Alcohol

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Dr Shah Murad

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Formation Santé & Médecine Business

ALCOHOL Prof. Dr. Shah Murad [email_address]

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The earliest voltammetric technique Heyrovsky invented the original polarographic method in 1922, conventional direct current polarography (DCP). It employs a dropping mercury electrode (DME) to continuously renew the electrode surface. Diffusion is the mechanism of mass transport. When an external potential is applied to a cell containing a reducing substance such as CdCl2, The following reaction will occur: Cd2+ + 2e + Hg = Cd(Hg) The technique depends on increasing the applied voltage at a steady rate and simultaneously record photographically the current-voltage curve (polarogram) The apparatus used is called a polarograph . When an external potential is applied to a cell containing a reducing substance such as CdCl2, The following reaction will occur: Cd2+ + 2e + Hg = Cd(Hg) The technique depends on increasing the applied voltage at a steady rate and simultaneously record photographically the current-voltage curve (polarogram) The apparatus used is called a polarograph . Capillary tube about 10-15cm Int. diameter of 0.05mm A vertical distance being maintained betwwen DME and the solution Drop time of 1-5 seconds Drop diameter 0.5mm The supporting electrolyte is a solution of (KNO3, NaCl, Na3PO4) in which the sample (which must be electroactive) is dissolved. Function of the supporting electrolyte It raises the conductivity of the solution. It carries the bulk of the current so prevent the migration of electroactive materials to working electrode. It may control pH It may associate with the electroactive solute as in the complexing of the metal ions by ligands.

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Alcohol

1. ALCOHOL Prof. Dr. Shah Murad [email_address]

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Alcohol

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