992 by Giorgio Frossati. Professor at the Kamerlingh
Onnes Laboratory, Leiden University from 1980-2006.
Workshops:
Kenauweg - Assembling
- Fabrication prototypes
- Cryogenic tests
Ananasweg - Production hall
Number of employees 17
Physicist 4
Electronical engineer 1
Mechanical engineer 12
Most of the engineers were trained at the
Leiden Instrument Making School, founded by
Kamerlingh Onnes
Leiden Cryogenics B.V.
Dilution
Refrigerators
Room temperature pumping system
3K plate
JT Heat
Exchanger
Still
Heat Exchangers
Mixing Chamber
50K plate
Pulse tube
Leiden Cryogenics B.V.
Still
Mixing
Chamber
Dilution
Refrigerators
3K plate
Heat
Exchangers
JT Heat
Exchanger
Room temperature
pumping system
3K plate
JT Heat
Exchanger
Still
Heat Exchangers
Mixing Chamber
50K plate
Pulse tube
Leiden Cryogenics B.V.
Still
Mixing
Chamber
Dilution Refrigerators; Operation principle
3K plate
Heat
Exchangers
JT Heat
Exchanger
gas flow
Leiden Cryogenics B.V.
Dilution Refrigerators
Still
Mixing
Chamber
3K plate
Heat
Exchangers
JT Heat
Exchanger
gas flow
vapor
< 1% 3He
> 90% 3He
100% 3He
6% 3He
Leiden Cryogenics B.V.
CF CS81 total system
Leiden Cryogenics B.V.
New pumping system – Maglev & GX1000
Leiden Cryogenics B.V.
New model (standard)
Leiden Cryogenics B.V.
Fast cool down with the LC Probe
50K
3K
Still (900mK)
50mK
Mc (10mK)
Tmin≤15mK
Advantages:
 Possibility of many wires
 Easy access to center of
magnet
 Fast cooling down to base
temperature (<5 hours)
 High cooling power, up to
300W @ 120 mK
Leiden Cryogenics B.V.
Cryogen-Free DR – Specials: CUORE
1000 kg
TeO2 crystals
Lead
shielding
LC CF Dilution
Refrigerator
CRYOGENIC UNDERGROUND OBSERVATORY FOR RARE EVENTS
Neutrinoless double-beta decay half-life of Majorana neutrinos
Cooling down 17 tons!!
Leiden Cryogenics B.V.
Cryogen-Free DR– Specials: CUORE
Tmin=4,5mK
Leiden Cryogenics B.V.
Our customers (>150 systems)
MIT/Harvard
Stanford
5
2
2
5
82
Leiden/Delft
UCSB
Maryland
Detroit Waterloo
6
Sydney
Melbourne
Leiden Cryogenics B.V.
Our compatitors
Short delivery time, small models,
expensive
Short delivery time, small models
UHV specialists Leiden Cryogenics B.V.
Large models, low vibration levels
Large cooling power, lowest temperature
Leiden Cryogenics B.V.
Our Future

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SmB Cafe - 8 May 2014 - Leiden Cryogenics

