Study of Titanium Surface Modification & Collagen Grafting for dental implants

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Ikhwan Hidayat

My research on Titanium surface modification using blasting, etching, 3-APTES and collagen grafting

Technologie Business

Writer: 이흐완 히다얏 Advisor: Prof. 김석영 생체재료실험실

Contents ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]

Introduction Nowadays Initially Research & Development Used to improve a patient’s masticator function Patients desired also the aesthetics , short treatment time and procedural reliability Improving Titanium’s surface activity , osseointegration and fixation Based on the discovery by Swedish Professor Per-Ingvar Brånemark , Titanium can be successfully fused into bone when osteoblasts grow on and into the rough surface of the implanted titanium Dental Implants Why Titanium?

Research Background ,[object Object],[object Object],[object Object]

Research Objectives ,[object Object],[object Object]

R&D Flow Chart Substrate: Titanium Interface: Coupling agent Coating: Collagen (type 1) Dental implants Orthopedic implant OH radical Surface Processing Collagen coating Cell Attachment/ Proliferation Materials Processing in vitro Tests Applications

Research Methodology Ti discs Polishing Treatment Heat Treatment TFAA treatment & XPS observation 3-APTES grafting SEM/EDS Observation Collagen Coating Cell Culture Blasting Chemical Treatment Surface Roughness Measurement Analysis

Research Progress ,[object Object],[object Object],[object Object],[object Object],[object Object]

Research Progress ,[object Object],[object Object],[object Object],[object Object],Fig. 1 Al 2 O 3 Blasted #200 & H 3 PO 4 Etched Table 1. HA blasted Ti discs Table 2. HA blasted - HNO 3 etching Table 3. HA blasted - H 3 PO 4 etching Element Weight% Atomic% Compd% Formula O K 39.37 65.69 98.29 O2Ti P K 1.71 1.47 0.00 Ti 58.93 32.84 Totals 100.00 Element Weight% Atomic% Compd% Formula O K 40.05 66.67 100.00 O2Ti Ti 59.95 33.33 Totals 100.00 Element Weight% Atomic% O K 30.60 55.38 P K 4.88 4.56 Ca K 9.09 6.56 Ti K 55.43 33.50 Totals 100.00

Research Progress ,[object Object],[object Object],[object Object],(a) NaOH etched (b) NaOH + 3-APTES 10 Min (c) H 2 O 2 etched (d) H 2 O 2 + 3-APTES 10 Min Chemical Temperature Concentration Time (Hr) NaOH 70 o C 5 M 24, 12 H 2 O 2 80 o C 35.4 Vol % 48, 24

Research Plans ,[object Object],[object Object],[object Object],[object Object],[object Object],[object Object],[object Object]

Terima Kasih Merci Xie xie Syukron Rahmat Danke Arigato Gracias Grazie Mahalo Salamat

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Study of Titanium Surface Modification & Collagen Grafting for dental implants

1. Writer: 이흐완 히다얏 Advisor: Prof. 김석영 생체재료실험실

3. Introduction Nowadays Initially Research & Development Used to improve a patient’s masticator function Patients desired also the aesthetics , short treatment time and procedural reliability Improving Titanium’s surface activity , osseointegration and fixation Based on the discovery by Swedish Professor Per-Ingvar Brånemark , Titanium can be successfully fused into bone when osteoblasts grow on and into the rough surface of the implanted titanium Dental Implants Why Titanium?

7. R&D Flow Chart Substrate: Titanium Interface: Coupling agent Coating: Collagen (type 1) Dental implants Orthopedic implant OH radical Surface Processing Collagen coating Cell Attachment/ Proliferation Materials Processing in vitro Tests Applications

8. Research Methodology Ti discs Polishing Treatment Heat Treatment TFAA treatment & XPS observation 3-APTES grafting SEM/EDS Observation Collagen Coating Cell Culture Blasting Chemical Treatment Surface Roughness Measurement Analysis

10.

11.

12.

13. Terima Kasih Merci Xie xie Syukron Rahmat Danke Arigato Gracias Grazie Mahalo Salamat

Study of Titanium Surface Modification & Collagen Grafting for dental implants

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