  • 1. Leiden Cryogenics B.V. The Dilution Refrigerators of Leiden Cryogenics SmB – 8 May 2014 Arlette de Waard
  • 2. Leiden Cryogenics B.V. Founder - Giorgio Frossati Plastic heat exchanger. T=5.5mK Grenoble, 1976 Silver heat exchanger. T=2mK Grenoble 1978-1982 CRYO1: WORLD RECORD for the lowest continuous temperature (T=1.85 mK). Leiden, 1982-1998 Silver Sinter Heat Exchangers Plastic dilution refrigerators All welded dilution refrigerators Magnetic field independent dielectric thermometers Plastic Pomeranchuk Cells Non-metal pressure transducer PhD Grenoble: Ultra Low Temperature Research World record lowest temperature for 25 years
  • 3. Leiden Cryogenics B.V. MiniGRAIL (my PhD) Gravitational Radiation Antenna In Leiden CuAl sphere – M=1400kg, Tmin=50mK
  • 4. Leiden Cryogenics B.V. The Company Founded in 1992 by Giorgio Frossati. Professor at the Kamerlingh Onnes Laboratory, Leiden University from 1980-2006. Workshops: Kenauweg - Assembling - Fabrication prototypes - Cryogenic tests Ananasweg - Production hall Number of employees 17 Physicist 4 Electronical engineer 1 Mechanical engineer 12 Most of the engineers were trained at the Leiden Instrument Making School, founded by Kamerlingh Onnes
  • 5. Leiden Cryogenics B.V. The Company Founded in 1992 by Giorgio Frossati. Professor at the Kamerlingh Onnes Laboratory, Leiden University from 1980-2006. Workshops: Kenauweg - Assembling - Fabrication prototypes - Cryogenic tests Ananasweg - Production hall Number of employees 17 Physicist 4 Electronical engineer 1 Mechanical engineer 12 Most of the engineers were trained at the Leiden Instrument Making School, founded by Kamerlingh Onnes
  • 6. Leiden Cryogenics B.V. Dilution Refrigerators Room temperature pumping system 3K plate JT Heat Exchanger Still Heat Exchangers Mixing Chamber 50K plate Pulse tube
  • 7. Leiden Cryogenics B.V. Still Mixing Chamber Dilution Refrigerators 3K plate Heat Exchangers JT Heat Exchanger Room temperature pumping system 3K plate JT Heat Exchanger Still Heat Exchangers Mixing Chamber 50K plate Pulse tube
  • 8. Leiden Cryogenics B.V. Still Mixing Chamber Dilution Refrigerators; Operation principle 3K plate Heat Exchangers JT Heat Exchanger gas flow
  • 9. Leiden Cryogenics B.V. Dilution Refrigerators Still Mixing Chamber 3K plate Heat Exchangers JT Heat Exchanger gas flow vapor < 1% 3He > 90% 3He 100% 3He 6% 3He
  • 10. Leiden Cryogenics B.V. CF CS81 total system
  • 11. Leiden Cryogenics B.V. New pumping system – Maglev & GX1000
  • 12. Leiden Cryogenics B.V. New model (standard)
  • 13. Leiden Cryogenics B.V. Fast cool down with the LC Probe 50K 3K Still (900mK) 50mK Mc (10mK) Tmin≤15mK Advantages:  Possibility of many wires  Easy access to center of magnet  Fast cooling down to base temperature (<5 hours)  High cooling power, up to 300W @ 120 mK
  • 14. Leiden Cryogenics B.V. Cryogen-Free DR – Specials: CUORE 1000 kg TeO2 crystals Lead shielding LC CF Dilution Refrigerator CRYOGENIC UNDERGROUND OBSERVATORY FOR RARE EVENTS Neutrinoless double-beta decay half-life of Majorana neutrinos Cooling down 17 tons!!
  • 15. Leiden Cryogenics B.V. Cryogen-Free DR– Specials: CUORE Tmin=4,5mK
  • 16. Leiden Cryogenics B.V. Our customers (>150 systems) MIT/Harvard Stanford 5 2 2 5 82 Leiden/Delft UCSB Maryland Detroit Waterloo 6 Sydney Melbourne
  • 17. Leiden Cryogenics B.V. Our compatitors Short delivery time, small models, expensive Short delivery time, small models UHV specialists Leiden Cryogenics B.V. Large models, low vibration levels Large cooling power, lowest temperature

Notes de l'éditeur

  1. 3He is lighter → larger zero point energy 4He will occupy smaller volume → binding energy for 3He atom larger than in 3He 3He is a Fermion and should obey the Pauli principle (no atoms in the same energy state) → increasing energy, so decreasing binding energy of 3He inside 4He Osmotic pressure of 3He is constant (20 mbar) Remove 3He gas from the still → will be replaced by 3He from the concentrated phase Due to a larger enthalpy of 3He in the diluted phase, cooling will occur Upside-down evaporation